Abrasão-corrosão em aços inoxidáveis ferríticos

Detalhes bibliográficos
Autor(a) principal: Labiapari, Wilian da Silva
Data de Publicação: 2015
Tipo de documento: Tese
Idioma: por
Título da fonte: Repositório Institucional da UFU
Texto Completo: https://repositorio.ufu.br/handle/123456789/14772
https://doi.org/10.14393/ufu.te.2015.72
Resumo: The aim of this work was to study the behavior of ferritic stainless steels in abrasive-corrosive environment of 10%wt SiO2 + 1N H2SO4. It was developed an apparatus and a methodology to perform the tests. The equipment has a load cell to measure the normal and friction forces during the test, an original device due to the difficulty to use it without damaging in abrasivecorrosive environment. It was used samples of ferritic stainless 11Cr, 11CrTi, 16Cr, 16CrNb (Nb stabilized) and, for comparative purposes, the stainless steels 18Cr8Ni (austenitic), 17CrTiNb (ferritic) and the carbon steel A36. It was proceeded the mechanical characterization (hardness and tensile testing), chemical and metallographic test (grain size) of these samples. For 16Cr and 16CrNb steels the crystallographic texture was analyzed, by EBSD. It has been realized corrosion test at turbulent and aerated environment, abrasion and abrasion-corrosion test. So it was analyzed the polarization curves, the wear coefficient k and the samples, by SEM. It was clearly observed at the corrosion tests the increasing at corrosion resistance with the increasing of Cr content in the samples. Although the 18Cr8Ni was the hardest material, it had worse performance on the abrasion tests. In this abrasive system studied there was a wear resistance increased after prior cold deformation. For the abrasioncorrosion tests the 18Cr8Ni had the best performance, although it was the worse in abrasion test. The materials were ranked by the higher wear resistance due to the increasing Cr content that was associated to the corrosive influence on the total wear in this abrasive-corrosive environment. In abrasive-corrosive medium, the wear was lower when compared to the abrasive medium for all materials mainly due to the friction coefficient reduction. For the steels 16CrNb and 16Cr, it was observed a slight influence of crystallographic texture on the corrosion resistance in turbulent medium and abrasive wear. However, this distinction does not exist for the abrasion-corrosion tests. It was also noticed an influence of niobium carbides in reducing the wear coefficient, even in a soft matrix as 16CrNb steel.
id UFU_d80c7ea12c698b202f620a2682e64ab7
oai_identifier_str oai:repositorio.ufu.br:123456789/14772
network_acronym_str UFU
network_name_str Repositório Institucional da UFU
repository_id_str
spelling Abrasão-corrosão em aços inoxidáveis ferríticosAbrasion-corrosion of ferritic stainless steelAbrasão-corrosãoCoeficiente de atritoAços inoxidáveisResistência ao desgasteTextura cristalográficaDesgaste mecânicoCorrosãoAbrasion-corrosionFriction coefficientStainless steelWear resistantCrystallographic textureCNPQ::ENGENHARIAS::ENGENHARIA MECANICAThe aim of this work was to study the behavior of ferritic stainless steels in abrasive-corrosive environment of 10%wt SiO2 + 1N H2SO4. It was developed an apparatus and a methodology to perform the tests. The equipment has a load cell to measure the normal and friction forces during the test, an original device due to the difficulty to use it without damaging in abrasivecorrosive environment. It was used samples of ferritic stainless 11Cr, 11CrTi, 16Cr, 16CrNb (Nb stabilized) and, for comparative purposes, the stainless steels 18Cr8Ni (austenitic), 17CrTiNb (ferritic) and the carbon steel A36. It was proceeded the mechanical characterization (hardness and tensile testing), chemical and metallographic test (grain size) of these samples. For 