Caracterização da interface entre cilindros de pilares de implante e ligas fundidas de Co-Cr com diferentes técnicas de fundição

Detalhes bibliográficos
Autor(a) principal: Rodrigues Neto, Dimas João
Data de Publicação: 2017
Tipo de documento: Tese
Idioma: por
Título da fonte: Biblioteca Digital de Teses e Dissertações da PUC_RS
Texto Completo: http://tede2.pucrs.br/tede2/handle/tede/7369
Resumo: For a satisfactory clinical performance, pre-fabricated Co-Cr cylinders must have metallurgical compatibility to Co-Cr based cast alloys. A uniform interface with adequate union and resistance, with absence of interfacial reaction and porosities must be obtained. The present in vitro study aimed to evaluate the metallurgical compatibility at the interface between pre-fabricated Co-Cr cylinders and alloys for Co-Cr compound casting applying different casting techniques. In manuscript 2 the metallurgical compatibility and the interface between implant and alloy cylinders were evaluated for Co-Cr casting with different melting temperatures. Methodology: Three pre-fabricated Co-Cr prosthetic implant cylinders (Neodent, Pi-Brånemark, Dentium) were subjected to casting with Co-Cr alloy using different casting techniques (Flame Torch, Induction / Centrifugation, Induction / Vacuum). Optical microscopy and Scanning Electron Microscopy (SEM) were used to characterize the obtained microstructures. The elementary composition of the cylinders and diffusion characteristics in the interfacial region between molten alloy and cylinder were determined by dispersive energy spectroscopy (EDS). Vickers microhardness was measured at interface, cylinder and cast alloy. The ANOVA and Tukey test were used to evaluate microhardness values. In the manuscript 2 cylinders based on Co-Cr were overfused with alloys with different melting temperatures and all microstructural analysis and microhardness tests were performed. Results: In the manuscript 1 a union between pre-fabricated cylinders and Co-Cr based alloys was observed microstructurally. An ideal interface was obtained with absence of interfacial reaction or significant porosities with the casting with the induction techniques (centrifugation and vacuum), but excess of porosities and failures were observed with the Torch casting technique. In manuscript 2 a microstructural bond was observed between the alloys and the cylinder, evidencing that both high melt alloy and low melt alloy presented compatibility with the Co-Cr cylinder. Microhardness values, both in manuscript 1 and in manuscript 2 also proved to form a satisfactory interface. Conclusions: It was concluded from manuscript 1 and 2 that both high and low melt temperature Co-Cr have metallurgical compatibility to pre-fabricated Co-Cr cylinders, showing an ideal interface. However, the technique of casting applied is relevant, and the torch technique has been shown to be less indicated due to the lack of standardization of the obtained results.
id P_RS_f095a1ff59858b0a00a66674e699d544
oai_identifier_str oai:tede2.pucrs.br:tede/7369
network_acronym_str P_RS
network_name_str Biblioteca Digital de Teses e Dissertações da PUC_RS
repository_id_str
spelling Teixeira, Eduardo Rolim389.514.950-00http://buscatextual.cnpq.br/buscatextual/visualizacv.do?id=K4799729E6042.411.299-00http://buscatextual.cnpq.br/buscatextual/visualizacv.do?id=K4443395U7Rodrigues Neto, Dimas João2017-06-26T14:53:16Z2017-01-19http://tede2.pucrs.br/tede2/handle/tede/7369For a satisfactory clinical performance, pre-fabricated Co-Cr cylinders must have metallurgical compatibility to Co-Cr based cast alloys. A uniform interface with adequate union and resistance, with absence of interfacial reaction and porosities must be obtained. The present in vitro study aimed to evaluate the metallurgical compatibility at the interface between pre-fabricated Co-Cr cylinders and alloys for Co-Cr compound casting applying different casting techniques. In manuscript 2 the metallurgical compatibility and the interface