Obtenção e caracterização de extrato microencapsulado de resíduo agroindustrial de acerola

Detalhes bibliográficos
Autor(a) principal: Moreira, Germano éder Gadelha
Data de Publicação: 2008
Tipo de documento: Dissertação
Idioma: por
Título da fonte: Repositório Institucional da UFRN
Texto Completo: https://repositorio.ufrn.br/jspui/handle/123456789/15742
Resumo: Acerola (Malpighia emarginata D.C.) is a red fruit widely cultivated in Brazil, especially in the Northeastern region. Its increasing demand is attributed to its high ascorbic acid contents. Besides ascorbic acid, widely known by its health-benefit effects, acerola is rich in anthocyanins, which contribute for the antioxidant power of the fruit. Acerola processing produces a bright-red pomace, usually discarded. The further processing of this pomace, in order to explore its antioxidant compounds, could enhance acerola market value and rentability of its processing. Both ascorbic acid and anthocyanins are highly susceptible to degradation, that can be delayed by microencapsulation, which consists on packing particles (core) in an edible matrix (wall material). This work has been made with the purpose of producing a microencapsulated acerola pomace extract, which could be used by the food industry as a functional ingredient with antioxidant and coloring properties. Antioxidant compounds were recovered by pressing the pomace diluted in a solvent (a citric acid aqueous solution), by using a central composite design, with two variables: citric acid concentration in the solvent (0-2%), and solvent: pomace mass ratio (2:1-6:1). The acerola pomace extract was then microencapsulated by spray drying. A central composite design was adopted, with three variables: inlet temperature of the spray dryer (170o-200oC), wall material: acerola solids mass ratio (2:1-5:1), and degree of maltodextrin replacement by cashew tree gum as wall material (0-100%). The cashew tree gum was used because of its similarity to arabic gum, which is regarded as the wall material by excellence. The following conditions were considered as optimal for extraction of anthocyanins and ascorbic acid: solvent/pomace ratio, 5:1, and no citric acid in the solvent. 82.47% of the anthocyanins were recovered, as well as 83.22% of the ascorbic acid. Anthocyanin and ascorbic acid retentions were favored by lower inlet temperatures, higher wall material: acerola solids mass ratio and higher maltodextrin replacement by cashew tree gum, which was presented as a promising wall material. The more adequate microencapsulation conditions, based not only on retention of antioxidant compounds but also on physical properties of the final powder, were the following: inlet temperature, 185oC; wall material: acerola solids mass ratio, 5:1, and minimum degree of maltodextrin replacement by cashew tree gum, 50%
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spelling Moreira, Germano éder Gadelhahttp://lattes.cnpq.br/9183668439545650http://buscatextual.cnpq.br/buscatextual/visualizacv.do?id=K4788622A0Azeredo, Henriette Monteiro Cordeiro dehttp://lattes.cnpq.br/8516223928904348Passos, Maria Laura de AzevedoPASSOS, Maria Laura de AzevedoPereira, Camila Gambinihttp://lattes.cnpq.br/8055289812908100Medeiros, Maria de Fátima Dantas de2014-12-17T15:01:13Z2014-12-122014-12-17T15:01:13Z2008-03-31MOREIRA, Germano éder Gadelha. Obtenção e caracterização de extrato microencapsulado de resíduo agroindustrial de acerola. 2008. 86 f. Dissertação (Mestrado em Pesquisa e Desenvolvimento de Tecnologias Regionais) - Universidade Federal do Rio Grande do Norte, Natal, 2008.https://repositorio.ufrn.br/jspui/handle/123456789/15742Acerola (Malpighia emarginata D.C.) is a red fruit widely cultivated in Brazil, especially in the Northeastern region. Its increasing demand is attributed to its high ascorbic acid contents. Besides ascorbic acid, widely known by its health-benefit effects, acerola is rich in anthocyanins, which contribute for the antioxidant power of the fruit. Acerola processing produces a bright-red pomace, usually discarded. The further processing of this pomace, in order to explore its antioxidant compounds, could enhance acerola market value and rentability of its processing. Both ascorbic