Optimization of the extraction process of compounds with antioxidant activity of tommy atkins mango peel

Detalhes bibliográficos
Autor(a) principal: Veloso , Felipe da Silva
Data de Publicação: 2020
Outros Autores: Colla, Eliane, Genena, Aziza Kamal
Tipo de documento: Artigo
Idioma: eng
Título da fonte: Research, Society and Development
Texto Completo: https://rsdjournal.org/index.php/rsd/article/view/9273
Resumo: It is well known that vegetable residues from the food industry can be used as a possible source for the extraction of compounds with antioxidant activity; in the case of mango, approximately 40 to 60% of the total mass of the fruit is considered as residue after processing. This work focused on the optimization of the extraction process of compounds with antioxidant activity from the rind of Tommy Atkins mango. Initially a Fractional Factorial Design 25-1 (FFD) was applied to study the effect of five variables on the extraction process, namely: extraction time (min), percentage of ethanol in aqueous solution (%), pH, dry/solvent mango peel ratio (g/mL) and ultrasound power range (%). The variables extraction time and dry/solvent mango peel ratio were selected, which were evaluated sequentially by the application of a Central Composite Rotatable Design (CCRD) to determine the conditions of maximum extraction of antioxidant compounds by the response surface analysis. The ABTS•+ and Folin-Ciocalteu methods were used for the quantification of the antioxidant activity.  The maximum extraction occurred with the use of water, extraction time of 30 min, dry mango peel/solvent ratio of g/mL (1:100), at natural pH of the mixture (pH 4.6 ± 0.20) and sonication amplitude at 50%. It was possible to develop an extraction process of compounds with antioxidant activity from the mango peel, in order to maximize yield through the use of non-toxic solvents and using an agro-industrial residue as raw material.
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spelling Optimization of the extraction process of compounds with antioxidant activity of tommy atkins mango peelOptimización del proceso de extracción de compuestos con actividad antioxidante de la cáscara de mango tommy atkinsOtimização do processo de extração de compostos com atividade antioxidante da casca de manga tommy atkinsTommy AtkinsPotencial antioxidanteEstrategia secuencial de diseño experimental.Tommy AtkinsPotencial antioxidanteEstratégia sequencial de planejamento experimental.Tommy AtkinsAntioxidant potentialSequential experimental planning strategy.It is well known that vegetable residues from the food industry can be used as a possible source for the extraction of compounds with antioxidant activity; in the case of mango, approximately 40 to 60% of the total mass of the fruit is considered as residue after processing. This work focused on the optimization of the extraction process of compounds with antioxidant activity from the rind of Tommy Atkins mango. Initially a Fractional Factorial Design 25-1 (FFD) was applied to study the effect of five variables on the extraction process, namely: extraction time (min), percentage of ethanol in aqueous solution (%), pH, dry/solvent mango peel ratio (g/mL) and ultrasound power range (%). The variables extraction time and dry/solvent mango peel ratio were selected, which were evaluated sequentially by the application of a Central Composite Rotatable Design (CCRD) to determine the conditions of maximum extraction of antioxidant compounds by the response surface analysis. The ABTS•+ and Folin-Ciocalteu methods were used for the quantification of the antioxidant activity.  The maximum extraction occurred with the use of water, extraction time of 30 min, dry mango peel/solvent ratio of g/mL (1:100), at natural pH of the mixture (pH 4.6 ± 0.20) and sonication amplitude at 50%. It was possible to develop an extraction process of compounds with antioxidant activity from the mango peel, in order to maximize yield through the use of non-toxic solvents and using an agro-industrial residue as raw material.Es bien sabido que los residuos vegetales de la industria alimentaria pueden utilizarse como una posible fuente para la extracción de compuestos con actividad antioxidante; en el caso del mango, aproximadamente del 40 al 60% de la masa total de la fruta se considera como residuo después de su procesamiento. Este trabajo se centró en la optimización del proceso de extracción de compuestos con actividad antioxidante de la corteza del mango de Tommy Atkins. Inicialmente, se aplicó un Plan de Factores Fraccionales 25-1 (PFF) para estudiar el efecto de cinco variables en el proceso de extracción, a saber: tiempo de extracción (min), porcentaje de etanol en solución acuosa (%), pH, relación cáscara de mango seca/solvente (g/mL) y rango de potencia de ultrasonido (%). Se seleccionaron las variables tiempo de extracción y relación cáscara de mango seca/solvente, que se evaluaron secuencialmente mediante la aplicación de uno Diseño Compuesto Central Rotacional (DCCR) para determinar las condiciones de máxima extracción de compuestos antioxidantes mediante el análisis de la superficie de respuesta. Se utilizaron los métodos ABTS•+ y Folin-Ciocalteu para la cuantificación de la actividad antioxidante.  