between implant and alloy cylinders were evaluated for Co-Cr casting with different melting temperatures. Methodology: Three pre-fabricated Co-Cr prosthetic implant cylinders (Neodent, Pi-Brånemark, Dentium) were subjected to casting with Co-Cr alloy using different casting techniques (Flame Torch, Induction / Centrifugation, Induction / Vacuum). Optical microscopy and Scanning Electron Microscopy (SEM) were used to characterize the obtained microstructures. The elementary composition of the cylinders and diffusion characteristics in the interfacial region between molten alloy and cylinder were determined by dispersive energy spectroscopy (EDS). Vickers microhardness was measured at interface, cylinder and cast alloy. The ANOVA and Tukey test were used to evaluate microhardness values. In the manuscript 2 cylinders based on Co-Cr were overfused with alloys with different melting temperatures and all microstructural analysis and microhardness tests were performed. Results: In the manuscript 1 a union between pre-fabricated cylinders and Co-Cr based alloys was observed microstructurally. An ideal interface was obtained with absence of interfacial reaction or significant porosities with the casting with the induction techniques (centrifugation and vacuum), but excess of porosities and failures were observed with the Torch casting technique. In manuscript 2 a microstructural bond was observed between the alloys and the cylinder, evidencing that both high melt alloy and low melt alloy presented compatibility with the Co-Cr cylinder. Microhardness values, both in manuscript 1 and in manuscript 2 also proved to form a satisfactory interface. Conclusions: It was concluded from manuscript 1 and 2 that both high and low melt temperature Co-Cr have metallurgical compatibility to pre-fabricated Co-Cr cylinders, showing an ideal interface. However, the technique of casting applied is relevant, and the torch technique has been shown to be less indicated due to the lack of standardization of the obtained results.Para um bom desempenho clinico, cilindros de pilares pré fabricados de Co-Cr devem apresentar compatibilidade metalúrgica a ligas de sobrefundição a base de Co-Cr. Uma interface uniforme com adequada união e resistência, com ausência de reação interfacial e porosidades devem ser obtidas. O presente estudo, in vitro, objetivou através do manuscrito 1 avaliar a compatibilidade metalúrgica na interface entre cilindros pré fabricados de Co-Cr e ligas para sobrefundição de Co-Cr com diferentes técnicas de fundição. No manuscrito 2, foi avaliado a compatibilidade metalúrgica e a interface entre cilindro de implante e ligas para sobrefundição de Co-Cr com diferentes temperaturas de fusão. Metodologia: Três cilindros pré-fabricados para prótese sobre implantes em Co-Cr (Neodent, Pi-Brånemark, Dentium) foram sorefundidos com liga de Co-Cr com diferentes técnicas de fundição (Maçarico, Indução/centrifugação, Indução/vácuo). Microscopia óptica e Microscopia eletrônica de varredura (MEV) foram usadas para caracterização das microestruturas. A composição elemental dos cilindros e características de difusão na região interfacial entre liga fundida e cilindro foram determinadas através de espectroscopia por energia dispersiva (EDS). Microdureza de Vickers foi aplicada na interface, cilindro e liga fundida. Foi aplicado o teste de ANOVA e Tukey para avaliação dos valores microdureza. No manuscrito 2, cilindros a base de Co-Cr foram sobrefundidos com ligas com diferentes temperaturas de fusão e foi realizada toda analise microestrutural e testes de microdureza. Resultados: No manuscrito 1 observou-se microestruturalmente uma união entre cilindros pré fabricados e ligas a base de Co-Cr. Foi obtida uma interface ideal com ausência de reação interfacial ou porosidades significantes com a fundição com as técnicas por indução (centrifugação e vácuo), porém excesso de porosidades e falhas foram observados com a técnica de fundição à maçarico. No manuscrito 2 observou-se