Synthesis and characterization of polyesters derived from glycerol and phthalic acid

Detalhes bibliográficos
Autor(a) principal: Guimarães, Danilo Hansen
Data de Publicação: 2007
Outros Autores: Brioude, Michel de Meireles, Fiuza, Raigenis da Paz, Prado, Luis Antônio Sanches de Almeida, Boaventura Filho, Jaime Soares, José, Nadia Mamede
Tipo de documento: Artigo
Idioma: eng
Título da fonte: Repositório Institucional da UFBA
Texto Completo: http://www.repositorio.ufba.br/ri/handle/ri/4915
Resumo: p. 257-260,July/Sept.
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spelling Guimarães, Danilo HansenBrioude, Michel de MeirelesFiuza, Raigenis da PazPrado, Luis Antônio Sanches de AlmeidaBoaventura Filho, Jaime SoaresJosé, Nadia MamedeGuimarães, Danilo HansenBrioude, Michel de MeirelesFiuza, Raigenis da PazPrado, Luis Antônio Sanches de AlmeidaBoaventura Filho, Jaime SoaresJosé, Nadia Mamede2011-12-20T10:03:35Z2011-12-20T10:03:35Z20071516-1439http://www.repositorio.ufba.br/ri/handle/ri/4915v. 10, n. 3.p. 257-260,July/Sept.The production of polyester via polycondensation between glycerol and phthalic acid using dibutyltin dilaurate is reported. Three glycerol:phthalic acid molar ratio used for the bulk polymerization were: 2:2; 2:3 and 2:4. FTIR confirmed the esterification of glycerol by the acid for all the polymers. DSC indicated no crystallinity, although the XRD plots indicate a very incipient crystallinity for the polymers containing higher amounts of phthalic anhydride. Scanning electron microscopy results indicates high homogeneity for all the polymers prepared.Submitted by JURANDI DE SOUZA SILVA (jssufba@hotmail.com) on 2011-12-20T10:03:35Z No. of bitstreams: 1 05.pdf: 711963 bytes, checksum: 73eb42841b8499fb0b83e8ddf43f1785 (MD5)Made available in DSpace on 2011-12-20T10:03:35Z (GMT). No. of bitstreams: 1 05.pdf: 711963 bytes, checksum: 73eb42841b8499fb0b83e8ddf43f1785 (MD5) Previous issue date: 2007São Carloshttp://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392007000300007&lng=en&nrm=isoreponame:Repositório Institucional da UFBAinstname:Universidade Federal da Bahia (UFBA)instacron:UFBAPolyesterGlycerolPhthalic acidSynthesis and characterization of polyesters derived from glycerol and phthalic acidMaterials Researchinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/articleenginfo:eu-repo/semantics/openAccessORIGINAL05.pdf05.pdfapplication/pdf711963https://repositorio.ufba.br/bitstream/ri/4915/1/05.pdf73eb42841b8499fb0b83e8ddf43f1785MD51LICENSElicense.txtlicense.txttext/plain1809https://repositorio.ufba.br/bitstream/ri/4915/2/license.txt8bb3e3eb871f5854a9ec419f68651b60MD52TEXT05.pdf.txt05.pdf.txtExtracted texttext/plain18200https://repositorio.ufba.br/bitstream/ri/4915/3/05.pdf.txt6fb48763e0742cdc3b3b7bdb1fa78e62MD53ri/49152022-07-05 14:03:20.583oai:repositorio.ufba.br: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ório InstitucionalPUBhttp://192.188.11.11:8080/oai/requestopendoar:19322022-07-05T17:03:20Repositório Institucional da UFBA - Universidade Federal da Bahia (UFBA)false
dc.title.pt_BR.fl_str_mv Synthesis and characterization of polyesters derived from glycerol and phthalic acid
dc.title.alternative.pt_BR.fl_str_mv Materials Research
title Synthesis and characterization of polyesters derived from glycerol and phthalic acid
spellingShingle Synthesis and characterization of polyesters derived from glycerol and phthalic acid
Guimarães, Danilo Hansen
Polyester
Glycerol
Phthalic acid
title_short Synthesis and characterization of polyesters derived from glycerol and phthalic acid
title_full Synthesis and characterization of polyesters derived from glycerol and phthalic acid
title_fullStr Synthesis and characterization of polyesters derived from glycerol and phthalic acid
title_full_unstemmed Synthesis and characterization of polyesters derived from glycerol and phthalic acid
title_sort Synthesis and characterization of polyesters derived from glycerol and phthalic acid
author Guimarães, Danilo Hansen
author_facet Guimarães, Danilo Hansen
Brioude, Michel de Meireles
Fiuza, Raigenis da Paz
Prado, Luis Antônio Sanches de Almeida
Boaventura Filho, Jaime Soares
José, Nadia Mamede
author_role author
author2 Brioude, Michel de Meireles
Fiuza, Raigenis da Paz
Prado, Luis Antônio Sanches de Almeida
Boaventura Filho, Jaime Soares
José, Nadia Mamede
author2_role author
author
author
author
author
dc.contributor.author.fl_str_mv Guimarães, Danilo Hansen
Brioude, Michel de Meireles
Fiuza, Raigenis da Paz
Prado, Luis Antônio Sanches de Almeida
Boaventura Filho, Jaime Soares
José, Nadia Mamede
Guimarães, Danilo Hansen
Brioude, Michel de Meireles
Fiuza, Raigenis da Paz
Prado, Luis Antônio Sanches de Almeida
Boaventura Filho, Jaime Soares
José, Nadia Mamede
dc.subject.por.fl_str_mv Polyester
Glycerol
Phthalic acid
topic Polyester
Glycerol
Phthalic acid
description p. 257-260,July/Sept.
publishDate 2007
dc.date.issued.fl_str_mv 2007
dc.date.accessioned.fl_str_mv 2011-12-20T10:03:35Z
dc.date.available.fl_str_mv 2011-12-20T10:03:35Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv http://www.repositorio.ufba.br/ri/handle/ri/4915
dc.identifier.issn.none.fl_str_mv 1516-1439
dc.identifier.number.pt_BR.fl_str_mv v. 10, n. 3.
identifier_str_mv 1516-1439
v. 10, n. 3.
url http://www.repositorio.ufba.br/ri/handle/ri/4915
dc.language.iso.fl_str_mv eng
language eng
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
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