acid and anthocyanins are highly susceptible to degradation, that can be delayed by microencapsulation, which consists on packing particles (core) in an edible matrix (wall material). This work has been made with the purpose of producing a microencapsulated acerola pomace extract, which could be used by the food industry as a functional ingredient with antioxidant and coloring properties. Antioxidant compounds were recovered by pressing the pomace diluted in a solvent (a citric acid aqueous solution), by using a central composite design, with two variables: citric acid concentration in the solvent (0-2%), and solvent: pomace mass ratio (2:1-6:1). The acerola pomace extract was then microencapsulated by spray drying. A central composite design was adopted, with three variables: inlet temperature of the spray dryer (170o-200oC), wall material: acerola solids mass ratio (2:1-5:1), and degree of maltodextrin replacement by cashew tree gum as wall material (0-100%). The cashew tree gum was used because of its similarity to arabic gum, which is regarded as the wall material by excellence. The following conditions were considered as optimal for extraction of anthocyanins and ascorbic acid: solvent/pomace ratio, 5:1, and no citric acid in the solvent. 82.47% of the anthocyanins were recovered, as well as 83.22% of the ascorbic acid. Anthocyanin and ascorbic acid retentions were favored by lower inlet temperatures, higher wall material: acerola solids mass ratio and higher maltodextrin replacement by cashew tree gum, which was presented as a promising wall material. The more adequate microencapsulation conditions, based not only on retention of antioxidant compounds but also on physical properties of the final powder, were the following: inlet temperature, 185oC; wall material: acerola solids mass ratio, 5:1, and minimum degree of maltodextrin replacement by cashew tree gum, 50%A acerola (Malpighia emarginata D.C.) é um fruto avermelhado bastante cultivado no Brasil, principalmente no Nordeste. A demanda por esse fruto tem crescido muito, principalmente devido ao seu alto teor de ácido ascórbico. Além do ácido ascórbico, amplamente conhecido por seus efeitos benéficos à saúde, a acerola é rica em antocianinas, que contribuem para o poder antioxidante da fruta. O processamento de acerola produz um resíduo (bagaço) vermelho intenso, geralmente descartado. O processamento desse bagaço para aproveitamento dos compostos de interesse poderia aumentar o valor comercial da acerola e a rentabilidade de seu processamento. Tanto o ácido ascórbico quanto as antocianinas são altamente suscetíveis à degradação, que pode ser reduzida pela aplicação de um processo de microencapsulação, que consiste no empacotamento de partículas (núcleo) em uma matriz comestível (encapsulante). Este trabalho foi feito com o objetivo de produzir um extrato microencapsulado a partir de bagaço de acerola, com possibilidades de ser usado pela indústria de alimentos como ingrediente funcional com propriedades antioxidantes e/ou corantes. Os compostos de interesse foram recuperados por prensagem do bagaço diluído em um solvente (solução aquosa de ácido cítrico), utilizando-se um delineamento composto central com duas variáveis: concentração de ácido cítrico no solvente (0-2%), e proporção solvente: bagaço (2:1-6:1). O extrato de bagaço de acerola foi então submetido a microencapsulação por atomização. Foi adotado um delineamento composto central, com três variáveis: temperatura de entrada do atomizador (170o-200oC), proporção mássica encapsulante: sólidos de acerola (2:1-5:1), e percentual de substituição de maltodextrina por goma de cajueiro como material encapsulante (0-100%). A goma de cajueiro foi utilizada por ser um material de composição similar à goma arábica, que é considerada o agente encapsulante por excelência. As condições consideradas ótimas para a extração foram: proporção solvente: bagaço, 5:1, e ausência de ácido cítrico no solvente, que resultaram em 82,47% de recuperação de antocianinas e 83,22% de recuperação de ácido ascórbico. A retenção dos compostos de interesse durante a atomização foi favorecida por menores valores de temperatura de entrada, maiores proporções encapsulante/sólidos de acerola e maior grau