A fast sonochemical method to prepare 1D and 3D nanostructures of bismuth sulfide
Autor(a) principal: | |
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Data de Publicação: | 2013 |
Outros Autores: | , , , |
Tipo de documento: | Artigo |
Idioma: | eng |
Título da fonte: | Journal of the Brazilian Chemical Society (Online) |
Texto Completo: | http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532013000200015 |
Resumo: | In this work, a sonochemical method to synthesize nanostructures of bismuth sulfide in 1D and 3D framework was developed and compared with a synthetic route with heating under reflux. The sonochemical method showed to be faster and more efficient than refluxing method to obtain nanostructures with high morphological homogeneity. Form and quality of the nanocrystals were dependent on the type of solvent employed in the synthesis procedure. 3D flower-like superstructures were obtained when ethylene glycol was used as solvent, while 1D nanorods were obtained when a mixture of dimethyl sulfoxide and ethylene glycol was used as solvent. |
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Journal of the Brazilian Chemical Society (Online) |
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A fast sonochemical method to prepare 1D and 3D nanostructures of bismuth sulfidebismuth sulfidesonochemical methodnanomaterialsIn this work, a sonochemical method to synthesize nanostructures of bismuth sulfide in 1D and 3D framework was developed and compared with a synthetic route with heating under reflux. The sonochemical method showed to be faster and more efficient than refluxing method to obtain nanostructures with high morphological homogeneity. Form and quality of the nanocrystals were dependent on the type of solvent employed in the synthesis procedure. 3D flower-like superstructures were obtained when ethylene glycol was used as solvent, while 1D nanorods were obtained when a mixture of dimethyl sulfoxide and ethylene glycol was used as solvent.Sociedade Brasileira de Química2013-02-01info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersiontext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532013000200015Journal of the Brazilian Chemical Society v.24 n.2 2013reponame:Journal of the Brazilian Chemical Society (Online)instname:Sociedade Brasileira de Química (SBQ)instacron:SBQ10.5935/0103-5053.20130036info:eu-repo/semantics/openAccessMesquita,Paulo R. R.Almeida,Jorge S.Teixeira,Leonardo S. G.Silva,Antônio F. daSilva,Luciana A.eng2013-05-20T00:00:00Zoai:scielo:S0103-50532013000200015Revistahttp://jbcs.sbq.org.brONGhttps://old.scielo.br/oai/scielo-oai.php||office@jbcs.sbq.org.br1678-47900103-5053opendoar:2013-05-20T00:00Journal of the Brazilian Chemical Society (Online) - Sociedade Brasileira de Química (SBQ)false |
dc.title.none.fl_str_mv |
A fast sonochemical method to prepare 1D and 3D nanostructures of bismuth sulfide |
title |
A fast sonochemical method to prepare 1D and 3D nanostructures of bismuth sulfide |
spellingShingle |
A fast sonochemical method to prepare 1D and 3D nanostructures of bismuth sulfide Mesquita,Paulo R. R. bismuth sulfide sonochemical method nanomaterials |
title_short |
A fast sonochemical method to prepare 1D and 3D nanostructures of bismuth sulfide |
title_full |
A fast sonochemical method to prepare 1D and 3D nanostructures of bismuth sulfide |
title_fullStr |
A fast sonochemical method to prepare 1D and 3D nanostructures of bismuth sulfide |
title_full_unstemmed |
A fast sonochemical method to prepare 1D and 3D nanostructures of bismuth sulfide |
title_sort |
A fast sonochemical method to prepare 1D and 3D nanostructures of bismuth sulfide |
author |
Mesquita,Paulo R. R. |
author_facet |
Mesquita,Paulo R. R. Almeida,Jorge S. Teixeira,Leonardo S. G. Silva,Antônio F. da Silva,Luciana A. |
author_role |
author |
author2 |
Almeida,Jorge S. Teixeira,Leonardo S. G. Silva,Antônio F. da Silva,Luciana A. |
author2_role |
author author author author |
dc.contributor.author.fl_str_mv |
Mesquita,Paulo R. R. Almeida,Jorge S. Teixeira,Leonardo S. G. Silva,Antônio F. da Silva,Luciana A. |
dc.subject.por.fl_str_mv |
bismuth sulfide sonochemical method nanomaterials |
topic |
bismuth sulfide sonochemical method nanomaterials |
description |
In this work, a sonochemical method to synthesize nanostructures of bismuth sulfide in 1D and 3D framework was developed and compared with a synthetic route with heating under reflux. The sonochemical method showed to be faster and more efficient than refluxing method to obtain nanostructures with high morphological homogeneity. Form and quality of the nanocrystals were dependent on the type of solvent employed in the synthesis procedure. 3D flower-like superstructures were obtained when ethylene glycol was used as solvent, while 1D nanorods were obtained when a mixture of dimethyl sulfoxide and ethylene glycol was used as solvent. |
publishDate |
2013 |
dc.date.none.fl_str_mv |
2013-02-01 |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532013000200015 |
url |
http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532013000200015 |
dc.language.iso.fl_str_mv |
eng |
language |
eng |
dc.relation.none.fl_str_mv |
10.5935/0103-5053.20130036 |
dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess |
eu_rights_str_mv |
openAccess |
dc.format.none.fl_str_mv |
text/html |
dc.publisher.none.fl_str_mv |
Sociedade Brasileira de Química |
publisher.none.fl_str_mv |
Sociedade Brasileira de Química |
dc.source.none.fl_str_mv |
Journal of the Brazilian Chemical Society v.24 n.2 2013 reponame:Journal of the Brazilian Chemical Society (Online) instname:Sociedade Brasileira de Química (SBQ) instacron:SBQ |
instname_str |
Sociedade Brasileira de Química (SBQ) |
instacron_str |
SBQ |
institution |
SBQ |
reponame_str |
Journal of the Brazilian Chemical Society (Online) |
collection |
Journal of the Brazilian Chemical Society (Online) |
repository.name.fl_str_mv |
Journal of the Brazilian Chemical Society (Online) - Sociedade Brasileira de Química (SBQ) |
repository.mail.fl_str_mv |
||office@jbcs.sbq.org.br |
_version_ |
1750318174476173312 |