Development of powder mixtures of pulp and acerola papaya.

Detalhes bibliográficos
Autor(a) principal: Silas Rafael Figueiredo de AraÃjo
Data de Publicação: 2013
Tipo de documento: Dissertação
Idioma: por
Título da fonte: Biblioteca Digital de Teses e Dissertações da UFC
Texto Completo: http://www.teses.ufc.br/tde_busca/arquivo.php?codArquivo=10025
Resumo: The acerola tropical fruit and papaya are of great industrial interest for its nutritional and sensory characteristics. Due to the perishable nature of these fruits to adopt conservation methods is necessary. The present study aimed at obtaining "blends" powder from freeze-drying the pulp of acerola and papaya. First were performed compounds central rotational schedules, which evaluated the influence of lyophilization time and maltodextrin concentration and humidity on the hygroscopicity of the powders. From the results of the design were produced powders from acerola and papaya in optimal process conditions based on lower hygroscopicity, moisture was not considered by the planning because the powders obtained were within the standards established by Brazilian legislation. From the physico-chemical characterizations of the pulps and the pulps fresh powder was noticed good nutritional quality for both pulps primarily by ascorbic acid, in addition to considerable amounts of anthocyanins and carotenoids in relation to adsorption isotherms both the powders exhibited type III curves concave-shaped "J" typically associated with the food powders from fruit, yet papaya pulp powder showed reversal of the effect of temperature on adsorption capacity for water a range of water activity of 0,8. The Oswin model was the best fit curves for the prediction of the pulp powder at all temperatures analyzed for papaya pulp, the model proposed by BET was the best fit the data. Then experiment was conducted mixtures simplex centroid increased to three components (acerola pulp, papaya pulp and maltodextrin) to obtain the "blend" lyophilized powder, by determining the effect of the proportions of the mixture on the hygroscopicity , solubility, time and degree of rehydration Caking. The time lyophilization of "blends" was the simple arithmetic average between the times of lyophilization obtained by central composite design for the pulp powder acerola and papaya. The results of qualitative analysis of the mixture enabled the choice of test 6 with the proportions 25% acerola pulp, 50% papaya pulp and 25% maltodextrin as best assay for production of "blend" powder. The "blend" powder obtained under optimum conditions showed good physicochemical characteristics, in relation to sorption isotherms, the GAB model was the best fit the experimental data, where the curves were type III. Then there was the study of the stability of the "blend" powder in storage period of 20 days packed in polyethylene wrapped in aluminum foil. Thus, it was concluded that, after this storage period, the "blend" powder, the patient was still in powder form and has good chemical-physical characteristics and hygroscopic.
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spelling info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/masterThesisDevelopment of powder mixtures of pulp and acerola papaya.ElaboraÃÃo de misturas em pà das polpas de acerola e mamÃo2013-04-15Marcos Rodrigues Amorim Afonso15232275836http://buscatextual.cnpq.br/buscatextual/visualizacv.jsp?id=K4701595T6&dataRevisao=nullSueli Rodrigues19633877830http://buscatextual.cnpq.br/buscatextual/visualizacv.jsp?id=K4707745Z6LuciclÃia Barros de Vasconcelos Torres02749067405http://buscatextual.cnpq.br/buscatextual/visualizacv.do?id=K4778490E600322529271http://buscatextual.cnpq.br/buscatextual/visualizacv.do?id=K4208608Y1Silas Rafael Figueiredo de AraÃjoUniversidade Federal do CearÃPrograma de PÃs-GraduaÃÃo em CiÃncia e Tecnologia de AlimentosUFCBRIsotermas higroscopicidade blendIsotermas higroscopicidade blendIsotherms hygroscopicity blendCIENCIA E TECNOLOGIA DE ALIMENTOSThe acerola tropical fruit and papaya are of great industrial interest for its nutritional and sensory characteristics. Due to the perishable nature of these fruits to adopt conservation methods is necessary. The present study aimed at obtaining "blends" powder from freeze-drying the pulp of acerola and papaya. First were performed compounds central rotational schedules, which evaluated the influence of lyophilization time and maltodextrin concentration and humidity on the hygroscopicity of the powders. From the results of the design were produced powders from acerola and papaya in optimal process conditions based on lower hygroscopicity, moisture was not considered by the planning because the powders obtained were within the standards established by Brazilian legislation. From the physico-chemical characterizations of the pulps and the pulps fresh powder was noticed good nutritional quality for both pulps primarily by ascorbic acid, in addition to considerable amounts of anthocyanins and