de substituição de maltodextrina por goma de cajueiro. A goma de cajueiro mostrou-se bastante promissora como material encapsulante. As condições mais adequadas de microencapsulação por atomização, baseadas não apenas na retenção dos compostos de interesse, mas também nas propriedades físicas dos pós obtidos (solubilidade, higroscopicidade e fluidez) foram as seguintes: temperatura de entrada, 185oC; proporção encapsulante/sólidos de acerola, 5:1, tendo o material encapsulante pelo menos 50% de goma de cajueiroCoordenação de Aperfeiçoamento de Pessoal de Nível Superiorapplication/pdfporUniversidade Federal do Rio Grande do NortePrograma de Pós-Graduação em Engenharia QuímicaUFRNBRPesquisa e Desenvolvimento de Tecnologias RegionaisAntocianinasÁcido ascórbicoAntioxidantesGoma de cajueiro.AnthocyaninsAscorbic acidAntioxidantsCashew tree gumCNPQ::ENGENHARIAS::ENGENHARIA QUIMICAObtenção e caracterização de extrato microencapsulado de resíduo agroindustrial de acerolainfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/masterThesisinfo:eu-repo/semantics/openAccessreponame:Repositório Institucional da UFRNinstname:Universidade Federal do Rio Grande do Norte (UFRN)instacron:UFRNORIGINALGermanoEGM.pdfapplication/pdf926195https://repositorio.ufrn.br/bitstream/123456789/15742/1/GermanoEGM.pdf568b715287468c63c1f4f41fd8c65496MD51TEXTGermanoEGM.pdf.txtGermanoEGM.pdf.txtExtracted texttext/plain148258https://repositorio.ufrn.br/bitstream/123456789/15742/6/GermanoEGM.pdf.txt1c630868cbf56e64ede763e9e958f3a9MD56THUMBNAILGermanoEGM.pdf.jpgGermanoEGM.pdf.jpgIM Thumbnailimage/jpeg3541https://repositorio.ufrn.br/bitstream/123456789/15742/7/GermanoEGM.pdf.jpged4582d634bff40a395b2f96652e8026MD57123456789/157422017-11-02 02:50:13.084oai:https://repositorio.ufrn.br:123456789/15742Repositório de PublicaçõesPUBhttp://repositorio.ufrn.br/oai/opendoar:2017-11-02T05:50:13Repositório Institucional da UFRN - Universidade Federal do Rio Grande do Norte (UFRN)false
dc.title.por.fl_str_mv Obtenção e caracterização de extrato microencapsulado de resíduo agroindustrial de acerola
title Obtenção e caracterização de extrato microencapsulado de resíduo agroindustrial de acerola
spellingShingle Obtenção e caracterização de extrato microencapsulado de resíduo agroindustrial de acerola
Moreira, Germano éder Gadelha
Antocianinas
Ácido ascórbico
Antioxidantes
Goma de cajueiro.
Anthocyanins
Ascorbic acid
Antioxidants
Cashew tree gum
CNPQ::ENGENHARIAS::ENGENHARIA QUIMICA
title_short Obtenção e caracterização de extrato microencapsulado de resíduo agroindustrial de acerola
title_full Obtenção e caracterização de extrato microencapsulado de resíduo agroindustrial de acerola
title_fullStr Obtenção e caracterização de extrato microencapsulado de resíduo agroindustrial de acerola
title_full_unstemmed Obtenção e caracterização de extrato microencapsulado de resíduo agroindustrial de acerola
title_sort Obtenção e caracterização de extrato microencapsulado de resíduo agroindustrial de acerola
author Moreira, Germano éder Gadelha
author_facet Moreira, Germano éder Gadelha
author_role author
dc.contributor.authorID.por.fl_str_mv
dc.contributor.authorLattes.por.fl_str_mv http://lattes.cnpq.br/9183668439545650
dc.contributor.advisorID.por.fl_str_mv
dc.contributor.advisorLattes.por.fl_str_mv http://buscatextual.cnpq.br/buscatextual/visualizacv.do?id=K4788622A0
dc.contributor.advisor-co1ID.por.fl_str_mv
dc.contributor.referees1.pt_BR.fl_str_mv Passos, Maria Laura de Azevedo
dc.contributor.referees1ID.por.fl_str_mv
dc.contributor.referees1Lattes.por.fl_str_mv PASSOS, Maria Laura de Azevedo
dc.contributor.referees2.pt_BR.fl_str_mv Pereira, Camila Gambini
dc.contributor.referees2ID.por.fl_str_mv
dc.contributor.referees2Lattes.por.fl_str_mv http://lattes.cnpq.br/8055289812908100
dc.contributor.author.fl_str_mv Moreira, Germano éder Gadelha
dc.contributor.advisor-co1.fl_str_mv Azeredo, Henriette Monteiro Cordeiro de
dc.contributor.advisor-co1Lattes.fl_str_mv http://lattes.cnpq.br/8516223928904348
dc.contributor.advisor1.fl_str_mv Medeiros, Maria de Fátima Dantas de
contributor_str_mv Azeredo, Henriette Monteiro Cordeiro de
Medeiros, Maria de Fátima Dantas de
dc.subject.por.fl_str_mv Antocianinas
Ácido ascórbico
Antioxidantes
Goma de cajueiro.