uma união microestrutural entre as ligas e o cilindro avaliado, evidenciando que tanto liga de alta fusão, quanto de baixa fusão apresentam compatibilidade ao cilindro de Co-Cr. Valores de microdureza, tanto no manuscrito 1 como no manuscrito 2 também comprovaram a formação de uma interface satisfatória. Conclusões: Concluiu-se através do manuscrito 1 e 2 que ligas de alta e baixa temperatura de fusão a base de Co-Cr apresentam compatibilidade metalurgica a cilindros pré fabricados de Co-Cr apresentando uma interface ideal. Porém, a técnica de fundição aplicada é relevante, sendo que a técnica à maçarico se mostra a menos indicada devido a falta de padronização dos resultados obtidos.Submitted by Caroline Xavier (caroline.xavier@pucrs.br) on 2017-06-26T14:53:16Z No. of bitstreams: 1 TES_DIMAS_JOAO_RODRIGUES_NETO_PARCIAL.pdf: 405454 bytes, checksum: d48967a61777e3e773d5a2112997ee13 (MD5)Made available in DSpace on 2017-06-26T14:53:16Z (GMT). No. of bitstreams: 1 TES_DIMAS_JOAO_RODRIGUES_NETO_PARCIAL.pdf: 405454 bytes, checksum: d48967a61777e3e773d5a2112997ee13 (MD5) Previous issue date: 2017-01-19Coordenação de Aperfeiçoamento de Pessoal de Nível Superior - CAPESapplication/pdfhttp://tede2.pucrs.br:80/tede2/retrieve/168755/TES_DIMAS_JOAO_RODRIGUES_NETO_PARCIAL.pdf.jpgporPontifícia Universidade Católica do Rio Grande do SulPrograma de Pós-Graduação em OdontologiaPUCRSBrasilFaculdade de OdontologiaFundição OdontológicaLigas OdontológicasCo-Cr LigasImplantes DentáriosPilares ProtéticosCIENCIAS DA SAUDE::ODONTOLOGIACaracterização da interface entre cilindros de pilares de implante e ligas fundidas de Co-Cr com diferentes técnicas de fundiçãoinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/doctoralThesis-80965548187336651646006006006004673435736271820140-20704984698792443492075167498588264571info:eu-repo/semantics/openAccessreponame:Biblioteca Digital de Teses e Dissertações da PUC_RSinstname:Pontifícia Universidade Católica do Rio Grande do Sul (PUCRS)instacron:PUC_RSTHUMBNAILTES_DIMAS_JOAO_RODRIGUES_NETO_PARCIAL.pdf.jpgTES_DIMAS_JOAO_RODRIGUES_NETO_PARCIAL.pdf.jpgimage/jpeg3552http://tede2.pucrs.br/tede2/bitstream/tede/7369/5/TES_DIMAS_JOAO_RODRIGUES_NETO_PARCIAL.pdf.jpgd670a241e6714f4a75e5ad67724f807bMD55TEXTTES_DIMAS_JOAO_RODRIGUES_NETO_PARCIAL.pdf.txtTES_DIMAS_JOAO_RODRIGUES_NETO_PARCIAL.pdf.txttext/plain17206http://tede2.pucrs.br/tede2/bitstream/tede/7369/4/TES_DIMAS_JOAO_RODRIGUES_NETO_PARCIAL.pdf.txt15a601104793f0653c69215cd9d21277MD54LICENSElicense.txtlicense.txttext/plain; charset=utf-8590http://tede2.pucrs.br/tede2/bitstream/tede/7369/3/license.txt220e11f2d3ba5354f917c7035aadef24MD53ORIGINALTES_DIMAS_JOAO_RODRIGUES_NETO_PARCIAL.pdfTES_DIMAS_JOAO_RODRIGUES_NETO_PARCIAL.pdfapplication/pdf405454http://tede2.pucrs.br/tede2/bitstream/tede/7369/2/TES_DIMAS_JOAO_RODRIGUES_NETO_PARCIAL.pdfd48967a61777e3e773d5a2112997ee13MD52tede/73692017-06-26 12:00:36.393oai:tede2.pucrs.br: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Biblioteca Digital de Teses e Dissertaçõeshttp://tede2.pucrs.br/tede2/PRIhttps://tede2.pucrs.br/oai/requestbiblioteca.central@pucrs.br||opendoar:2017-06-26T15:00:36Biblioteca Digital de Teses e Dissertações da PUC_RS - Pontifícia Universidade Católica do Rio Grande do Sul (PUCRS)false
dc.title.por.fl_str_mv Caracterização da interface entre cilindros de pilares de implante e ligas fundidas de Co-Cr com diferentes técnicas de fundição
title Caracterização da interface entre cilindros de pilares de implante e ligas fundidas de Co-Cr com diferentes técnicas de fundição
spellingShingle Caracterização da interface entre cilindros de pilares de implante e ligas fundidas de Co-Cr com diferentes técnicas de fundição
Rodrigues Neto, Dimas João
Fundição Odontológica
Ligas Odontológicas
Co-Cr Ligas
Implantes Dentários
Pilares Protéticos
CIENCIAS DA SAUDE::ODONTOLOGIA
title_short Caracterização da interface entre cilindros de pilares de implante e ligas fundidas de Co-Cr com diferentes técnicas de fundição
