Ultrasonic Extracts of Morinda citrifolia L.: Characterization of Volatile Compounds by Gas Chromatography-Mass Spectrometry
Autor(a) principal: | |
---|---|
Data de Publicação: | 2019 |
Outros Autores: | , , , , , , , |
Tipo de documento: | Artigo |
Idioma: | eng |
Título da fonte: | Journal of the Brazilian Chemical Society (Online) |
Texto Completo: | http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532019000100132 |
Resumo: | Morinda citrifolia (noni) is found in the Atlantic and Amazonian Forest in Brazil and with recognized uses in folk medicine. However, few studies exist in its chemical characterization. The present work aims to investigate the efficiency of the sonication for extracting bioactive compounds from fruits and leaves of noni, using an experimental design of 23, whose variables were time, temperature and mass of the plant. Parallel extractions were performed using two extraction solvents (hexane and ethanol) and the same experimental design. The compounds were identified by gas chromatography coupled to mass spectrometry. The independent variable was the mass yield and all the variables studied in the sonication process were significant (p < 0.05%) for the process. Ethanol was more effective than hexane and the leaves produced higher yield and diversity of compounds than fruits. Vitamin E (tocopherol), octanoic acid, hydroxymethylfurfural, phytol and squalene were the main compounds identified. |
id |
SBQ-2_4c427f2f13a0eea019080eb796544824 |
---|---|
oai_identifier_str |
oai:scielo:S0103-50532019000100132 |
network_acronym_str |
SBQ-2 |
network_name_str |
Journal of the Brazilian Chemical Society (Online) |
repository_id_str |
|
spelling |
Ultrasonic Extracts of Morinda citrifolia L.: Characterization of Volatile Compounds by Gas Chromatography-Mass SpectrometryMorinda citrifolia L.sonicationgas chromatographyGC-MStocopherolsMorinda citrifolia (noni) is found in the Atlantic and Amazonian Forest in Brazil and with recognized uses in folk medicine. However, few studies exist in its chemical characterization. The present work aims to investigate the efficiency of the sonication for extracting bioactive compounds from fruits and leaves of noni, using an experimental design of 23, whose variables were time, temperature and mass of the plant. Parallel extractions were performed using two extraction solvents (hexane and ethanol) and the same experimental design. The compounds were identified by gas chromatography coupled to mass spectrometry. The independent variable was the mass yield and all the variables studied in the sonication process were significant (p < 0.05%) for the process. Ethanol was more effective than hexane and the leaves produced higher yield and diversity of compounds than fruits. Vitamin E (tocopherol), octanoic acid, hydroxymethylfurfural, phytol and squalene were the main compounds identified.Sociedade Brasileira de Química2019-01-01info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersiontext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532019000100132Journal of the Brazilian Chemical Society v.30 n.1 2019reponame:Journal of the Brazilian Chemical Society (Online)instname:Sociedade Brasileira de Química (SBQ)instacron:SBQ10.21577/0103-5053.20180162info:eu-repo/semantics/openAccessLima,Daiane B. M.Santos,Anaí L. dosCelestino,Ariel O.Sampaio,NaynaBaldez,JéssicaMelecchi,Maria I. S.Bjerk,Thiago R.Krause,Laíza C.Caramão,Elina B.eng2019-01-07T00:00:00Zoai:scielo:S0103-50532019000100132Revistahttp://jbcs.sbq.org.brONGhttps://old.scielo.br/oai/scielo-oai.php||office@jbcs.sbq.org.br1678-47900103-5053opendoar:2019-01-07T00:00Journal of the Brazilian Chemical Society (Online) - Sociedade Brasileira de Química (SBQ)false |
dc.title.none.fl_str_mv |
Ultrasonic Extracts of Morinda citrifolia L.: Characterization of Volatile Compounds by Gas Chromatography-Mass Spectrometry |
title |
Ultrasonic Extracts of Morinda citrifolia L.: Characterization of Volatile Compounds by Gas Chromatography-Mass Spectrometry |
