Ultrasonic Extracts of Morinda citrifolia L.: Characterization of Volatile Compounds by Gas Chromatography-Mass Spectrometry

Detalhes bibliográficos
Autor(a) principal: Lima,Daiane B. M.
Data de Publicação: 2019
Outros Autores: Santos,Anaí L. dos, Celestino,Ariel O., Sampaio,Nayna, Baldez,Jéssica, Melecchi,Maria I. S., Bjerk,Thiago R., Krause,Laíza C., Caramão,Elina B.
Tipo de documento: Artigo
Idioma: eng
Título da fonte: Journal of the Brazilian Chemical Society (Online)
Texto Completo: http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532019000100132
Resumo: Morinda citrifolia (noni) is found in the Atlantic and Amazonian Forest in Brazil and with recognized uses in folk medicine. However, few studies exist in its chemical characterization. The present work aims to investigate the efficiency of the sonication for extracting bioactive compounds from fruits and leaves of noni, using an experimental design of 23, whose variables were time, temperature and mass of the plant. Parallel extractions were performed using two extraction solvents (hexane and ethanol) and the same experimental design. The compounds were identified by gas chromatography coupled to mass spectrometry. The independent variable was the mass yield and all the variables studied in the sonication process were significant (p < 0.05%) for the process. Ethanol was more effective than hexane and the leaves produced higher yield and diversity of compounds than fruits. Vitamin E (tocopherol), octanoic acid, hydroxymethylfurfural, phytol and squalene were the main compounds identified.
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spelling Ultrasonic Extracts of Morinda citrifolia L.: Characterization of Volatile Compounds by Gas Chromatography-Mass SpectrometryMorinda citrifolia L.sonicationgas chromatographyGC-MStocopherolsMorinda citrifolia (noni) is found in the Atlantic and Amazonian Forest in Brazil and with recognized uses in folk medicine. However, few studies exist in its chemical characterization. The present work aims to investigate the efficiency of the sonication for extracting bioactive compounds from fruits and leaves of noni, using an experimental design of 23, whose variables were time, temperature and mass of the plant. Parallel extractions were performed using two extraction solvents (hexane and ethanol) and the same experimental design. The compounds were identified by gas chromatography coupled to mass spectrometry. The independent variable was the mass yield and all the variables studied in the sonication process were significant (p < 0.05%) for the process. Ethanol was more effective than hexane and the leaves produced higher yield and diversity of compounds than fruits. Vitamin E (tocopherol), octanoic acid, hydroxymethylfurfural, phytol and squalene were the main compounds identified.Sociedade Brasileira de Química2019-01-01info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersiontext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532019000100132Journal of the Brazilian Chemical Society v.30 n.1 2019reponame:Journal of the Brazilian Chemical Society (Online)instname:Sociedade Brasileira de Química (SBQ)instacron:SBQ10.21577/0103-5053.20180162info:eu-repo/semantics/openAccessLima,Daiane B. M.Santos,Anaí L. dosCelestino,Ariel O.Sampaio,NaynaBaldez,JéssicaMelecchi,Maria I. S.Bjerk,Thiago R.Krause,Laíza C.Caramão,Elina B.eng2019-01-07T00:00:00Zoai:scielo:S0103-50532019000100132Revistahttp://jbcs.sbq.org.brONGhttps://old.scielo.br/oai/scielo-oai.php||office@jbcs.sbq.org.br1678-47900103-5053opendoar:2019-01-07T00:00Journal of the Brazilian Chemical Society (Online) - Sociedade Brasileira de Química (SBQ)false
dc.title.none.fl_str_mv Ultrasonic Extracts of Morinda citrifolia L.: Characterization of Volatile Compounds by Gas Chromatography-Mass Spectrometry
title Ultrasonic Extracts of Morinda citrifolia L.: Characterization of Volatile Compounds by Gas Chromatography-Mass Spectrometry
spellingShingle Ultrasonic Extracts of Morinda citrifolia L.: Characterization of Volatile Compounds by Gas Chromatography-Mass Spectrometry
Lima,Daiane B. M.