carotenoids in relation to adsorption isotherms both the powders exhibited type III curves concave-shaped "J" typically associated with the food powders from fruit, yet papaya pulp powder showed reversal of the effect of temperature on adsorption capacity for water a range of water activity of 0,8. The Oswin model was the best fit curves for the prediction of the pulp powder at all temperatures analyzed for papaya pulp, the model proposed by BET was the best fit the data. Then experiment was conducted mixtures simplex centroid increased to three components (acerola pulp, papaya pulp and maltodextrin) to obtain the "blend" lyophilized powder, by determining the effect of the proportions of the mixture on the hygroscopicity , solubility, time and degree of rehydration Caking. The time lyophilization of "blends" was the simple arithmetic average between the times of lyophilization obtained by central composite design for the pulp powder acerola and papaya. The results of qualitative analysis of the mixture enabled the choice of test 6 with the proportions 25% acerola pulp, 50% papaya pulp and 25% maltodextrin as best assay for production of "blend" powder. The "blend" powder obtained under optimum conditions showed good physicochemical characteristics, in relation to sorption isotherms, the GAB model was the best fit the experimental data, where the curves were type III. Then there was the study of the stability of the "blend" powder in storage period of 20 days packed in polyethylene wrapped in aluminum foil. Thus, it was concluded that, after this storage period, the "blend" powder, the patient was still in powder form and has good chemical-physical characteristics and hygroscopic.A acerola e mamÃo sÃo frutos tropicais de grande interesse industrial por suas caracterÃsticas nutricionais e sensoriais. Em virtude do carÃter perecÃvel desses frutos a adoÃÃo de mÃtodos de conservaÃÃo faz-se necessÃria. O presente trabalho teve como objetivo obter âblendsâ em pà a partir da liofilizaÃÃo das polpas de acerola e mamÃo. Primeiramente foram realizados planejamentos compostos central rotacionais, onde se avaliou a influÃncia do tempo de liofilizaÃÃo e concentraÃÃo de maltodextrina sobre a higroscopicidade e umidade dos pÃs obtidos. A partir dos resultados do planejamento foram produzidos os pÃs de acerola e mamÃo em condiÃÃes Ãtimas, baseadas na menor higroscopicidade. A umidade nÃo foi considerada pelo planejamento, pois os pÃs encontravam-se dentro do especificado pela legislaÃÃo brasileira. A partir das caracterizaÃÃes fÃsico-quÃmicas das polpas in natura e das polpas em pà percebeu-se boa qualidade nutricional para ambas as polpas principalmente pelo teor de Ãcido ascÃrbico, alÃm de considerÃveis teores de antocianinas e carotenÃides, em relaÃÃo Ãs isotermas de adsorÃÃo, ambos os pÃs apresentaram curvas do tipo III, cÃncavas em formato de âJâ, tipicamente associado a pÃs a base de frutos, contudo a polpa de mamÃo em pà apresentou inversÃo do efeito da temperatura sobre a capacidade de adsorÃÃo da Ãgua em uma faixa de atividade de Ãgua de 0,75. O modelo de Oswin foi o que melhor se ajustou na prediÃÃo das curvas para polpa de acerola em pà nas temperaturas analisadas. Para a polpa de mamÃo, o modelo proposto por BET foi o que melhor se ajustou aos dados. Em seguida realizou-se delineamento experimental de misturas simplex centrÃide aumentado para 3 componentes (polpa de acerola; polpa de mamÃo e maltodextrina) para obter-se âblendâ em pà liofilizado, atravÃs da determinaÃÃo do efeito das proporÃÃes da mistura sobre a higroscopicidade, solubilidade, tempo de reidrataÃÃo e grau de Caking. O tempo de liofilizaÃÃo dos âblendsâ foi à mÃdia aritmÃtica simples entre os tempos de liofilizaÃÃo obtidos pelo planejamento composto central para as polpas em pà de acerola e mamÃo. Os resultados da anÃlise qualitativa da mistura possibilitou a escolha do ensaio 6 com as proporÃÃes 25% de polpa de acerola, 50% de polpa de mamÃo e 25% de maltodextrina como melhor ensaio para produÃÃo do âblendâ em pÃ. O âblendâ em pà nas condiÃÃes Ãtimas apresentou boas caracterÃsticas fÃsico-quÃmicas, em relaÃÃo Ãs isotermas de sorÃÃo, o modelo de GAB foi o que melhor se ajustou aos dados experimentais, onde as curvas foram do tipo III. Em seguida, realizou-se o estudo da estabilidade do âblendâ em pÃ, pelo perÃodo de 20 dias acondicionados em embalagem de polietileno envolvidos em folha de alumÃnio. Com isso, concluiu-se que, apÃs este perÃodo de armazenamento, o âblendâ em pÃ, ainda apresentava-se na forma de pà e com boas caracterÃsticas fÃsico-quÃmicas e higroscÃpicas.CoordenaÃÃo de AperfeiÃoamento de Pessoal de NÃvel Superiorhttp://www.teses.ufc.br/tde_busca/arquivo.php?codArquivo=10025application/pdfinfo:eu-repo/semantics/openAccessporreponame:Biblioteca Digital de Teses e Dissertações da UFCinstname:Universidade Federal do Cearáinstacron:UFC2019-01-21T11:23:13Zmail@mail.com -
dc.title.en.fl_str_mv Development of powder mixtures of pulp and acerola papaya.