title_full Caracterização da interface entre cilindros de pilares de implante e ligas fundidas de Co-Cr com diferentes técnicas de fundição
title_fullStr Caracterização da interface entre cilindros de pilares de implante e ligas fundidas de Co-Cr com diferentes técnicas de fundição
title_full_unstemmed Caracterização da interface entre cilindros de pilares de implante e ligas fundidas de Co-Cr com diferentes técnicas de fundição
title_sort Caracterização da interface entre cilindros de pilares de implante e ligas fundidas de Co-Cr com diferentes técnicas de fundição
author Rodrigues Neto, Dimas João
author_facet Rodrigues Neto, Dimas João
author_role author
dc.contributor.advisor1.fl_str_mv Teixeira, Eduardo Rolim
dc.contributor.advisor1ID.fl_str_mv 389.514.950-00
dc.contributor.advisor1Lattes.fl_str_mv http://buscatextual.cnpq.br/buscatextual/visualizacv.do?id=K4799729E6
dc.contributor.authorID.fl_str_mv 042.411.299-00
dc.contributor.authorLattes.fl_str_mv http://buscatextual.cnpq.br/buscatextual/visualizacv.do?id=K4443395U7
dc.contributor.author.fl_str_mv Rodrigues Neto, Dimas João
contributor_str_mv Teixeira, Eduardo Rolim
dc.subject.por.fl_str_mv Fundição Odontológica
Ligas Odontológicas
Co-Cr Ligas
Implantes Dentários
Pilares Protéticos
topic Fundição Odontológica
Ligas Odontológicas
Co-Cr Ligas
Implantes Dentários
Pilares Protéticos
CIENCIAS DA SAUDE::ODONTOLOGIA
dc.subject.cnpq.fl_str_mv CIENCIAS DA SAUDE::ODONTOLOGIA
description For a satisfactory clinical performance, pre-fabricated Co-Cr cylinders must have metallurgical compatibility to Co-Cr based cast alloys. A uniform interface with adequate union and resistance, with absence of interfacial reaction and porosities must be obtained. The present in vitro study aimed to evaluate the metallurgical compatibility at the interface between pre-fabricated Co-Cr cylinders and alloys for Co-Cr compound casting applying different casting techniques. In manuscript 2 the metallurgical compatibility and the interface between implant and alloy cylinders were evaluated for Co-Cr casting with different melting temperatures. Methodology: Three pre-fabricated Co-Cr prosthetic implant cylinders (Neodent, Pi-Brånemark, Dentium) were subjected to casting with Co-Cr alloy using different casting techniques (Flame Torch, Induction / Centrifugation, Induction / Vacuum). Optical microscopy and Scanning Electron Microscopy (SEM) were used to characterize the obtained microstructures. The elementary composition of the cylinders and diffusion characteristics in the interfacial region between molten alloy and cylinder were determined by dispersive energy spectroscopy (EDS). Vickers microhardness was measured at interface, cylinder and cast alloy. The ANOVA and Tukey test were used to evaluate microhardness values. In the manuscript 2 cylinders based on Co-Cr were overfused with alloys with different melting temperatures and all microstructural analysis and microhardness tests were performed. Results: In the manuscript 1 a union between pre-fabricated cylinders and Co-Cr based alloys was observed microstructurally. An ideal interface was obtained with absence of interfacial reaction or significant porosities with the casting with the induction techniques (centrifugation and vacuum), but excess of porosities and failures were observed with the Torch casting technique. In manuscript 2 a microstructural bond was observed between the alloys and the cylinder, evidencing that both high melt alloy and low melt alloy presented compatibility with the Co-Cr cylinder. Microhardness values, both in manuscript 1 and in manuscript 2 also proved to form a satisfactory interface. Conclusions: It was concluded from manuscript 1 and 2 that both high and low melt temperature Co-Cr have metallurgical compatibility to pre-fabricated Co-Cr cylinders, showing an ideal interface. However, the technique of casting applied is relevant, and the torch technique has been shown to be less indicated due to the lack of standardization of the obtained results.