La máxima extracción se produjo con el uso de agua, tiempo de extracción de 30 min, relación cáscara de mango seco/solvente de g/mL, a pH natural de la mezcla (pH 4,6 ± 0,20) 50% de rango de potencia del ultrasonido. Fue posible desarrollar un proceso de extracción de compuestos con actividad antioxidante de la cáscara del mango a fin de maximizar el rendimiento mediante el uso de solventes no tóxicos y la utilización de un residuo agroindustrial como materia prima.É notório que os resíduos vegetais oriundos da indústria de alimentos podem ser utilizados como possível fonte para a extração de compostos com atividade antioxidante; no caso da manga, aproximadamente 40 a 60% da massa total da fruta é considerada como resíduo após seu processamento. Este trabalho teve como foco a otimização do processo de extração de compostos com atividade antioxidante da casca da manga Tommy Atkins. Inicialmente foi aplicado um Planejamento Fatorial Fracionário 25-1 (PFF) para o estudo do efeito de cinco variáveis sobre o processo de extração, a citar: tempo de extração (min), porcentagem de etanol em solução aquosa (%), pH, razão casca de manga seca/solvente (g/mL) e amplitude de potência do ultrassom (%). Foram selecionadas as variáveis tempo de extração e razão casca de manga seca/solvente, as quais foram avaliadas sequencialmente pela aplicação de um Delineamento Composto Central Rotacional (DCCR) para determinação das condições de máxima extração de compostos antioxidantes pela análise de superfície de resposta. Para a quantificação da atividade antioxidante utilizou-se o método ABTS•+ e Folin-Ciocalteu.  A máxima extração ocorreu com utilização de água, tempo de extração de 30 min, razão casca de manga seca/solvente de g/mL, no pH natural da mistura (pH 4,6 ± 0,20) amplitude de potência do ultrassom 50%. Foi possível desenvolver um processo de extração de compostos com atividade antioxidante da casca de manga, de forma a se maximizar o rendimento por meio da utilização de solventes não-tóxicos e utilizando um resíduo agroindustrial como matéria-prima.Research, Society and Development2020-10-30info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionapplication/pdfhttps://rsdjournal.org/index.php/rsd/article/view/927310.33448/rsd-v9i10.9273Research, Society and Development; Vol. 9 No. 10; e9939109273Research, Society and Development; Vol. 9 Núm. 10; e9939109273Research, Society and Development; v. 9 n. 10; e99391092732525-3409reponame:Research, Society and Developmentinstname:Universidade Federal de Itajubá (UNIFEI)instacron:UNIFEIenghttps://rsdjournal.org/index.php/rsd/article/view/9273/8450Copyright (c) 2020 Felipe da Silva Veloso ; Eliane Colla; Aziza Kamal Genenahttps://creativecommons.org/licenses/by/4.0info:eu-repo/semantics/openAccessVeloso , Felipe da Silva Colla, ElianeGenena, Aziza Kamal 2020-10-31T12:03:23Zoai:ojs.pkp.sfu.ca:article/9273Revistahttps://rsdjournal.org/index.php/rsd/indexPUBhttps://rsdjournal.org/index.php/rsd/oairsd.articles@gmail.com2525-34092525-3409opendoar:2024-01-17T09:31:36.115336Research, Society and Development - Universidade Federal de Itajubá (UNIFEI)false
dc.title.none.fl_str_mv Optimization of the extraction process of compounds with antioxidant activity of tommy atkins mango peel
Optimización del proceso de extracción de compuestos con actividad antioxidante de la cáscara de mango tommy atkins
Otimização do processo de extração de compostos com atividade antioxidante da casca de manga tommy atkins
title Optimization of the extraction process of compounds with antioxidant activity of tommy atkins mango peel
spellingShingle Optimization of the extraction process of compounds with antioxidant activity of tommy atkins mango peel
Veloso , Felipe da Silva
Tommy Atkins
Potencial antioxidante
Estrategia secuencial de diseño experimental.
Tommy Atkins
Potencial antioxidante
Estratégia sequencial de planejamento experimental.