dc.title.alternative.pt.fl_str_mv ElaboraÃÃo de misturas em pà das polpas de acerola e mamÃo
title Development of powder mixtures of pulp and acerola papaya.
spellingShingle Development of powder mixtures of pulp and acerola papaya.
Silas Rafael Figueiredo de AraÃjo
Isotermas
higroscopicidade
blend
Isotermas
higroscopicidade
blend
Isotherms
hygroscopicity
blend
CIENCIA E TECNOLOGIA DE ALIMENTOS
title_short Development of powder mixtures of pulp and acerola papaya.
title_full Development of powder mixtures of pulp and acerola papaya.
title_fullStr Development of powder mixtures of pulp and acerola papaya.
title_full_unstemmed Development of powder mixtures of pulp and acerola papaya.
title_sort Development of powder mixtures of pulp and acerola papaya.
author Silas Rafael Figueiredo de AraÃjo
author_facet Silas Rafael Figueiredo de AraÃjo
author_role author
dc.contributor.advisor1.fl_str_mv Marcos Rodrigues Amorim Afonso
dc.contributor.advisor1ID.fl_str_mv 15232275836
dc.contributor.advisor1Lattes.fl_str_mv http://buscatextual.cnpq.br/buscatextual/visualizacv.jsp?id=K4701595T6&dataRevisao=null
dc.contributor.referee1.fl_str_mv Sueli Rodrigues
dc.contributor.referee1ID.fl_str_mv 19633877830
dc.contributor.referee1Lattes.fl_str_mv http://buscatextual.cnpq.br/buscatextual/visualizacv.jsp?id=K4707745Z6
dc.contributor.referee2.fl_str_mv LuciclÃia Barros de Vasconcelos Torres
dc.contributor.referee2ID.fl_str_mv 02749067405
dc.contributor.referee2Lattes.fl_str_mv http://buscatextual.cnpq.br/buscatextual/visualizacv.do?id=K4778490E6
dc.contributor.authorID.fl_str_mv 00322529271
dc.contributor.authorLattes.fl_str_mv http://buscatextual.cnpq.br/buscatextual/visualizacv.do?id=K4208608Y1
dc.contributor.author.fl_str_mv Silas Rafael Figueiredo de AraÃjo
contributor_str_mv Marcos Rodrigues Amorim Afonso
Sueli Rodrigues
LuciclÃia Barros de Vasconcelos Torres
dc.subject.por.fl_str_mv Isotermas
higroscopicidade
blend
Isotermas
higroscopicidade
blend
topic Isotermas
higroscopicidade
blend
Isotermas
higroscopicidade
blend
Isotherms
hygroscopicity
blend
CIENCIA E TECNOLOGIA DE ALIMENTOS
dc.subject.eng.fl_str_mv Isotherms
hygroscopicity
blend
dc.subject.cnpq.fl_str_mv CIENCIA E TECNOLOGIA DE ALIMENTOS
dc.description.sponsorship.fl_txt_mv CoordenaÃÃo de AperfeiÃoamento de Pessoal de NÃvel Superior
dc.description.abstract.por.fl_txt_mv The acerola tropical fruit and papaya are of great industrial interest for its nutritional and sensory characteristics. Due to the perishable nature of these fruits to adopt conservation methods is necessary. The present study aimed at obtaining "blends" powder from freeze-drying the pulp of acerola and papaya. First were performed compounds central rotational schedules, which evaluated the influence of lyophilization time and maltodextrin concentration and humidity on the hygroscopicity of the powders. From the results of the design were produced powders from acerola and papaya in optimal process conditions based on lower hygroscopicity, moisture was not considered by the planning because the powders obtained were within the standards established by Brazilian legislation. From the physico-chemical characterizations of the pulps and the pulps fresh powder was noticed good nutritional quality for both pulps primarily by ascorbic acid, in addition to considerable amounts of anthocyanins and carotenoids in relation to adsorption isotherms both the powders exhibited type III curves concave-shaped "J" typically associated with the food powders from fruit, yet papaya pulp powder showed reversal of the effect of temperature on adsorption capacity for water a range of water activity of 0,8. The Oswin model was the best fit curves for the prediction of the pulp powder at all temperatures analyzed for papaya pulp, the model proposed by BET was the best