16Cr and 16CrNb steels the crystallographic texture was analyzed, by EBSD. It has been realized corrosion test at turbulent and aerated environment, abrasion and abrasion-corrosion test. So it was analyzed the polarization curves, the wear coefficient k and the samples, by SEM. It was clearly observed at the corrosion tests the increasing at corrosion resistance with the increasing of Cr content in the samples. Although the 18Cr8Ni was the hardest material, it had worse performance on the abrasion tests. In this abrasive system studied there was a wear resistance increased after prior cold deformation. For the abrasioncorrosion tests the 18Cr8Ni had the best performance, although it was the worse in abrasion test. The materials were ranked by the higher wear resistance due to the increasing Cr content that was associated to the corrosive influence on the total wear in this abrasive-corrosive environment. In abrasive-corrosive medium, the wear was lower when compared to the abrasive medium for all materials mainly due to the friction coefficient reduction. For the steels 16CrNb and 16Cr, it was observed a slight influence of crystallographic texture on the corrosion resistance in turbulent medium and abrasive wear. However, this distinction does not exist for the abrasion-corrosion tests. It was also noticed an influence of niobium carbides in reducing the wear coefficient, even in a soft matrix as 16CrNb steel.Doutor em Engenharia MecânicaO objetivo deste trabalho foi estudar o comportamento de aços inoxidáveis ferríticos em ambiente abrasivo-corrosivo, em solução de 10% SiO2 + 1N H2SO4. Foi projetado e construído um equipamento dotado de uma célula de carga para medir as forças normal e de atrito durante o ensaio, sendo um dispositivo inédito para este tipo de equipamento em sistema abrasivo-corrosivo. Em seguida, desenvolveu-se uma metodologia específica para os ensaios. Utilizou-se amostras de inoxidáveis ferríticos 11Cr, 11CrTi, 16Cr, 16CrNb (estabilizado ao Nb) e, para efeito comparativo, os aços inoxidáveis 18Cr8Ni (austenítico), 17CrTiNb (ferrítico), e aço carbono A36. Executou-se a caracterização mecânica (ensaio de dureza e de tração), química e metalográfica (tamanho de grão) das amostras. Para os aços 16Cr e 16CrNb analisou-se a textura cristalográfica, via EBSD. Foram realizados ensaios de corrosão em meio aerado e agitado, abrasão e abrasão-corrosão, sendo analisadas as curvas de polarização, o coeficiente de atrito e o coeficiente de desgaste k. Os ensaios de corrosão em meio aerado e agitado evidenciam de forma clara a maior resistência à corrosão em função do teor crescente de Cr nos materiais. O aço 18Cr8Ni teve pior desempenho nos ensaios de abrasão, embora fosse o mais duro. Neste sistema abrasivo houve um acréscimo da resistência ao desgaste após prévia deformação a frio. Para os ensaios de abrasão-corrosão o aço 18Cr8Ni, pior em abrasão, teve o melhor desempenho. No meio abrasivo-corrosivo, os materiais foram hierarquizados pela maior resistência ao desgaste em função do teor crescente de Cr, com o efeito da corrosão influenciando no desgaste. Em meio abrasivo o desgaste foi maior em relação ao meio abrasivo-corrosivo para todos os materiais. A causa fundamental foi a redução do coeficiente de atrito, sendo medido de forma inédita devido à versatilidade do equipamento construído. Para os aços 16Cr e 16CrNb verificou-se uma influência discreta da textura cristalográfica na resistência à corrosão em meio agitado, bem como ao desgaste abrasivo. Contudo, esta distinção inexiste para os ensaios de abrasão-corrosão combinados. Percebeu-se também uma influência dos carbonetos de Nb na redução do coeficiente de desgaste, mesmo em uma matriz macia como o aço 16CrNb.Universidade Federal de UberlândiaBRPrograma de Pós-graduação em