spellingShingle |
Ultrasonic Extracts of Morinda citrifolia L.: Characterization of Volatile Compounds by Gas Chromatography-Mass Spectrometry Lima,Daiane B. M. Morinda citrifolia L. sonication gas chromatography GC-MS tocopherols |
title_short |
Ultrasonic Extracts of Morinda citrifolia L.: Characterization of Volatile Compounds by Gas Chromatography-Mass Spectrometry |
title_full |
Ultrasonic Extracts of Morinda citrifolia L.: Characterization of Volatile Compounds by Gas Chromatography-Mass Spectrometry |
title_fullStr |
Ultrasonic Extracts of Morinda citrifolia L.: Characterization of Volatile Compounds by Gas Chromatography-Mass Spectrometry |
title_full_unstemmed |
Ultrasonic Extracts of Morinda citrifolia L.: Characterization of Volatile Compounds by Gas Chromatography-Mass Spectrometry |
title_sort |
Ultrasonic Extracts of Morinda citrifolia L.: Characterization of Volatile Compounds by Gas Chromatography-Mass Spectrometry |
author |
Lima,Daiane B. M. |
author_facet |
Lima,Daiane B. M. Santos,Anaí L. dos Celestino,Ariel O. Sampaio,Nayna Baldez,Jéssica Melecchi,Maria I. S. Bjerk,Thiago R. Krause,Laíza C. Caramão,Elina B. |
author_role |
author |
author2 |
Santos,Anaí L. dos Celestino,Ariel O. Sampaio,Nayna Baldez,Jéssica Melecchi,Maria I. S. Bjerk,Thiago R. Krause,Laíza C. Caramão,Elina B. |
author2_role |
author author author author author author author author |
dc.contributor.author.fl_str_mv |
Lima,Daiane B. M. Santos,Anaí L. dos Celestino,Ariel O. Sampaio,Nayna Baldez,Jéssica Melecchi,Maria I. S. Bjerk,Thiago R. Krause,Laíza C. Caramão,Elina B. |
dc.subject.por.fl_str_mv |
Morinda citrifolia L. sonication gas chromatography GC-MS tocopherols |
topic |
Morinda citrifolia L. sonication gas chromatography GC-MS tocopherols |
description |
Morinda citrifolia (noni) is found in the Atlantic and Amazonian Forest in Brazil and with recognized uses in folk medicine. However, few studies exist in its chemical characterization. The present work aims to investigate the efficiency of the sonication for extracting bioactive compounds from fruits and leaves of noni, using an experimental design of 23, whose variables were time, temperature and mass of the plant. Parallel extractions were performed using two extraction solvents (hexane and ethanol) and the same experimental design. The compounds were identified by gas chromatography coupled to mass spectrometry. The independent variable was the mass yield and all the variables studied in the sonication process were significant (p < 0.05%) for the process. Ethanol was more effective than hexane and the leaves produced higher yield and diversity of compounds than fruits. Vitamin E (tocopherol), octanoic acid, hydroxymethylfurfural, phytol and squalene were the main compounds identified. |
publishDate |
2019 |
dc.date.none.fl_str_mv |
2019-01-01 |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532019000100132 |
url |
http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532019000100132 |
dc.language.iso.fl_str_mv |
eng |
language |
eng |
dc.relation.none.fl_str_mv |
10.21577/0103-5053.20180162 |
dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess |
eu_rights_str_mv |
openAccess |
dc.format.none.fl_str_mv |
text/html |
dc.publisher.none.fl_str_mv |
Sociedade Brasileira de Química |
publisher.none.fl_str_mv |
Sociedade Brasileira de Química |
dc.source.none.fl_str_mv |
Journal of the Brazilian Chemical Society v.30 n.1 2019 reponame:Journal of the Brazilian Chemical Society (Online) instname:Sociedade Brasileira de Química (SBQ) instacron:SBQ |
instname_str |
Sociedade Brasileira de Química (SBQ) |
instacron_str |
SBQ |
institution |
SBQ |
reponame_str |
Journal of the Brazilian Chemical Society (Online) |
collection |
Journal of the Brazilian Chemical Society (Online) |
repository.name.fl_str_mv |
Journal of the Brazilian Chemical Society (Online) - Sociedade Brasileira de Química (SBQ) |
repository.mail.fl_str_mv |
||office@jbcs.sbq.org.br |
_version_ |
1750318181321277440 |