fit the data. Then experiment was conducted mixtures simplex centroid increased to three components (acerola pulp, papaya pulp and maltodextrin) to obtain the "blend" lyophilized powder, by determining the effect of the proportions of the mixture on the hygroscopicity , solubility, time and degree of rehydration Caking. The time lyophilization of "blends" was the simple arithmetic average between the times of lyophilization obtained by central composite design for the pulp powder acerola and papaya. The results of qualitative analysis of the mixture enabled the choice of test 6 with the proportions 25% acerola pulp, 50% papaya pulp and 25% maltodextrin as best assay for production of "blend" powder. The "blend" powder obtained under optimum conditions showed good physicochemical characteristics, in relation to sorption isotherms, the GAB model was the best fit the experimental data, where the curves were type III. Then there was the study of the stability of the "blend" powder in storage period of 20 days packed in polyethylene wrapped in aluminum foil. Thus, it was concluded that, after this storage period, the "blend" powder, the patient was still in powder form and has good chemical-physical characteristics and hygroscopic.
A acerola e mamÃo sÃo frutos tropicais de grande interesse industrial por suas caracterÃsticas nutricionais e sensoriais. Em virtude do carÃter perecÃvel desses frutos a adoÃÃo de mÃtodos de conservaÃÃo faz-se necessÃria. O presente trabalho teve como objetivo obter âblendsâ em pà a partir da liofilizaÃÃo das polpas de acerola e mamÃo. Primeiramente foram realizados planejamentos compostos central rotacionais, onde se avaliou a influÃncia do tempo de liofilizaÃÃo e concentraÃÃo de maltodextrina sobre a higroscopicidade e umidade dos pÃs obtidos. A partir dos resultados do planejamento foram produzidos os pÃs de acerola e mamÃo em condiÃÃes Ãtimas, baseadas na menor higroscopicidade. A umidade nÃo foi considerada pelo planejamento, pois os pÃs encontravam-se dentro do especificado pela legislaÃÃo brasileira. A partir das caracterizaÃÃes fÃsico-quÃmicas das polpas in natura e das polpas em pà percebeu-se boa qualidade nutricional para ambas as polpas principalmente pelo teor de Ãcido ascÃrbico, alÃm de considerÃveis teores de antocianinas e carotenÃides, em relaÃÃo Ãs isotermas de adsorÃÃo, ambos os pÃs apresentaram curvas do tipo III, cÃncavas em formato de âJâ, tipicamente associado a pÃs a base de frutos, contudo a polpa de mamÃo em pà apresentou inversÃo do efeito da temperatura sobre a capacidade de adsorÃÃo da Ãgua em uma faixa de atividade de Ãgua de 0,75. O modelo de Oswin foi o que melhor se ajustou na prediÃÃo das curvas para polpa de acerola em pà nas temperaturas analisadas. Para a polpa de mamÃo, o modelo proposto por BET foi o que melhor se ajustou aos dados. Em seguida realizou-se delineamento experimental de misturas simplex centrÃide aumentado para 3 componentes (polpa de acerola; polpa de mamÃo e maltodextrina) para obter-se âblendâ em pà liofilizado, atravÃs da determinaÃÃo do efeito das proporÃÃes da mistura sobre a higroscopicidade, solubilidade, tempo de reidrataÃÃo e grau de Caking. O tempo de liofilizaÃÃo dos âblendsâ foi à mÃdia aritmÃtica simples entre os tempos de liofilizaÃÃo obtidos pelo planejamento composto central para as polpas em pà de acerola e mamÃo. Os resultados da anÃlise qualitativa da mistura possibilitou a escolha do ensaio 6 com as proporÃÃes 25% de polpa de acerola, 50% de polpa de mamÃo e 25% de maltodextrina como melhor ensaio para produÃÃo do âblendâ em pÃ. O âblendâ em pà nas condiÃÃes Ãtimas apresentou boas caracterÃsticas fÃsico-quÃmicas, em relaÃÃo Ãs isotermas de sorÃÃo, o modelo de GAB foi o que melhor se ajustou aos dados experimentais, onde as curvas foram do tipo III. Em seguida, realizou-se o estudo da estabilidade do âblendâ em pÃ, pelo perÃodo de 20 dias acondicionados em embalagem de polietileno envolvidos em folha de alumÃnio. Com isso, concluiu-se que, apÃs este perÃodo de armazenamento, o âblendâ em pÃ, ainda apresentava-se na forma de pà e com boas caracterÃsticas fÃsico-quÃmicas e higroscÃpicas.
