Propriedades mecânicas das ligas Ti34Cu36Ni8Zr22 e (TiZr)80Co12Fe8

Detalhes bibliográficos
Autor(a) principal: Medeiros, Marcia Moreira
Data de Publicação: 2012
Tipo de documento: Tese
Idioma: por
Título da fonte: Repositório Institucional da UFSCAR
Texto Completo: https://repositorio.ufscar.br/handle/ufscar/701
Resumo: Bulk amorphous and nanocrystalline alloys have attracted great interest from the scientific community. Titanium based alloys have demonstrated potential for formation of amorphous. This study aimed at to evaluate the mechanical properties of the Ti34Cu36Ni8Zr22 and (TiZr)80Co12Fe8 alloys, at room temperature. Thereby, nanoindentation, compression and three points bending tests were performed. The methodology involved the following steps: (i) production of alloys by arc melting under argon atmosphere, (ii) production of amorphous ribbon by melt-spinning, (iii) heat treatment of the ribbons at different temperatures, (iv) production of test specimens through casting in copper chill followed by quenching (v) microstructural characterization via scanning electron microscopy (SEM) with energy dispersive spectroscopy (EDS), transmission electron microscopy (TEM), differential scanning calorimetry (DSC) and X-ray diffraction (XRD), (vi) mechanical characterization based on nanoindentation, compression and torsion tests. The results of nanoindentation showed an increase in hardness and reduced Young's modulus as the temperature of the heat treatment approachs the crystallization temperature. Results of compression and bending showed strong dependence on the preparation surface and internal defects of the specimens. The Young's modules and tensile strengths are below those reported in the literature, probably due to internal defects present in the samples such as pores.
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spelling Medeiros, Marcia MoreiraBolfarini, Claudemirohttp://lattes.cnpq.br/9231627080617037http://lattes.cnpq.br/82603911215439622016-06-02T19:10:13Z2012-12-122016-06-02T19:10:13Z2012-03-23MEDEIROS, Marcia Moreira. Mechanical Properties of Ti34Cu36Ni8Zr22 and (TiZr)80Co12Fe8 Alloys. 2012. 98 f. Tese (Doutorado em Ciências Exatas e da Terra) - Universidade Federal de São Carlos, São Carlos, 2012.https://repositorio.ufscar.br/handle/ufscar/701Bulk amorphous and nanocrystalline alloys have attracted great interest from the scientific community. Titanium based alloys have demonstrated potential for formation of amorphous. This study aimed at to evaluate the mechanical properties of the Ti34Cu36Ni8Zr22 and (TiZr)80Co12Fe8 alloys, at room temperature. Thereby, nanoindentation, compression and three points bending tests were performed. The methodology involved the following steps: (i) production of alloys by arc melting under argon atmosphere, (ii) production of amorphous ribbon by melt-spinning, (iii) heat treatment of the ribbons at different temperatures, (iv) production of test specimens through casting in copper chill followed by quenching (v) microstructural characterization via scanning electron microscopy (SEM) with energy dispersive spectroscopy (EDS), transmission electron microscopy (TEM), differential scanning calorimetry (DSC) and X-ray diffraction (XRD), (vi) mechanical characterization based on nanoindentation, compression and torsion tests. The results of nanoindentation showed an increase in hardness and reduced Young's modulus as the temperature of the heat treatment approachs the crystallization temperature. Results of compression and bending showed strong dependence on the preparation surface and internal defects of the specimens. The Young's modules and tensile strengths are below those reported in the literature, probably due to internal defects present in the samples such as pores.Ligas amorfas e nanocristalinas de grande volume vêm despertando grande interesse da comunidade científica. Ligas à base de titânio têm demonstrado potencial para formação de amorfo. O presente estudo objetivou avaliar as propriedades mecânicas, em temperatura ambiente, das ligas Ti34Cu36Ni8Zr22 e (TiZr)80Co12Fe8. Para tanto, foram realizados ensaios de nanoindentação, compressão e flexão em três pontos. A metodologia empregada envolveu as seguintes etapas: (i) produção das ligas via fusão a arco sob atmosfera de argônio; (ii) produção de fitas amorfas via melt-spinning, (iii) tratamento térmico das fitas em diferentes temperaturas, (iv) produção de corpos de prova através do vazamento em coquilha de cobre seguido de resfriamento rápido; (v) caracterização microestrutural através de microscopia eletrônica de varredura (MEV) com espectroscopia por dispersão de energia (EDS), microscopia eletrônica de transmissão (MET), calorimetria exploratória de varredura (DSC) e difratometria de raios-X (DRX); (vi) caracterização mecânica baseada em ensaios de nanoindentação, compressão e flexão em três pontos. Os resultados de nanoindentação mostraram um aumento nos valores de dureza e módulo de Young reduzido conforme o tratamento térmico se aproxima da liga cristalina. Resultados de compressão e flexão mostraram forte dependência em relação a preparação superficial e defeitos