Surface study of vitreous carbon obtained from glassy carbon powder

• Autor(a) principal: Dondeo, F.
• Data de Publicação: 2012
• Outros Autores: Damiao, A. J., Miyakawa, W., Nascimento, F., Fernandes, L., Oishi, S. [UNESP], Botelho, E. [UNESP]
• Tipo de documento: Artigo de conferência
• Idioma: eng
• Título da fonte: Repositório Institucional da UNESP
• Texto Completo: http://dx.doi.org/10.1557/opl.2012.291; http://hdl.handle.net/11449/73334
• topic: Granulometries; Height variation; Hydraulic press; Nanometrics; Nitrogen atmospheres; Production methods; Surface study; Vitreous carbon; Atomic force microscopy; Ball mills; Carbonization; Hydraulic machinery; Surface roughness; Glassy carbon

This work presents a surface study of monolithic vitreous (or glassy) carbon - MVC - obtained from vitreous carbon powder. Defective MVC pieces are crushed in a ball mill and size classified by sifting. The MVC powder is mixed with furfuryl-alcohol resin and compacted in a mould using a hydraulic press. Samples with different powder granulometries are produced in this way and carbonized in a furnace under nitrogen atmosphere. Complete carbonization of the powder is achieved in only one day and losses due to breakage of the pieces is less than 5%. These results compare very favorably with respect to traditional MVC production methods where full carbonization may require up to seven days and losses due to breakage can be as high as 70%. After carbonization, samples are sanded and polished. Surface roughness and microstructure are characterized by light microscopy. Porosity is quantified from micrographs using ImageJ software and nanometric height variations are measured by atomic force microscopy. © 2012 Materials Research Society.