topic Antocianinas
Ácido ascórbico
Antioxidantes
Goma de cajueiro.
Anthocyanins
Ascorbic acid
Antioxidants
Cashew tree gum
CNPQ::ENGENHARIAS::ENGENHARIA QUIMICA
dc.subject.eng.fl_str_mv Anthocyanins
Ascorbic acid
Antioxidants
Cashew tree gum
dc.subject.cnpq.fl_str_mv CNPQ::ENGENHARIAS::ENGENHARIA QUIMICA
description Acerola (Malpighia emarginata D.C.) is a red fruit widely cultivated in Brazil, especially in the Northeastern region. Its increasing demand is attributed to its high ascorbic acid contents. Besides ascorbic acid, widely known by its health-benefit effects, acerola is rich in anthocyanins, which contribute for the antioxidant power of the fruit. Acerola processing produces a bright-red pomace, usually discarded. The further processing of this pomace, in order to explore its antioxidant compounds, could enhance acerola market value and rentability of its processing. Both ascorbic acid and anthocyanins are highly susceptible to degradation, that can be delayed by microencapsulation, which consists on packing particles (core) in an edible matrix (wall material). This work has been made with the purpose of producing a microencapsulated acerola pomace extract, which could be used by the food industry as a functional ingredient with antioxidant and coloring properties. Antioxidant compounds were recovered by pressing the pomace diluted in a solvent (a citric acid aqueous solution), by using a central composite design, with two variables: citric acid concentration in the solvent (0-2%), and solvent: pomace mass ratio (2:1-6:1). The acerola pomace extract was then microencapsulated by spray drying. A central composite design was adopted, with three variables: inlet temperature of the spray dryer (170o-200oC), wall material: acerola solids mass ratio (2:1-5:1), and degree of maltodextrin replacement by cashew tree gum as wall material (0-100%). The cashew tree gum was used because of its similarity to arabic gum, which is regarded as the wall material by excellence. The following conditions were considered as optimal for extraction of anthocyanins and ascorbic acid: solvent/pomace ratio, 5:1, and no citric acid in the solvent. 82.47% of the anthocyanins were recovered, as well as 83.22% of the ascorbic acid. Anthocyanin and ascorbic acid retentions were favored by lower inlet temperatures, higher wall material: acerola solids mass ratio and higher maltodextrin replacement by cashew tree gum, which was presented as a promising wall material. The more adequate microencapsulation conditions, based not only on retention of antioxidant compounds but also on physical properties of the final powder, were the following: inlet temperature, 185oC; wall material: acerola solids mass ratio, 5:1, and minimum degree of maltodextrin replacement by cashew tree gum, 50%
publishDate 2008
dc.date.issued.fl_str_mv 2008-03-31
dc.date.accessioned.fl_str_mv 2014-12-17T15:01:13Z
dc.date.available.fl_str_mv 2014-12-12
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dc.identifier.citation.fl_str_mv MOREIRA, Germano éder Gadelha. Obtenção e caracterização de extrato microencapsulado de resíduo agroindustrial de acerola. 2008. 86 f. Dissertação (Mestrado em Pesquisa e Desenvolvimento de Tecnologias Regionais) - Universidade Federal do Rio Grande do Norte, Natal, 2008.
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identifier_str_mv MOREIRA, Germano éder Gadelha. Obtenção e caracterização de extrato microencapsulado de resíduo agroindustrial de acerola. 2008. 86 f. Dissertação (Mestrado em Pesquisa e Desenvolvimento de Tecnologias Regionais) - Universidade Federal do Rio Grande do Norte, Natal, 2008.
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