Engenharia MecânicaEngenhariasUFUMello, José Daniel Biasoli dehttp://buscatextual.cnpq.br/buscatextual/visualizacv.do?id=K4783817J1Costa, Henara Lillianhttp://buscatextual.cnpq.br/buscatextual/visualizacv.do?id=K4721823P9Canobre, Sheila Cristinahttp://buscatextual.cnpq.br/buscatextual/visualizacv.do?id=K4775037T8Sinatora, Amiltonhttp://buscatextual.cnpq.br/buscatextual/visualizacv.do?id=K4787947H7Rocha, Luís Augusto Sousa Marques dahttp://buscatextual.cnpq.br/buscatextual/visualizacv.do?id=K4587040Z7Oliveira, Tarcísio Reis dehttp://buscatextual.cnpq.br/buscatextual/visualizacv.do?id=K4728115A1Labiapari, Wilian da Silva2016-06-22T18:39:48Z2016-02-172016-06-22T18:39:48Z2015-05-25info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/doctoralThesisapplication/pdfapplication/pdfapplication/pdfLABIAPARI, Wilian da Silva. Abrasion-corrosion of ferritic stainless steel. 2015. 211 f. Tese (Doutorado em Engenharias) - Universidade Federal de Uberlândia, Uberlândia, 2015. DOI https://doi.org/10.14393/ufu.te.2015.72.https://repositorio.ufu.br/handle/123456789/14772https://doi.org/10.14393/ufu.te.2015.72porinfo:eu-repo/semantics/openAccessreponame:Repositório Institucional da UFUinstname:Universidade Federal de Uberlândia (UFU)instacron:UFU2021-03-04T16:18:55Zoai:repositorio.ufu.br:123456789/14772Repositório InstitucionalONGhttp://repositorio.ufu.br/oai/requestdiinf@dirbi.ufu.bropendoar:2021-03-04T16:18:55Repositório Institucional da UFU - Universidade Federal de Uberlândia (UFU)false
dc.title.none.fl_str_mv Abrasão-corrosão em aços inoxidáveis ferríticos
Abrasion-corrosion of ferritic stainless steel
title Abrasão-corrosão em aços inoxidáveis ferríticos
spellingShingle Abrasão-corrosão em aços inoxidáveis ferríticos
Labiapari, Wilian da Silva
Abrasão-corrosão
Coeficiente de atrito
Aços inoxidáveis
Resistência ao desgaste
Textura cristalográfica
Desgaste mecânico
Corrosão
Abrasion-corrosion
Friction coefficient
Stainless steel
Wear resistant
Crystallographic texture
CNPQ::ENGENHARIAS::ENGENHARIA MECANICA
title_short Abrasão-corrosão em aços inoxidáveis ferríticos
title_full Abrasão-corrosão em aços inoxidáveis ferríticos
title_fullStr Abrasão-corrosão em aços inoxidáveis ferríticos
title_full_unstemmed Abrasão-corrosão em aços inoxidáveis ferríticos
title_sort Abrasão-corrosão em aços inoxidáveis ferríticos
author Labiapari, Wilian da Silva
author_facet Labiapari, Wilian da Silva
author_role author
dc.contributor.none.fl_str_mv Mello, José Daniel Biasoli de
http://buscatextual.cnpq.br/buscatextual/visualizacv.do?id=K4783817J1
Costa, Henara Lillian
http://buscatextual.cnpq.br/buscatextual/visualizacv.do?id=K4721823P9
Canobre, Sheila Cristina
http://buscatextual.cnpq.br/buscatextual/visualizacv.do?id=K4775037T8
Sinatora, Amilton
http://buscatextual.cnpq.br/buscatextual/visualizacv.do?id=K4787947H7
Rocha, Luís Augusto Sousa Marques da
http://buscatextual.cnpq.br/buscatextual/visualizacv.do?id=K4587040Z7
Oliveira, Tarcísio Reis de
http://buscatextual.cnpq.br/buscatextual/visualizacv.do?id=K4728115A1
dc.contributor.author.fl_str_mv Labiapari, Wilian da Silva
dc.subject.por.fl_str_mv Abrasão-corrosão
Coeficiente de atrito
Aços inoxidáveis
Resistência ao desgaste
Textura cristalográfica
Desgaste mecânico
Corrosão
Abrasion-corrosion
Friction coefficient
Stainless steel
Wear resistant
Crystallographic texture
CNPQ::ENGENHARIAS::ENGENHARIA MECANICA
topic Abrasão-corrosão
Coeficiente de atrito
Aços inoxidáveis
Resistência ao desgaste
Textura cristalográfica
Desgaste mecânico
Corrosão
Abrasion-corrosion
Friction coefficient
Stainless steel
Wear resistant
Crystallographic texture
CNPQ::ENGENHARIAS::ENGENHARIA MECANICA