Morinda citrifolia L.
sonication
gas chromatography
GC-MS
tocopherols
title_short Ultrasonic Extracts of Morinda citrifolia L.: Characterization of Volatile Compounds by Gas Chromatography-Mass Spectrometry
title_full Ultrasonic Extracts of Morinda citrifolia L.: Characterization of Volatile Compounds by Gas Chromatography-Mass Spectrometry
title_fullStr Ultrasonic Extracts of Morinda citrifolia L.: Characterization of Volatile Compounds by Gas Chromatography-Mass Spectrometry
title_full_unstemmed Ultrasonic Extracts of Morinda citrifolia L.: Characterization of Volatile Compounds by Gas Chromatography-Mass Spectrometry
title_sort Ultrasonic Extracts of Morinda citrifolia L.: Characterization of Volatile Compounds by Gas Chromatography-Mass Spectrometry
author Lima,Daiane B. M.
author_facet Lima,Daiane B. M.
Santos,Anaí L. dos
Celestino,Ariel O.
Sampaio,Nayna
Baldez,Jéssica
Melecchi,Maria I. S.
Bjerk,Thiago R.
Krause,Laíza C.
Caramão,Elina B.
author_role author
author2 Santos,Anaí L. dos
Celestino,Ariel O.
Sampaio,Nayna
Baldez,Jéssica
Melecchi,Maria I. S.
Bjerk,Thiago R.
Krause,Laíza C.
Caramão,Elina B.
author2_role author
author
author
author
author
author
author
author
dc.contributor.author.fl_str_mv Lima,Daiane B. M.
Santos,Anaí L. dos
Celestino,Ariel O.
Sampaio,Nayna
Baldez,Jéssica
Melecchi,Maria I. S.
Bjerk,Thiago R.
Krause,Laíza C.
Caramão,Elina B.
dc.subject.por.fl_str_mv Morinda citrifolia L.
sonication
gas chromatography
GC-MS
tocopherols
topic Morinda citrifolia L.
sonication
gas chromatography
GC-MS
tocopherols
description Morinda citrifolia (noni) is found in the Atlantic and Amazonian Forest in Brazil and with recognized uses in folk medicine. However, few studies exist in its chemical characterization. The present work aims to investigate the efficiency of the sonication for extracting bioactive compounds from fruits and leaves of noni, using an experimental design of 23, whose variables were time, temperature and mass of the plant. Parallel extractions were performed using two extraction solvents (hexane and ethanol) and the same experimental design. The compounds were identified by gas chromatography coupled to mass spectrometry. The independent variable was the mass yield and all the variables studied in the sonication process were significant (p < 0.05%) for the process. Ethanol was more effective than hexane and the leaves produced higher yield and diversity of compounds than fruits. Vitamin E (tocopherol), octanoic acid, hydroxymethylfurfural, phytol and squalene were the main compounds identified.
publishDate 2019
dc.date.none.fl_str_mv 2019-01-01
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
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dc.identifier.uri.fl_str_mv http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532019000100132
url http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532019000100132
dc.language.iso.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv 10.21577/0103-5053.20180162
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
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dc.format.none.fl_str_mv text/html
dc.publisher.none.fl_str_mv Sociedade Brasileira de Química
publisher.none.fl_str_mv Sociedade Brasileira de Química
dc.source.none.fl_str_mv Journal of the Brazilian Chemical Society v.30 n.1 2019
reponame:Journal of the Brazilian Chemical Society (Online)
instname:Sociedade Brasileira de Química (SBQ)
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reponame_str Journal of the Brazilian Chemical Society (Online)
collection Journal of the Brazilian Chemical Society (Online)
repository.name.fl_str_mv Journal of the Brazilian Chemical Society (Online) - Sociedade Brasileira de Química (SBQ)
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