Characterization of PVDF/HAP composites for medical applications
Autor(a) principal: | |
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Data de Publicação: | 2007 |
Outros Autores: | , , , , |
Tipo de documento: | Artigo |
Idioma: | eng |
Título da fonte: | Repositório Institucional da UNESP |
Texto Completo: | http://dx.doi.org/10.1590/S1516-14392007000300005 http://hdl.handle.net/11449/30583 |
Resumo: | Biomaterials (composites and blends) play a major role in the health of modern society. This paper reports on the preparation and characterization of polyvinylidene fluoride (PVDF) and hydroxyapatite (HAP) composites, analyzing the incorporation of HAP in PVDF and investigating their mechanical properties and cytotoxicity (biocompatibility) for use in bone restoration and filling. The material was prepared in film form by the casting method. PVDF pellets were dissolved in dimethylacetamide (DMA), a HAP/DMA emulsion was prepared. The materials were mixed in proportions of 100/00, 90/10, 80/20, 70/30, 60/40, 50/50, 40/60, 30/70 in weight and left to dry in an oven, resulting in homogeneous, flexible films which were characterized by scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS), X ray diffractometry (XRD), contact angle measurement, and by mechanical and cytotoxicity tests. |
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Repositório Institucional da UNESP |
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Characterization of PVDF/HAP composites for medical applicationspolyvinylidene fluoridepolymer compositesbiomaterialshydroxyapatiteBiomaterials (composites and blends) play a major role in the health of modern society. This paper reports on the preparation and characterization of polyvinylidene fluoride (PVDF) and hydroxyapatite (HAP) composites, analyzing the incorporation of HAP in PVDF and investigating their mechanical properties and cytotoxicity (biocompatibility) for use in bone restoration and filling. The material was prepared in film form by the casting method. PVDF pellets were dissolved in dimethylacetamide (DMA), a HAP/DMA emulsion was prepared. The materials were mixed in proportions of 100/00, 90/10, 80/20, 70/30, 60/40, 50/50, 40/60, 30/70 in weight and left to dry in an oven, resulting in homogeneous, flexible films which were characterized by scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS), X ray diffractometry (XRD), contact angle measurement, and by mechanical and cytotoxicity tests.Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)Instituto de Pesquisas Energéticas e Nucleares Centro de Ciência e Tecnologia de MateriaisUNESP Instituto de Química Departamento de Físico-QuímicaUniversidade Estadual de Campinas Faculdade de Engenharia Química Departamento de Tecnologia de PolímerosUNESP Instituto de Química Departamento de Físico-QuímicaABM, ABC, ABPolInstituto de Pesquisas Energéticas e Nucleares (IPEN)Universidade Estadual Paulista (Unesp)Universidade Estadual de Campinas (UNICAMP)Braga, Francisco José CorreaRogero, Sizue OtaCouto, Antônio AugustoMarques, Rodrigo Fernando Costa [UNESP]Ribeiro, Alexandre AntunesCampos, João Sinézio de Carvalho2014-05-20T15:17:43Z2014-05-20T15:17:43Z2007-09-01info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/article247-251application/pdfhttp://dx.doi.org/10.1590/S1516-14392007000300005Materials Research. ABM, ABC, ABPol, v. 10, n. 3, p. 247-251, 2007.1516-1439http://hdl.handle.net/11449/3058310.1590/S1516-14392007000300005S1516-14392007000300005S1516-14392007000300005.pdf21159426216941740000-0003-0195-3885SciELOreponame:Repositório Institucional da UNESPinstname:Universidade Estadual Paulista (UNESP)instacron:UNESPengMaterials Research1.1030,398info:eu-repo/semantics/openAccess2023-12-15T06:20:11Zoai:repositorio.unesp.br:11449/30583Repositório InstitucionalPUBhttp://repositorio.unesp.br/oai/requestopendoar:29462024-08-05T20:26:09.813806Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP)false |
dc.title.none.fl_str_mv |
Characterization of PVDF/HAP composites for medical applications |
title |
Characterization of PVDF/HAP composites for medical applications |