description The acerola tropical fruit and papaya are of great industrial interest for its nutritional and sensory characteristics. Due to the perishable nature of these fruits to adopt conservation methods is necessary. The present study aimed at obtaining "blends" powder from freeze-drying the pulp of acerola and papaya. First were performed compounds central rotational schedules, which evaluated the influence of lyophilization time and maltodextrin concentration and humidity on the hygroscopicity of the powders. From the results of the design were produced powders from acerola and papaya in optimal process conditions based on lower hygroscopicity, moisture was not considered by the planning because the powders obtained were within the standards established by Brazilian legislation. From the physico-chemical characterizations of the pulps and the pulps fresh powder was noticed good nutritional quality for both pulps primarily by ascorbic acid, in addition to considerable amounts of anthocyanins and carotenoids in relation to adsorption isotherms both the powders exhibited type III curves concave-shaped "J" typically associated with the food powders from fruit, yet papaya pulp powder showed reversal of the effect of temperature on adsorption capacity for water a range of water activity of 0,8. The Oswin model was the best fit curves for the prediction of the pulp powder at all temperatures analyzed for papaya pulp, the model proposed by BET was the best fit the data. Then experiment was conducted mixtures simplex centroid increased to three components (acerola pulp, papaya pulp and maltodextrin) to obtain the "blend" lyophilized powder, by determining the effect of the proportions of the mixture on the hygroscopicity , solubility, time and degree of rehydration Caking. The time lyophilization of "blends" was the simple arithmetic average between the times of lyophilization obtained by central composite design for the pulp powder acerola and papaya. The results of qualitative analysis of the mixture enabled the choice of test 6 with the proportions 25% acerola pulp, 50% papaya pulp and 25% maltodextrin as best assay for production of "blend" powder. The "blend" powder obtained under optimum conditions showed good physicochemical characteristics, in relation to sorption isotherms, the GAB model was the best fit the experimental data, where the curves were type III. Then there was the study of the stability of the "blend" powder in storage period of 20 days packed in polyethylene wrapped in aluminum foil. Thus, it was concluded that, after this storage period, the "blend" powder, the patient was still in powder form and has good chemical-physical characteristics and hygroscopic.
publishDate 2013
dc.date.issued.fl_str_mv 2013-04-15
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/masterThesis
status_str publishedVersion
format masterThesis
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url http://www.teses.ufc.br/tde_busca/arquivo.php?codArquivo=10025
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dc.publisher.none.fl_str_mv Universidade Federal do CearÃ
dc.publisher.program.fl_str_mv Programa de PÃs-GraduaÃÃo em CiÃncia e Tecnologia de Alimentos
dc.publisher.initials.fl_str_mv UFC
dc.publisher.country.fl_str_mv BR
publisher.none.fl_str_mv Universidade Federal do CearÃ
dc.source.none.fl_str_mv reponame:Biblioteca Digital de Teses e Dissertações da UFC
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