Formation of Composite Polyaniline and Graphene Oxide by Physical Mixture Method
Autor(a) principal: | |
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Data de Publicação: | 2017 |
Outros Autores: | , , , , |
Tipo de documento: | Artigo |
Idioma: | eng |
Título da fonte: | Repositório Institucional da UNIFESP |
Texto Completo: | https://repositorio.unifesp.br/handle/11600/56394 http://dx.doi.org/10.5028/jatm.v9i1.697 |
Resumo: | The development of polyaniline and graphene oxide composites aims to join the unique properties of each material for aerospace applications. The present paper demonstrates an easy and quick method, compared to the ones found in the literature, to obtain a composite made with polyaniline doped with dodecylbenzenesulfonic acid, a combination commonly called polyaniline, and graphene oxide. Nowadays, the most common studied methods are electrochemistry and in situ chemical polymerization. Differently from these methods, the films were obtained by a physical mixture of equimolar suspension of graphene oxide (4 mg/mL) with 3 concentrations of polyaniline powder: 25 |
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Vargas, Ludmila ResendePoli, Anne KarolineLazzarini Dutra, Rita de CassiaSouza, Camila Brito de [UNIFESP]Baldan, Mauricio RibeiroGoncalves, Emerson Sarmento2020-07-31T12:46:50Z2020-07-31T12:46:50Z2017Journal Of Aerospace Technology And Management. Sao Paulo, v. 9, n. 1, p. 29-38, 2017.1984-9648https://repositorio.unifesp.br/handle/11600/56394http://dx.doi.org/10.5028/jatm.v9i1.697WOS000395632200003.pdf10.5028/jatm.v9i1.697WOS:000395632200003The development of polyaniline and graphene oxide composites aims to join the unique properties of each material for aerospace applications. The present paper demonstrates an easy and quick method, compared to the ones found in the literature, to obtain a composite made with polyaniline doped with dodecylbenzenesulfonic acid, a combination commonly called polyaniline, and graphene oxide. Nowadays, the most common studied methods are electrochemistry and in situ chemical polymerization. Differently from these methods, the films were obtained by a physical mixture of equimolar suspension of graphene oxide (4 mg/mL) with 3 concentrations of polyaniline powder: 2550 and 75%, being compared to pure graphene oxide and polyaniline. The morphology and structure behavior of all the films were studied, besides the bonding nature between both materials. The films were analyzed by scanning electron microscopy, X-ray diffraction, Fourier transform infrared spectroscopy, and differential scanning calorimetry. The apparent interaction between graphene oxide corrugated sheets and polyaniline grains was verified by scanning electron microscopy images. It can be noticed, as the concentration of polyaniline increases, that more polymer was entrapped. To prove the formation of polyaniline/graphene oxide composite, X-ray diffraction and Fourier transform infrared spectroscopy techniques demonstrated the changes on graphene oxide crystallographic plans and on the chemical bonding between polyaniline and graphene oxide, suggesting an interaction between polyaniline and graphene oxide, especially in the composite with 50% polyaniline/50% graphene oxide. Differential scanning calorimetry was used to highlight this effect through the increase in thermal stability. The method of physical mixture was efficient to obtain the polyaniline/graphene oxide composites.Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)Instituto Tecnológico de AeronáuticaDivisão de Química of the Instituto de Aeronáutica e EspaçoInst Tecnol Aeronaut, Dept Ciencia & Tecnol Aeroespacial, Sao Jose Dos Campos, BrazilInst Aeronaut Espaco, Dept Ciencia Tecnol Aeroespacial, Div Mat, Sao Jose Dos Campos, BrazilUniv Fed Sao Paulo, Inst Ciencia Tecnol, Campus Parque Tecnol, Sao Jose Dos Campos, BrazilInst Nacl Pesquisas Espaciais, Lab Associado Sensores, Sao Jose Dos Campos, BrazilInst Aeronaut Espaco, Dept Ciencia Tecnol Aeroespacial, Div Mat, 50 Vila Acacias, Sao Jose Dos Campos, BrazilUniversidade Federal de São Paulo – Instituto de Ciência e Tecnologia – Campus Parque Tecnológico – São José dos Campos/SP – BrazilWeb of Science29-38engInst Aeronautica & Espaco-IaeJournal Of Aerospace Technology And ManagementGraphene oxidePolyanilineStructureMorphologyFT-IRDSCFormation of Composite Polyaniline and Graphene Oxide by Physical Mixture Methodinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/articleSao Paulo91info:eu-repo/semantics/openAccessreponame:Repositório Institucional da UNIFESPinstname:Universidade Federal de São Paulo (UNIFESP)instacron:UNIFESPORIGINALWOS000395632200003.pdfapplication/pdf2247809${dspace.ui.url}/bitstream/11600/56394/1/WOS000395632200003.pdf0812dbbe9a57e18f23fa9c382dc8d1fcMD51open