spellingShingle |
Characterization of PVDF/HAP composites for medical applications Braga, Francisco José Correa polyvinylidene fluoride polymer composites biomaterials hydroxyapatite |
title_short |
Characterization of PVDF/HAP composites for medical applications |
title_full |
Characterization of PVDF/HAP composites for medical applications |
title_fullStr |
Characterization of PVDF/HAP composites for medical applications |
title_full_unstemmed |
Characterization of PVDF/HAP composites for medical applications |
title_sort |
Characterization of PVDF/HAP composites for medical applications |
author |
Braga, Francisco José Correa |
author_facet |
Braga, Francisco José Correa Rogero, Sizue Ota Couto, Antônio Augusto Marques, Rodrigo Fernando Costa [UNESP] Ribeiro, Alexandre Antunes Campos, João Sinézio de Carvalho |
author_role |
author |
author2 |
Rogero, Sizue Ota Couto, Antônio Augusto Marques, Rodrigo Fernando Costa [UNESP] Ribeiro, Alexandre Antunes Campos, João Sinézio de Carvalho |
author2_role |
author author author author author |
dc.contributor.none.fl_str_mv |
Instituto de Pesquisas Energéticas e Nucleares (IPEN) Universidade Estadual Paulista (Unesp) Universidade Estadual de Campinas (UNICAMP) |
dc.contributor.author.fl_str_mv |
Braga, Francisco José Correa Rogero, Sizue Ota Couto, Antônio Augusto Marques, Rodrigo Fernando Costa [UNESP] Ribeiro, Alexandre Antunes Campos, João Sinézio de Carvalho |
dc.subject.por.fl_str_mv |
polyvinylidene fluoride polymer composites biomaterials hydroxyapatite |
topic |
polyvinylidene fluoride polymer composites biomaterials hydroxyapatite |
description |
Biomaterials (composites and blends) play a major role in the health of modern society. This paper reports on the preparation and characterization of polyvinylidene fluoride (PVDF) and hydroxyapatite (HAP) composites, analyzing the incorporation of HAP in PVDF and investigating their mechanical properties and cytotoxicity (biocompatibility) for use in bone restoration and filling. The material was prepared in film form by the casting method. PVDF pellets were dissolved in dimethylacetamide (DMA), a HAP/DMA emulsion was prepared. The materials were mixed in proportions of 100/00, 90/10, 80/20, 70/30, 60/40, 50/50, 40/60, 30/70 in weight and left to dry in an oven, resulting in homogeneous, flexible films which were characterized by scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS), X ray diffractometry (XRD), contact angle measurement, and by mechanical and cytotoxicity tests. |
publishDate |
2007 |
dc.date.none.fl_str_mv |
2007-09-01 2014-05-20T15:17:43Z 2014-05-20T15:17:43Z |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
http://dx.doi.org/10.1590/S1516-14392007000300005 Materials Research. ABM, ABC, ABPol, v. 10, n. 3, p. 247-251, 2007. 1516-1439 http://hdl.handle.net/11449/30583 10.1590/S1516-14392007000300005 S1516-14392007000300005 S1516-14392007000300005.pdf 2115942621694174 0000-0003-0195-3885 |
url |
http://dx.doi.org/10.1590/S1516-14392007000300005 http://hdl.handle.net/11449/30583 |
identifier_str_mv |
Materials Research. ABM, ABC, ABPol, v. 10, n. 3, p. 247-251, 2007. 1516-1439 10.1590/S1516-14392007000300005 S1516-14392007000300005 S1516-14392007000300005.pdf 2115942621694174 0000-0003-0195-3885 |
dc.language.iso.fl_str_mv |
eng |
language |
eng |
dc.relation.none.fl_str_mv |
Materials Research 1.103 0,398 |
dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess |
eu_rights_str_mv |
openAccess |
dc.format.none.fl_str_mv |
247-251 application/pdf |
dc.publisher.none.fl_str_mv |
ABM, ABC, ABPol |
publisher.none.fl_str_mv |
ABM, ABC, ABPol |
dc.source.none.fl_str_mv |
SciELO reponame:Repositório Institucional da UNESP instname:Universidade Estadual Paulista (UNESP) instacron:UNESP |
instname_str |
Universidade Estadual Paulista (UNESP) |
instacron_str |
UNESP |
institution |
UNESP |
reponame_str |
Repositório Institucional da UNESP |
collection |
Repositório Institucional da UNESP |
repository.name.fl_str_mv |
Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP) |
repository.mail.fl_str_mv |
|
_version_ |
1808129201336745984 |