Methods for the determination of organochlorine pesticide residues in human serum

Detalhes bibliográficos
Autor(a) principal: Lino, Celeste Matos
Data de Publicação: 1998
Outros Autores: Azzolini, Clara B. Ferreira, Nunes, Domingos S. Valente, Silva, José, Silveira, Maria Irene Noronha da
Tipo de documento: Artigo
Idioma: eng
Título da fonte: Repositório Científico de Acesso Aberto de Portugal (Repositórios Cientìficos)
Texto Completo: http://hdl.handle.net/10316/5824
https://doi.org/10.1016/S0378-4347(98)00284-9
Resumo: The effectiveness of solid-phase extraction with Florisil for the determination of 12 organochlorine pesticide residues from human serum was examined. Recoveries greater than 84% and coefficients of variation better than 19% were obtained. Others methods, such as column partition and matrix solid-phase dispersion, were compared. The better method provides quantification limits ranging from 1.08 [mu]g/l for [gamma]-HCH and 37.5 [mu]g/l for p,p'-DDT when capillary gas-liquid chromatography with electron-capture detection is used for the final determination.
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spelling Methods for the determination of organochlorine pesticide residues in human serumOrganochlorine pesticidesThe effectiveness of solid-phase extraction with Florisil for the determination of 12 organochlorine pesticide residues from human serum was examined. Recoveries greater than 84% and coefficients of variation better than 19% were obtained. Others methods, such as column partition and matrix solid-phase dispersion, were compared. The better method provides quantification limits ranging from 1.08 [mu]g/l for [gamma]-HCH and 37.5 [mu]g/l for p,p'-DDT when capillary gas-liquid chromatography with electron-capture detection is used for the final determination.http://www.sciencedirect.com/science/article/B6TG9-3TWXX3J-J/1/b7804f2ca479d02daf6147329c4f29c31998info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/articleaplication/PDFhttp://hdl.handle.net/10316/5824http://hdl.handle.net/10316/5824https://doi.org/10.1016/S0378-4347(98)00284-9engJournal of Chromatography B: Biomedical Sciences and Applications. 716:1-2 (1998) 147-152Lino, Celeste MatosAzzolini, Clara B. FerreiraNunes, Domingos S. ValenteSilva, JoséSilveira, Maria Irene Noronha dainfo:eu-repo/semantics/openAccessreponame:Repositório Científico de Acesso Aberto de Portugal (Repositórios Cientìficos)instname:Agência para a Sociedade do Conhecimento (UMIC) - FCT - Sociedade da Informaçãoinstacron:RCAAP2021-10-27T11:33:44ZPortal AgregadorONG
dc.title.none.fl_str_mv Methods for the determination of organochlorine pesticide residues in human serum
title Methods for the determination of organochlorine pesticide residues in human serum
spellingShingle Methods for the determination of organochlorine pesticide residues in human serum
Lino, Celeste Matos
Organochlorine pesticides
title_short Methods for the determination of organochlorine pesticide residues in human serum
title_full Methods for the determination of organochlorine pesticide residues in human serum
title_fullStr Methods for the determination of organochlorine pesticide residues in human serum
title_full_unstemmed Methods for the determination of organochlorine pesticide residues in human serum
title_sort Methods for the determination of organochlorine pesticide residues in human serum
author Lino, Celeste Matos
author_facet Lino, Celeste Matos
Azzolini, Clara B. Ferreira
Nunes, Domingos S. Valente
Silva, José
Silveira, Maria Irene Noronha da
author_role author
author2 Azzolini, Clara B. Ferreira
Nunes, Domingos S. Valente
Silva, José
Silveira, Maria Irene Noronha da
author2_role author
author
author
author
dc.contributor.author.fl_str_mv Lino, Celeste Matos
Azzolini, Clara B. Ferreira
Nunes, Domingos S. Valente
Silva, José
Silveira, Maria Irene Noronha da
dc.subject.por.fl_str_mv Organochlorine pesticides
topic Organochlorine pesticides
description The effectiveness of solid-phase extraction with Florisil for the determination of 12 organochlorine pesticide residues from human serum was examined. Recoveries greater than 84% and coefficients of variation better than 19% were obtained. Others methods, such as column partition and matrix solid-phase dispersion, were compared. The better method provides quantification limits ranging from 1.08 [mu]g/l for [gamma]-HCH and 37.5 [mu]g/l for p,p'-DDT when capillary gas-liquid chromatography with electron-capture detection is used for the final determination.
publishDate 1998
dc.date.none.fl_str_mv 1998
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
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status_str publishedVersion
dc.identifier.uri.fl_str_mv http://hdl.handle.net/10316/5824
http://hdl.handle.net/10316/5824
https://doi.org/10.1016/S0378-4347(98)00284-9
url http://hdl.handle.net/10316/5824
https://doi.org/10.1016/S0378-4347(98)00284-9
dc.language.iso.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv Journal of Chromatography B: Biomedical Sciences and Applications. 716:1-2 (1998) 147-152
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv aplication/PDF
dc.source.none.fl_str_mv reponame:Repositório Científico de Acesso Aberto de Portugal (Repositórios Cientìficos)
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