Study of the incorporation of TiO2/Ag nanoparticles in polyamide by casting method aiming for biocide application

Detalhes bibliográficos
Autor(a) principal: VECCHIA, MARIA E.K.D.
Data de Publicação: 2022
Outros Autores: ZAINE, MARIANA A., KOMATSU, LUIZ G.H., DIPOLD, JESSICA, FREITAS, ANDERSON Z., WETTER, NIKLAUS, PARRA, DUCLERC F., CONGRESSO BRASILEIRO DE POL??MEROS, 16.
Tipo de documento: Artigo de conferência
Título da fonte: Repositório Institucional do IPEN
Texto Completo: http://repositorio.ipen.br/handle/123456789/32857
Resumo: This study consists in the characterization of polyamide (PA6) films charged with different concentrations of silver nanoparticles deposited in titanium dioxide (TiO2) carrier. The silver nanoparticles were synthesized according to the method adapted from Turkevich using a titanium dioxide carrier and inserted, by suspension, in a polyamide solution. The preparation of PA: AgNp films was performed by the casting method by the dissolution of PA pellets in formic acid. The analysis and characterization of the films by the XRD, DSC, TGA and Raman confocal techniques indicated incorporation of nanoparticles into the polymers, a second thermogravimetric decomposition event as the concentration of AgNp-TiO2 increased and there was no significant change in crystallinity.
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spelling 2022-03-25T13:40:50Z2022-03-25T13:40:50Z24-28 de outubro, 2021http://repositorio.ipen.br/handle/123456789/328570000-0002-6481-01550000-0002-9379-95300000-0002-5018-9126This study consists in the characterization of polyamide (PA6) films charged with different concentrations of silver nanoparticles deposited in titanium dioxide (TiO2) carrier. The silver nanoparticles were synthesized according to the method adapted from Turkevich using a titanium dioxide carrier and inserted, by suspension, in a polyamide solution. The preparation of PA: AgNp films was performed by the casting method by the dissolution of PA pellets in formic acid. The analysis and characterization of the films by the XRD, DSC, TGA and Raman confocal techniques indicated incorporation of nanoparticles into the polymers, a second thermogravimetric decomposition event as the concentration of AgNp-TiO2 increased and there was no significant change in crystallinity.Submitted by Pedro Silva Filho (pfsilva@ipen.br) on 2022-03-25T13:40:50Z No. of bitstreams: 1 28579.pdf: 934386 bytes, checksum: 54aaaa897a1c9e194bbed9a71454122f (MD5)Made available in DSpace on 2022-03-25T13:40:50Z (GMT). No. of bitstreams: 1 28579.pdf: 934386 bytes, checksum: 54aaaa897a1c9e194bbed9a71454122f (MD5)Conselho Nacional de Desenvolvimento Cient??fico e Tecnol??gico (CNPq)Funda????o de Amparo ?? Pesquisa do Estado de S??o Paulo (FAPESP)CNPq: 161392/2020-2; 101108/2021-4FAPESP: 18/19240-5; 17/50332-0789-793Aptor Softwarenanoparticlespolyamidesnanostructuressilvertitanium oxidesStudy of the incorporation of TiO2/Ag nanoparticles in polyamide by casting method aiming for biocide applicationinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/conferenceObjectCBPOLNS??o Carlos, SPOuro Preto, MG1533415519972215190880919562600600600600600600600VECCHIA, MARIA E.K.D.ZAINE, MARIANA A.KOMATSU, LUIZ G.H.DIPOLD, JESSICAFREITAS, ANDERSON Z.WETTER, NIKLAUSPARRA, DUCLERC F.CONGRESSO BRASILEIRO DE POL??MEROS, 16.info:eu-repo/semantics/openAccessreponame:Repositório Institucional do IPENinstname:Instituto de Pesquisas Energéticas e Nucleares (IPEN)instacron:IPEN285792021PARRA, DUCLERC F.WETTER, NIKLAUSFREITAS, ANDERSON Z.DIPOLD, JESSICAKOMATSU, LUIZ G.H.ZAINE, MARIANA A.VECCHIA, MARIA E.K.D.22-03Anais5629198801519097221551915334PARRA, DUCLERC F.:562:740:NWETTER, NIKLAUS:919:910:NFREITAS, ANDERSON Z.:880:920:NDIPOLD, JESSICA:15190:910:NKOMATSU, LUIZ G.H.:9722:750:NZAINE, MARIANA A.:15519:740:NVECCHIA, MARIA E.K.D.:15334:740:SLICENSElicense.txtlicense.txttext/plain; charset=utf-81748http://repositorio.ipen.br/bitstream/123456789/32857/2/license.txt8a4605be74aa9ea9d79846c1fba20a33MD52ORIGINAL28579.pdf28579.pdfapplication/pdf934386http://repositorio.ipen.br/bitstream/123456789/32857/1/28579.pdf54aaaa897a1c9e194bbed9a71454122fMD51123456789/328572022-05-03 12:59:27.588oai:repositorio.ipen.br:123456789/32857Tk9URTogUExBQ0UgWU9VUiBPV04gTElDRU5TRSBIRVJFClRoaXMgc2FtcGxlIGxpY2Vuc2UgaXMgcHJvdmlkZWQgZm9yIGluZm9ybWF0aW9uYWwgcHVycG9zZXMgb25seS4KCk5PTi1FWENMVVNJVkUgRElTVFJJQlVUSU9OIExJQ0VOU0UKCkJ5IHNpZ25pbmcgYW5kIHN1Ym1pdHRpbmcgdGhpcyBsaWNlbnNlLCB5b3UgKHRoZSBhdXRob3Iocykgb3IgY29weXJpZ2h0Cm93bmVyKSBncmFudHMgdG8gRFNwYWNlIFVuaXZlcnNpdHkgKERTVSkgdGhlIG5vbi1leGNsdXNpdmUgcmlnaHQgdG8gcmVwcm9kdWNlLAp0cmFuc2xhdGUgKGFzIGRlZmluZWQgYmVsb3cpLCBhbmQvb3IgZGlzdHJpYnV0ZSB5b3VyIHN1Ym1pc3Npb24gKGluY2x1ZGluZwp0aGUgYWJzdHJhY3QpIHdvcmxkd2lkZSBpbiBwcmludCBhbmQgZWxlY3Ryb25pYyBmb3JtYXQgYW5kIGluIGFueSBtZWRpdW0sCmluY2x1ZGluZyBidXQgbm90IGxpbWl0ZWQgdG8gYXVkaW8gb3IgdmlkZW8uCgpZb3UgYWdyZWUgdGhhdCBEU1UgbWF5LCB3aXRob3V0IGNoYW5naW5nIHRoZSBjb250ZW50LCB0cmFuc2xhdGUgdGhlCnN1Ym1pc3Npb24gdG8gYW55IG1lZGl1bSBvciBmb3JtYXQgZm9yIHRoZSBwdXJwb3NlIG9mIHByZXNlcnZhdGlvbi4KCllvdSBhbHNvIGFncmVlIHRoYXQgRFNVIG1heSBrZWVwIG1vcmUgdGhhbiBvbmUgY29weSBvZiB0aGlzIHN1Ym1pc3Npb24gZm9yCnB1cnBvc2VzIG9mIHNlY3VyaXR5LCBiYWNrLXVwIGFuZCBwcmVzZXJ2YXRpb24uCgpZb3UgcmVwcmVzZW50IHRoYXQgdGhlIHN1Ym1pc3Npb24gaXMgeW91ciBvcmlnaW5hbCB3b3JrLCBhbmQgdGhhdCB5b3UgaGF2ZQp0aGUgcmlnaHQgdG8gZ3JhbnQgdGhlIHJpZ2h0cyBjb250YWluZWQgaW4gdGhpcyBsaWNlbnNlLiBZb3UgYWxzbyByZXByZXNlbnQKdGhhdCB5b3VyIHN1Ym1pc3Npb24gZG9lcyBub3QsIHRvIHRoZSBiZXN0IG9mIHlvdXIga25vd2xlZGdlLCBpbmZyaW5nZSB1cG9uCmFueW9uZSdzIGNvcHlyaWdodC4KCklmIHRoZSBzdWJtaXNzaW9uIGNvbnRhaW5zIG1hdGVyaWFsIGZvciB3aGljaCB5b3UgZG8gbm90IGhvbGQgY29weXJpZ2h0LAp5b3UgcmVwcmVzZW50IHRoYXQgeW91IGhhdmUgb2J0YWluZWQgdGhlIHVucmVzdHJpY3RlZCBwZXJtaXNzaW9uIG9mIHRoZQpjb3B5cmlnaHQgb3duZXIgdG8gZ3JhbnQgRFNVIHRoZSByaWdodHMgcmVxdWlyZWQgYnkgdGhpcyBsaWNlbnNlLCBhbmQgdGhhdApzdWNoIHRoaXJkLXBhcnR5IG93bmVkIG1hdGVyaWFsIGlzIGNsZWFybHkgaWRlbnRpZmllZCBhbmQgYWNrbm93bGVkZ2VkCndpdGhpbiB0aGUgdGV4dCBvciBjb250ZW50IG9mIHRoZSBzdWJtaXNzaW9uLgoKSUYgVEhFIFNVQk1JU1NJT04gSVMgQkFTRUQgVVBPTiBXT1JLIFRIQVQgSEFTIEJFRU4gU1BPTlNPUkVEIE9SIFNVUFBPUlRFRApCWSBBTiBBR0VOQ1kgT1IgT1JHQU5JWkFUSU9OIE9USEVSIFRIQU4gRFNVLCBZT1UgUkVQUkVTRU5UIFRIQVQgWU9VIEhBVkUKRlVMRklMTEVEIEFOWSBSSUdIVCBPRiBSRVZJRVcgT1IgT1RIRVIgT0JMSUdBVElPTlMgUkVRVUlSRUQgQlkgU1VDSApDT05UUkFDVCBPUiBBR1JFRU1FTlQuCgpEU1Ugd2lsbCBjbGVhcmx5IGlkZW50aWZ5IHlvdXIgbmFtZShzKSBhcyB0aGUgYXV0aG9yKHMpIG9yIG93bmVyKHMpIG9mIHRoZQpzdWJtaXNzaW9uLCBhbmQgd2lsbCBub3QgbWFrZSBhbnkgYWx0ZXJhdGlvbiwgb3RoZXIgdGhhbiBhcyBhbGxvd2VkIGJ5IHRoaXMKbGljZW5zZSwgdG8geW91ciBzdWJtaXNzaW9uLgo=Repositório InstitucionalPUBhttp://repositorio.ipen.br/oai/requestbibl@ipen.bropendoar:45102022-05-03T12:59:27Repositório Institucional do IPEN - Instituto de Pesquisas Energéticas e Nucleares (IPEN)false
