HPLC profile and simultaneous quantitative analysis of tingenone and pristimerin in four Celastraceae species using HPLC-UV-DAD-MS

Detalhes bibliográficos
Autor(a) principal: Araujo-León,Jesús Alfredo
Data de Publicação: 2019
Outros Autores: Cantillo-Ciau,Zulema, Ruiz-Ciau,Durcy Verenice, Coral-Martínez,Tania Isolina
Tipo de documento: Artigo
Idioma: eng
Título da fonte: Revista Brasileira de Farmacognosia (Online)
Texto Completo: http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0102-695X2019000200171
Resumo: ABSTRACT A validated method for the identification and authentication of tingenone and pristimerin was developed using HPLC. The chromatographic profile analysis was combined with simultaneous quantification in Crossopetalum rhacoma Crantz, Cassine xylocarpa Vent, Semialarium mexicanum (Miers) Mennega (known as cancerina), and Maytenus phyllanthoides Benth, through microwave-assisted extraction. The HPLC profiles of the four analyzed species showed three similar signals, which corresponded to the main chemotaxonomic markers of the Celastraceae family: quinonemethide triterpenes. HPLC profile analysis was used as a tool to identify the relationship with the quinonemethide triterpenes, for establishing the taxonomic position of some species whose placement in, or within, the Celastraceae family is uncertain.
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spelling HPLC profile and simultaneous quantitative analysis of tingenone and pristimerin in four Celastraceae species using HPLC-UV-DAD-MSChemotaxonic markersHPLC-UV-DAD-MSHPLC profileQuinonemethide triterpenesABSTRACT A validated method for the identification and authentication of tingenone and pristimerin was developed using HPLC. The chromatographic profile analysis was combined with simultaneous quantification in Crossopetalum rhacoma Crantz, Cassine xylocarpa Vent, Semialarium mexicanum (Miers) Mennega (known as cancerina), and Maytenus phyllanthoides Benth, through microwave-assisted extraction. The HPLC profiles of the four analyzed species showed three similar signals, which corresponded to the main chemotaxonomic markers of the Celastraceae family: quinonemethide triterpenes. HPLC profile analysis was used as a tool to identify the relationship with the quinonemethide triterpenes, for establishing the taxonomic position of some species whose placement in, or within, the Celastraceae family is uncertain.Sociedade Brasileira de Farmacognosia2019-04-01info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersiontext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S0102-695X2019000200171Revista Brasileira de Farmacognosia v.29 n.2 2019reponame:Revista Brasileira de Farmacognosia (Online)instname:Sociedade Brasileira de Farmacognosia (SBFgnosia)instacron:SBFGNOSIA10.1016/j.bjp.2018.12.009info:eu-repo/semantics/openAccessAraujo-León,Jesús AlfredoCantillo-Ciau,ZulemaRuiz-Ciau,Durcy VereniceCoral-Martínez,Tania Isolinaeng2019-05-21T00:00:00Zoai:scielo:S0102-695X2019000200171Revistahttp://www.sbfgnosia.org.br/revista/https://old.scielo.br/oai/scielo-oai.phprbgnosia@ltf.ufpb.br1981-528X0102-695Xopendoar:2019-05-21T00:00Revista Brasileira de Farmacognosia (Online) - Sociedade Brasileira de Farmacognosia (SBFgnosia)false
dc.title.none.fl_str_mv HPLC profile and simultaneous quantitative analysis of tingenone and pristimerin in four Celastraceae species using HPLC-UV-DAD-MS
title HPLC profile and simultaneous quantitative analysis of tingenone and pristimerin in four Celastraceae species using HPLC-UV-DAD-MS
spellingShingle HPLC profile and simultaneous quantitative analysis of tingenone and pristimerin in four Celastraceae species using HPLC-UV-DAD-MS
Araujo-León,Jesús Alfredo
Chemotaxonic markers
HPLC-UV-DAD-MS
HPLC profile
Quinonemethide triterpenes
title_short HPLC profile and simultaneous quantitative analysis of tingenone and pristimerin in four Celastraceae species using HPLC-UV-DAD-MS
title_full HPLC profile and simultaneous quantitative analysis of tingenone and pristimerin in four Celastraceae species using HPLC-UV-DAD-MS
title_fullStr HPLC profile and simultaneous quantitative analysis of tingenone and pristimerin in four Celastraceae species using HPLC-UV-DAD-MS
title_full_unstemmed HPLC profile and simultaneous quantitative analysis of tingenone and pristimerin in four Celastraceae species using HPLC-UV-DAD-MS
title_sort HPLC profile and simultaneous quantitative analysis of tingenone and pristimerin in four Celastraceae species using HPLC-UV-DAD-MS
author Araujo-León,Jesús Alfredo
author_facet Araujo-León,Jesús Alfredo
Cantillo-Ciau,Zulema
Ruiz-Ciau,Durcy Verenice
Coral-Martínez,Tania Isolina
author_role author
author2 Cantillo-Ciau,Zulema
Ruiz-Ciau,Durcy Verenice
Coral-Martínez,Tania Isolina
author2_role author
author
author
dc.contributor.author.fl_str_mv Araujo-León,Jesús Alfredo
Cantillo-Ciau,Zulema
Ruiz-Ciau,Durcy Verenice
Coral-Martínez,Tania Isolina
dc.subject.por.fl_str_mv Chemotaxonic markers
HPLC-UV-DAD-MS
HPLC profile
Quinonemethide triterpenes
topic Chemotaxonic markers
HPLC-UV-DAD-MS
HPLC profile
Quinonemethide triterpenes
description ABSTRACT A validated method for the identification and authentication of tingenone and pristimerin was developed using HPLC. The chromatographic profile analysis was combined with simultaneous quantification in Crossopetalum rhacoma Crantz, Cassine xylocarpa Vent, Semialarium mexicanum (Miers) Mennega (known as cancerina), and Maytenus phyllanthoides Benth, through microwave-assisted extraction. The HPLC profiles of the four analyzed species showed three similar signals, which corresponded to the main chemotaxonomic markers of the Celastraceae family: quinonemethide triterpenes. HPLC profile analysis was used as a tool to identify the relationship with the quinonemethide triterpenes, for establishing the taxonomic position of some species whose placement in, or within, the Celastraceae family is uncertain.
publishDate 2019
dc.date.none.fl_str_mv 2019-04-01
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0102-695X2019000200171
url http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0102-695X2019000200171
dc.language.iso.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv 10.1016/j.bjp.2018.12.009
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv text/html
dc.publisher.none.fl_str_mv Sociedade Brasileira de Farmacognosia
publisher.none.fl_str_mv Sociedade Brasileira de Farmacognosia
dc.source.none.fl_str_mv Revista Brasileira de Farmacognosia v.29 n.2 2019
reponame:Revista Brasileira de Farmacognosia (Online)
instname:Sociedade Brasileira de Farmacognosia (SBFgnosia)
instacron:SBFGNOSIA
instname_str Sociedade Brasileira de Farmacognosia (SBFgnosia)
instacron_str SBFGNOSIA
institution SBFGNOSIA
reponame_str Revista Brasileira de Farmacognosia (Online)
collection Revista Brasileira de Farmacognosia (Online)
repository.name.fl_str_mv Revista Brasileira de Farmacognosia (Online) - Sociedade Brasileira de Farmacognosia (SBFgnosia)
repository.mail.fl_str_mv rbgnosia@ltf.ufpb.br
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