publishDate 2017
dc.date.accessioned.fl_str_mv 2017-06-26T14:53:16Z
dc.date.issued.fl_str_mv 2017-01-19
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/doctoralThesis
format doctoralThesis
status_str publishedVersion
dc.identifier.uri.fl_str_mv http://tede2.pucrs.br/tede2/handle/tede/7369
url http://tede2.pucrs.br/tede2/handle/tede/7369
dc.language.iso.fl_str_mv por
language por
dc.relation.program.fl_str_mv -8096554818733665164
dc.relation.confidence.fl_str_mv 600
600
600
600
dc.relation.department.fl_str_mv 4673435736271820140
dc.relation.cnpq.fl_str_mv -2070498469879244349
dc.relation.sponsorship.fl_str_mv 2075167498588264571
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv application/pdf
dc.publisher.none.fl_str_mv Pontifícia Universidade Católica do Rio Grande do Sul
dc.publisher.program.fl_str_mv Programa de Pós-Graduação em Odontologia
dc.publisher.initials.fl_str_mv PUCRS
dc.publisher.country.fl_str_mv Brasil
dc.publisher.department.fl_str_mv Faculdade de Odontologia
publisher.none.fl_str_mv Pontifícia Universidade Católica do Rio Grande do Sul
dc.source.none.fl_str_mv reponame:Biblioteca Digital de Teses e Dissertações da PUC_RS
instname:Pontifícia Universidade Católica do Rio Grande do Sul (PUCRS)
instacron:PUC_RS
instname_str Pontifícia Universidade Católica do Rio Grande do Sul (PUCRS)
instacron_str PUC_RS
institution PUC_RS
reponame_str Biblioteca Digital de Teses e Dissertações da PUC_RS
collection Biblioteca Digital de Teses e Dissertações da PUC_RS
bitstream.url.fl_str_mv http://tede2.pucrs.br/tede2/bitstream/tede/7369/5/TES_DIMAS_JOAO_RODRIGUES_NETO_PARCIAL.pdf.jpg
http://tede2.pucrs.br/tede2/bitstream/tede/7369/4/TES_DIMAS_JOAO_RODRIGUES_NETO_PARCIAL.pdf.txt
http://tede2.pucrs.br/tede2/bitstream/tede/7369/3/license.txt
http://tede2.pucrs.br/tede2/bitstream/tede/7369/2/TES_DIMAS_JOAO_RODRIGUES_NETO_PARCIAL.pdf
bitstream.checksum.fl_str_mv d670a241e6714f4a75e5ad67724f807b
15a601104793f0653c69215cd9d21277
220e11f2d3ba5354f917c7035aadef24
d48967a61777e3e773d5a2112997ee13
bitstream.checksumAlgorithm.fl_str_mv MD5
MD5
MD5
MD5
repository.name.fl_str_mv Biblioteca Digital de Teses e Dissertações da PUC_RS - Pontifícia Universidade Católica do Rio Grande do Sul (PUCRS)
repository.mail.fl_str_mv biblioteca.central@pucrs.br||
_version_ 1799765325463420928