dc.title.pt_BR.fl_str_mv Study of the incorporation of TiO2/Ag nanoparticles in polyamide by casting method aiming for biocide application
title Study of the incorporation of TiO2/Ag nanoparticles in polyamide by casting method aiming for biocide application
spellingShingle Study of the incorporation of TiO2/Ag nanoparticles in polyamide by casting method aiming for biocide application
VECCHIA, MARIA E.K.D.
nanoparticles
polyamides
nanostructures
silver
titanium oxides
title_short Study of the incorporation of TiO2/Ag nanoparticles in polyamide by casting method aiming for biocide application
title_full Study of the incorporation of TiO2/Ag nanoparticles in polyamide by casting method aiming for biocide application
title_fullStr Study of the incorporation of TiO2/Ag nanoparticles in polyamide by casting method aiming for biocide application
title_full_unstemmed Study of the incorporation of TiO2/Ag nanoparticles in polyamide by casting method aiming for biocide application
title_sort Study of the incorporation of TiO2/Ag nanoparticles in polyamide by casting method aiming for biocide application
author VECCHIA, MARIA E.K.D.
author_facet VECCHIA, MARIA E.K.D.
ZAINE, MARIANA A.
KOMATSU, LUIZ G.H.
DIPOLD, JESSICA
FREITAS, ANDERSON Z.
WETTER, NIKLAUS
PARRA, DUCLERC F.
CONGRESSO BRASILEIRO DE POL??MEROS, 16.
author_role author
author2 ZAINE, MARIANA A.
KOMATSU, LUIZ G.H.
DIPOLD, JESSICA
FREITAS, ANDERSON Z.
WETTER, NIKLAUS
PARRA, DUCLERC F.
CONGRESSO BRASILEIRO DE POL??MEROS, 16.
author2_role author
author
author
author
author
author
author
dc.contributor.author.fl_str_mv VECCHIA, MARIA E.K.D.
ZAINE, MARIANA A.
KOMATSU, LUIZ G.H.
DIPOLD, JESSICA
FREITAS, ANDERSON Z.
WETTER, NIKLAUS
PARRA, DUCLERC F.
CONGRESSO BRASILEIRO DE POL??MEROS, 16.
dc.subject.por.fl_str_mv nanoparticles
polyamides
nanostructures
silver
titanium oxides
topic nanoparticles
polyamides
nanostructures
silver
titanium oxides
description This study consists in the characterization of polyamide (PA6) films charged with different concentrations of silver nanoparticles deposited in titanium dioxide (TiO2) carrier. The silver nanoparticles were synthesized according to the method adapted from Turkevich using a titanium dioxide carrier and inserted, by suspension, in a polyamide solution. The preparation of PA: AgNp films was performed by the casting method by the dissolution of PA pellets in formic acid. The analysis and characterization of the films by the XRD, DSC, TGA and Raman confocal techniques indicated incorporation of nanoparticles into the polymers, a second thermogravimetric decomposition event as the concentration of AgNp-TiO2 increased and there was no significant change in crystallinity.
publishDate 2022
dc.date.evento.pt_BR.fl_str_mv 24-28 de outubro, 2021
dc.date.accessioned.fl_str_mv 2022-03-25T13:40:50Z
dc.date.available.fl_str_mv 2022-03-25T13:40:50Z
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