Tommy Atkins
Antioxidant potential
Sequential experimental planning strategy.
title_short Optimization of the extraction process of compounds with antioxidant activity of tommy atkins mango peel
title_full Optimization of the extraction process of compounds with antioxidant activity of tommy atkins mango peel
title_fullStr Optimization of the extraction process of compounds with antioxidant activity of tommy atkins mango peel
title_full_unstemmed Optimization of the extraction process of compounds with antioxidant activity of tommy atkins mango peel
title_sort Optimization of the extraction process of compounds with antioxidant activity of tommy atkins mango peel
author Veloso , Felipe da Silva
author_facet Veloso , Felipe da Silva
Colla, Eliane
Genena, Aziza Kamal
author_role author
author2 Colla, Eliane
Genena, Aziza Kamal
author2_role author
author
dc.contributor.author.fl_str_mv Veloso , Felipe da Silva
Colla, Eliane
Genena, Aziza Kamal
dc.subject.por.fl_str_mv Tommy Atkins
Potencial antioxidante
Estrategia secuencial de diseño experimental.
Tommy Atkins
Potencial antioxidante
Estratégia sequencial de planejamento experimental.
Tommy Atkins
Antioxidant potential
Sequential experimental planning strategy.
topic Tommy Atkins
Potencial antioxidante
Estrategia secuencial de diseño experimental.
Tommy Atkins
Potencial antioxidante
Estratégia sequencial de planejamento experimental.
Tommy Atkins
Antioxidant potential
Sequential experimental planning strategy.
description It is well known that vegetable residues from the food industry can be used as a possible source for the extraction of compounds with antioxidant activity; in the case of mango, approximately 40 to 60% of the total mass of the fruit is considered as residue after processing. This work focused on the optimization of the extraction process of compounds with antioxidant activity from the rind of Tommy Atkins mango. Initially a Fractional Factorial Design 25-1 (FFD) was applied to study the effect of five variables on the extraction process, namely: extraction time (min), percentage of ethanol in aqueous solution (%), pH, dry/solvent mango peel ratio (g/mL) and ultrasound power range (%). The variables extraction time and dry/solvent mango peel ratio were selected, which were evaluated sequentially by the application of a Central Composite Rotatable Design (CCRD) to determine the conditions of maximum extraction of antioxidant compounds by the response surface analysis. The ABTS•+ and Folin-Ciocalteu methods were used for the quantification of the antioxidant activity.  The maximum extraction occurred with the use of water, extraction time of 30 min, dry mango peel/solvent ratio of g/mL (1:100), at natural pH of the mixture (pH 4.6 ± 0.20) and sonication amplitude at 50%. It was possible to develop an extraction process of compounds with antioxidant activity from the mango peel, in order to maximize yield through the use of non-toxic solvents and using an agro-industrial residue as raw material.
publishDate 2020
dc.date.none.fl_str_mv 2020-10-30
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv https://rsdjournal.org/index.php/rsd/article/view/9273
10.33448/rsd-v9i10.9273
url https://rsdjournal.org/index.php/rsd/article/view/9273
identifier_str_mv 10.33448/rsd-v9i10.9273
dc.language.iso.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv https://rsdjournal.org/index.php/rsd/article/view/9273/8450
dc.rights.driver.fl_str_mv Copyright (c) 2020 Felipe da Silva Veloso ; Eliane Colla; Aziza Kamal Genena
https://creativecommons.org/licenses/by/4.0
info:eu-repo/semantics/openAccess
rights_invalid_str_mv Copyright (c) 2020 Felipe da Silva Veloso ; Eliane Colla; Aziza Kamal Genena
https://creativecommons.org/licenses/by/4.0
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv application/pdf
dc.publisher.none.fl_str_mv Research, Society and Development
publisher.none.fl_str_mv Research, Society and Development
dc.source.none.fl_str_mv Research, Society and Development; Vol. 9 No. 10; e9939109273
Research, Society and Development; Vol. 9 Núm. 10; e9939109273
Research, Society and Development; v. 9 n. 10; e9939109273
2525-3409
reponame:Research, Society and Development
instname:Universidade Federal de Itajubá (UNIFEI)
instacron:UNIFEI
instname_str Universidade Federal de Itajubá (UNIFEI)
instacron_str UNIFEI
institution UNIFEI
reponame_str Research, Society and Development
collection Research, Society and Development
repository.name.fl_str_mv Research, Society and Development - Universidade Federal de Itajubá (UNIFEI)
repository.mail.fl_str_mv rsd.articles@gmail.com
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