internos dos corpos de prova. Os módulos de Young e tensão de ruptura estão abaixo dos relatados pela literatura, provavelmente devido a defeitos internos presentes nas amostras, como poros.Financiadora de Estudos e Projetosapplication/pdfporUniversidade Federal de São CarlosPrograma de Pós-Graduação em Ciência e Engenharia de Materiais - PPGCEMUFSCarBRPropriedades mecânicasLigas de titânioMetal amorfoENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICAPropriedades mecânicas das ligas Ti34Cu36Ni8Zr22 e (TiZr)80Co12Fe8Mechanical Properties of Ti34Cu36Ni8Zr22 and (TiZr)80Co12Fe8 Alloysinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/doctoralThesisinfo:eu-repo/semantics/openAccessreponame:Repositório Institucional da UFSCARinstname:Universidade Federal de São Carlos (UFSCAR)instacron:UFSCARORIGINAL4739.pdfapplication/pdf8852417https://{{ getenv "DSPACE_HOST" "repositorio.ufscar.br" }}/bitstream/ufscar/701/1/4739.pdf54d6a4b01ec455b6d6fc320e63d6dc26MD51TEXT4739.pdf.txt4739.pdf.txtExtracted texttext/plain0https://{{ getenv "DSPACE_HOST" "repositorio.ufscar.br" }}/bitstream/ufscar/701/2/4739.pdf.txtd41d8cd98f00b204e9800998ecf8427eMD52THUMBNAIL4739.pdf.jpg4739.pdf.jpgIM Thumbnailimage/jpeg5770https://{{ getenv "DSPACE_HOST" "repositorio.ufscar.br" }}/bitstream/ufscar/701/3/4739.pdf.jpg1651e55ca996d95ccf13433c5a65fbe4MD53ufscar/7012019-09-11 04:03:31.86oai:repositorio.ufscar.br:ufscar/701Repositório InstitucionalPUBhttps://repositorio.ufscar.br/oai/requestopendoar:43222019-09-11T04:03:31Repositório Institucional da UFSCAR - Universidade Federal de São Carlos (UFSCAR)false
dc.title.por.fl_str_mv Propriedades mecânicas das ligas Ti34Cu36Ni8Zr22 e (TiZr)80Co12Fe8
dc.title.alternative.eng.fl_str_mv Mechanical Properties of Ti34Cu36Ni8Zr22 and (TiZr)80Co12Fe8 Alloys
title Propriedades mecânicas das ligas Ti34Cu36Ni8Zr22 e (TiZr)80Co12Fe8
spellingShingle Propriedades mecânicas das ligas Ti34Cu36Ni8Zr22 e (TiZr)80Co12Fe8
Medeiros, Marcia Moreira
Propriedades mecânicas
Ligas de titânio
Metal amorfo
ENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA
title_short Propriedades mecânicas das ligas Ti34Cu36Ni8Zr22 e (TiZr)80Co12Fe8
title_full Propriedades mecânicas das ligas Ti34Cu36Ni8Zr22 e (TiZr)80Co12Fe8
title_fullStr Propriedades mecânicas das ligas Ti34Cu36Ni8Zr22 e (TiZr)80Co12Fe8
title_full_unstemmed Propriedades mecânicas das ligas Ti34Cu36Ni8Zr22 e (TiZr)80Co12Fe8
title_sort Propriedades mecânicas das ligas Ti34Cu36Ni8Zr22 e (TiZr)80Co12Fe8
author Medeiros, Marcia Moreira
author_facet Medeiros, Marcia Moreira
author_role author
dc.contributor.authorlattes.por.fl_str_mv http://lattes.cnpq.br/8260391121543962
dc.contributor.author.fl_str_mv Medeiros, Marcia Moreira
dc.contributor.advisor1.fl_str_mv Bolfarini, Claudemiro
dc.contributor.advisor1Lattes.fl_str_mv http://lattes.cnpq.br/9231627080617037
contributor_str_mv Bolfarini, Claudemiro
dc.subject.por.fl_str_mv Propriedades mecânicas
Ligas de titânio
Metal amorfo
topic Propriedades mecânicas
Ligas de titânio
Metal amorfo
ENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA
dc.subject.cnpq.fl_str_mv ENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA
description Bulk amorphous and nanocrystalline alloys have attracted great interest from the scientific community. Titanium based alloys have demonstrated potential for formation of amorphous. This study aimed at to evaluate the mechanical properties of the Ti34Cu36Ni8Zr22 and (TiZr)80Co12Fe8 alloys, at room temperature. Thereby, nanoindentation, compression and three points bending tests were performed. The methodology involved the following steps: (i) production of alloys by arc melting under argon atmosphere, (ii) production of amorphous ribbon by melt-spinning, (iii) heat treatment of the ribbons at different temperatures, (iv) production of test specimens through casting in copper chill followed by quenching (v) microstructural characterization via scanning electron microscopy (SEM) with energy dispersive spectroscopy (EDS), transmission electron microscopy (TEM), differential scanning calorimetry (DSC) and X-ray diffraction (XRD), (vi) mechanical characterization based on nanoindentation, compression and torsion tests. The results of nanoindentation showed an increase in hardness and reduced Young's modulus as the temperature of the heat treatment approachs the crystallization temperature. Results of compression and bending showed strong dependence on the preparation surface and internal defects of the specimens. The Young's modules and tensile strengths are below those reported in the literature, probably due to internal defects present in the samples such as pores.
publishDate 2012
dc.date.available.fl_str_mv 2012-12-12
2016-06-02T19:10:13Z
dc.date.issued.fl_str_mv 2012-03-23
dc.date.accessioned.fl_str_mv 2016-06-02T19:10:13Z
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dc.identifier.citation.fl_str_mv MEDEIROS, Marcia Moreira. Mechanical Properties of Ti34Cu36Ni8Zr22 and (TiZr)80Co12Fe8 Alloys. 2012. 98 f. Tese (Doutorado em Ciências Exatas e da Terra) - Universidade Federal de São Carlos, São Carlos, 2012.
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