accessTEXTWOS000395632200003.pdf.txtWOS000395632200003.pdf.txtExtracted texttext/plain37072${dspace.ui.url}/bitstream/11600/56394/8/WOS000395632200003.pdf.txtd79e11747a3c6e437a285bfb406087e1MD58open accessTHUMBNAILWOS000395632200003.pdf.jpgWOS000395632200003.pdf.jpgIM Thumbnailimage/jpeg6981${dspace.ui.url}/bitstream/11600/56394/10/WOS000395632200003.pdf.jpgad8801cf4ec70ed976caa49682d02216MD510open access11600/563942023-06-05 19:05:52.461open accessoai:repositorio.unifesp.br:11600/56394Repositório InstitucionalPUBhttp://www.repositorio.unifesp.br/oai/requestopendoar:34652023-06-05T22:05:52Repositório Institucional da UNIFESP - Universidade Federal de São Paulo (UNIFESP)false |
dc.title.en.fl_str_mv |
Formation of Composite Polyaniline and Graphene Oxide by Physical Mixture Method |
title |
Formation of Composite Polyaniline and Graphene Oxide by Physical Mixture Method |
spellingShingle |
Formation of Composite Polyaniline and Graphene Oxide by Physical Mixture Method Vargas, Ludmila Resende Graphene oxide Polyaniline Structure Morphology FT-IR DSC |
title_short |
Formation of Composite Polyaniline and Graphene Oxide by Physical Mixture Method |
title_full |
Formation of Composite Polyaniline and Graphene Oxide by Physical Mixture Method |
title_fullStr |
Formation of Composite Polyaniline and Graphene Oxide by Physical Mixture Method |
title_full_unstemmed |
Formation of Composite Polyaniline and Graphene Oxide by Physical Mixture Method |
title_sort |
Formation of Composite Polyaniline and Graphene Oxide by Physical Mixture Method |
author |
Vargas, Ludmila Resende |
author_facet |
Vargas, Ludmila Resende Poli, Anne Karoline Lazzarini Dutra, Rita de Cassia Souza, Camila Brito de [UNIFESP] Baldan, Mauricio Ribeiro Goncalves, Emerson Sarmento |
author_role |
author |
author2 |
Poli, Anne Karoline Lazzarini Dutra, Rita de Cassia Souza, Camila Brito de [UNIFESP] Baldan, Mauricio Ribeiro Goncalves, Emerson Sarmento |
author2_role |
author author author author author |
dc.contributor.author.fl_str_mv |
Vargas, Ludmila Resende Poli, Anne Karoline Lazzarini Dutra, Rita de Cassia Souza, Camila Brito de [UNIFESP] Baldan, Mauricio Ribeiro Goncalves, Emerson Sarmento |
dc.subject.eng.fl_str_mv |
Graphene oxide Polyaniline Structure Morphology FT-IR DSC |
topic |
Graphene oxide Polyaniline Structure Morphology FT-IR DSC |
description |
The development of polyaniline and graphene oxide composites aims to join the unique properties of each material for aerospace applications. The present paper demonstrates an easy and quick method, compared to the ones found in the literature, to obtain a composite made with polyaniline doped with dodecylbenzenesulfonic acid, a combination commonly called polyaniline, and graphene oxide. Nowadays, the most common studied methods are electrochemistry and in situ chemical polymerization. Differently from these methods, the films were obtained by a physical mixture of equimolar suspension of graphene oxide (4 mg/mL) with 3 concentrations of polyaniline powder: 25 |
publishDate |
2017 |
dc.date.issued.fl_str_mv |
2017 |
dc.date.accessioned.fl_str_mv |
2020-07-31T12:46:50Z |
dc.date.available.fl_str_mv |
2020-07-31T12:46:50Z |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article |
format |
article |
status_str |
publishedVersion |
dc.identifier.citation.fl_str_mv |
Journal Of Aerospace Technology And Management. Sao Paulo, v. 9, n. 1, p. 29-38, 2017. |
dc.identifier.uri.fl_str_mv |
https://repositorio.unifesp.br/handle/11600/56394 http://dx.doi.org/10.5028/jatm.v9i1.697 |
dc.identifier.issn.none.fl_str_mv |
1984-9648 |
dc.identifier.file.none.fl_str_mv |
WOS000395632200003.pdf |
dc.identifier.doi.none.fl_str_mv |
10.5028/jatm.v9i1.697 |
dc.identifier.wos.none.fl_str_mv |
WOS:000395632200003 |
identifier_str_mv |
Journal Of Aerospace Technology And Management. Sao Paulo, v. 9, n. 1, p. 29-38, 2017. 1984-9648 WOS000395632200003.pdf 10.5028/jatm.v9i1.697 WOS:000395632200003 |
url |
https://repositorio.unifesp.br/handle/11600/56394 http://dx.doi.org/10.5028/jatm.v9i1.697 |
dc.language.iso.fl_str_mv |
eng |
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eng |
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Journal Of Aerospace Technology And Management |
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info:eu-repo/semantics/openAccess |
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openAccess |
dc.format.none.fl_str_mv |
29-38 |
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Sao Paulo |
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Inst Aeronautica & Espaco-Iae |
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Inst Aeronautica & Espaco-Iae |
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