description The aim of this work was to study the behavior of ferritic stainless steels in abrasive-corrosive environment of 10%wt SiO2 + 1N H2SO4. It was developed an apparatus and a methodology to perform the tests. The equipment has a load cell to measure the normal and friction forces during the test, an original device due to the difficulty to use it without damaging in abrasivecorrosive environment. It was used samples of ferritic stainless 11Cr, 11CrTi, 16Cr, 16CrNb (Nb stabilized) and, for comparative purposes, the stainless steels 18Cr8Ni (austenitic), 17CrTiNb (ferritic) and the carbon steel A36. It was proceeded the mechanical characterization (hardness and tensile testing), chemical and metallographic test (grain size) of these samples. For 16Cr and 16CrNb steels the crystallographic texture was analyzed, by EBSD. It has been realized corrosion test at turbulent and aerated environment, abrasion and abrasion-corrosion test. So it was analyzed the polarization curves, the wear coefficient k and the samples, by SEM. It was clearly observed at the corrosion tests the increasing at corrosion resistance with the increasing of Cr content in the samples. Although the 18Cr8Ni was the hardest material, it had worse performance on the abrasion tests. In this abrasive system studied there was a wear resistance increased after prior cold deformation. For the abrasioncorrosion tests the 18Cr8Ni had the best performance, although it was the worse in abrasion test. The materials were ranked by the higher wear resistance due to the increasing Cr content that was associated to the corrosive influence on the total wear in this abrasive-corrosive environment. In abrasive-corrosive medium, the wear was lower when compared to the abrasive medium for all materials mainly due to the friction coefficient reduction. For the steels 16CrNb and 16Cr, it was observed a slight influence of crystallographic texture on the corrosion resistance in turbulent medium and abrasive wear. However, this distinction does not exist for the abrasion-corrosion tests. It was also noticed an influence of niobium carbides in reducing the wear coefficient, even in a soft matrix as 16CrNb steel.
publishDate 2015
dc.date.none.fl_str_mv 2015-05-25
2016-06-22T18:39:48Z
2016-02-17
2016-06-22T18:39:48Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/doctoralThesis
format doctoralThesis
status_str publishedVersion
dc.identifier.uri.fl_str_mv LABIAPARI, Wilian da Silva. Abrasion-corrosion of ferritic stainless steel. 2015. 211 f. Tese (Doutorado em Engenharias) - Universidade Federal de Uberlândia, Uberlândia, 2015. DOI https://doi.org/10.14393/ufu.te.2015.72.
https://repositorio.ufu.br/handle/123456789/14772
https://doi.org/10.14393/ufu.te.2015.72
identifier_str_mv LABIAPARI, Wilian da Silva. Abrasion-corrosion of ferritic stainless steel. 2015. 211 f. Tese (Doutorado em Engenharias) - Universidade Federal de Uberlândia, Uberlândia, 2015. DOI https://doi.org/10.14393/ufu.te.2015.72.
url https://repositorio.ufu.br/handle/123456789/14772
https://doi.org/10.14393/ufu.te.2015.72
dc.language.iso.fl_str_mv por
language por
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv application/pdf
application/pdf
application/pdf
dc.publisher.none.fl_str_mv Universidade Federal de Uberlândia
BR
Programa de Pós-graduação em Engenharia Mecânica
Engenharias
UFU
publisher.none.fl_str_mv Universidade Federal de Uberlândia
BR
Programa de Pós-graduação em Engenharia Mecânica
Engenharias
UFU
dc.source.none.fl_str_mv reponame:Repositório Institucional da UFU
instname:Universidade Federal de Uberlândia (UFU)
instacron:UFU
instname_str Universidade Federal de Uberlândia (UFU)
instacron_str UFU
institution UFU
reponame_str Repositório Institucional da UFU
collection Repositório Institucional da UFU
repository.name.fl_str_mv Repositório Institucional da UFU - Universidade Federal de Uberlândia (UFU)
repository.mail.fl_str_mv diinf@dirbi.ufu.br
_version_ 1805569706467262464