Determination of chloramphenicol in tablets by electrogenerated chemiluminescence
Autor(a) principal: | |
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Data de Publicação: | 2004 |
Outros Autores: | |
Tipo de documento: | Artigo |
Idioma: | eng |
Título da fonte: | Journal of the Brazilian Chemical Society (Online) |
Texto Completo: | http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532004000200004 |
Resumo: | Chloramphenicol was determinate by electrogenerated chemiluminescence coupled to FIA using Ru(bpy)3(2+) luminescent complex. Chloramphenicol cause a decrease in luminescence intensity from the ruthenium complex that is proportional to its concentration between 5 x 10-5 and 1 x 10-3 mol L-1. The relative standard deviation was estimated as £ 1.5 % for 1 x 10-4 mol L-1 chloramphenicol solution of 12 successive injections. The chloramphenicol was determined in tablets with success and the soluble components of the matrix did not interfere in the luminescent emission. Results obtained with the luminescent procedure were not statistically different from those obtained by UV-spectrophotometry at the 95 % confidence level. |
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Journal of the Brazilian Chemical Society (Online) |
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Determination of chloramphenicol in tablets by electrogenerated chemiluminescenceelectrogenerated chemiluminescenceFIAchloramphenicolpharmaceutical tabletsChloramphenicol was determinate by electrogenerated chemiluminescence coupled to FIA using Ru(bpy)3(2+) luminescent complex. Chloramphenicol cause a decrease in luminescence intensity from the ruthenium complex that is proportional to its concentration between 5 x 10-5 and 1 x 10-3 mol L-1. The relative standard deviation was estimated as £ 1.5 % for 1 x 10-4 mol L-1 chloramphenicol solution of 12 successive injections. The chloramphenicol was determined in tablets with success and the soluble components of the matrix did not interfere in the luminescent emission. Results obtained with the luminescent procedure were not statistically different from those obtained by UV-spectrophotometry at the 95 % confidence level.Sociedade Brasileira de Química2004-04-01info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersiontext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532004000200004Journal of the Brazilian Chemical Society v.15 n.2 2004reponame:Journal of the Brazilian Chemical Society (Online)instname:Sociedade Brasileira de Química (SBQ)instacron:SBQ10.1590/S0103-50532004000200004info:eu-repo/semantics/openAccessLindino,Cleber AntonioBulhões,Luís Otávio S.eng2004-06-29T00:00:00Zoai:scielo:S0103-50532004000200004Revistahttp://jbcs.sbq.org.brONGhttps://old.scielo.br/oai/scielo-oai.php||office@jbcs.sbq.org.br1678-47900103-5053opendoar:2004-06-29T00:00Journal of the Brazilian Chemical Society (Online) - Sociedade Brasileira de Química (SBQ)false |
dc.title.none.fl_str_mv |
Determination of chloramphenicol in tablets by electrogenerated chemiluminescence |
title |
Determination of chloramphenicol in tablets by electrogenerated chemiluminescence |
spellingShingle |
Determination of chloramphenicol in tablets by electrogenerated chemiluminescence Lindino,Cleber Antonio electrogenerated chemiluminescence FIA chloramphenicol pharmaceutical tablets |
title_short |
Determination of chloramphenicol in tablets by electrogenerated chemiluminescence |
title_full |
Determination of chloramphenicol in tablets by electrogenerated chemiluminescence |
title_fullStr |
Determination of chloramphenicol in tablets by electrogenerated chemiluminescence |
title_full_unstemmed |
Determination of chloramphenicol in tablets by electrogenerated chemiluminescence |
title_sort |
Determination of chloramphenicol in tablets by electrogenerated chemiluminescence |
author |
Lindino,Cleber Antonio |
author_facet |
Lindino,Cleber Antonio Bulhões,Luís Otávio S. |
author_role |
author |
author2 |
Bulhões,Luís Otávio S. |
author2_role |
author |
dc.contributor.author.fl_str_mv |
Lindino,Cleber Antonio Bulhões,Luís Otávio S. |
dc.subject.por.fl_str_mv |
electrogenerated chemiluminescence FIA chloramphenicol pharmaceutical tablets |
topic |
electrogenerated chemiluminescence FIA chloramphenicol pharmaceutical tablets |
description |
Chloramphenicol was determinate by electrogenerated chemiluminescence coupled to FIA using Ru(bpy)3(2+) luminescent complex. Chloramphenicol cause a decrease in luminescence intensity from the ruthenium complex that is proportional to its concentration between 5 x 10-5 and 1 x 10-3 mol L-1. The relative standard deviation was estimated as £ 1.5 % for 1 x 10-4 mol L-1 chloramphenicol solution of 12 successive injections. The chloramphenicol was determined in tablets with success and the soluble components of the matrix did not interfere in the luminescent emission. Results obtained with the luminescent procedure were not statistically different from those obtained by UV-spectrophotometry at the 95 % confidence level. |
publishDate |
2004 |
dc.date.none.fl_str_mv |
2004-04-01 |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532004000200004 |
url |
http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532004000200004 |
dc.language.iso.fl_str_mv |
eng |
language |
eng |
dc.relation.none.fl_str_mv |
10.1590/S0103-50532004000200004 |
dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess |
eu_rights_str_mv |
openAccess |
dc.format.none.fl_str_mv |
text/html |
dc.publisher.none.fl_str_mv |
Sociedade Brasileira de Química |
publisher.none.fl_str_mv |
Sociedade Brasileira de Química |
dc.source.none.fl_str_mv |
Journal of the Brazilian Chemical Society v.15 n.2 2004 reponame:Journal of the Brazilian Chemical Society (Online) instname:Sociedade Brasileira de Química (SBQ) instacron:SBQ |
instname_str |
Sociedade Brasileira de Química (SBQ) |
instacron_str |
SBQ |
institution |
SBQ |
reponame_str |
Journal of the Brazilian Chemical Society (Online) |
collection |
Journal of the Brazilian Chemical Society (Online) |
repository.name.fl_str_mv |
Journal of the Brazilian Chemical Society (Online) - Sociedade Brasileira de Química (SBQ) |
repository.mail.fl_str_mv |
||office@jbcs.sbq.org.br |
_version_ |
1750318165694349312 |