The production of hydroxyapatite prototypes from solid bodies of gypsum/polyvinyl alcohol composites

Detalhes bibliográficos
Autor(a) principal: Barbosa,Amanda Alves
Data de Publicação: 2014
Outros Autores: Ferraz,Andréa de Vasconcelos, Dantas,Alan Christie, Olivier,Nelson Cárdenas
Tipo de documento: Artigo
Idioma: eng
Título da fonte: Materials research (São Carlos. Online)
Texto Completo: http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392014000700008
Resumo: Prototypes of porous hydroxyapatite (HAp) were produced from Gypsum/PVA composite, using a mass proportion of 15% polymer. The material was obtained by means of chemical conversion in (NH4)2HPO4 0.5 mol.L-1 solution and NH4OH 6.0 mol.L-1 alkaline medium for pH control, maintained between 6.0 and 9.0. The reaction occurred at a temperature of 100ºC at different test times. The obtained HAp was characterized by several techniques, such as FTIR, which identified the SO4(2-) groups characteristic for the Gypsum block, and the PO4(3-) groups that are attributed to the biomaterial HAp, besides XRD and SEM, which made it possible to confirm a successful conversion of the material. Tests for mechanical resistance to compression (σc) were carried out for both materials as well.
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spelling The production of hydroxyapatite prototypes from solid bodies of gypsum/polyvinyl alcohol compositeshydroxyapatitegypsumPVAprototypesPrototypes of porous hydroxyapatite (HAp) were produced from Gypsum/PVA composite, using a mass proportion of 15% polymer. The material was obtained by means of chemical conversion in (NH4)2HPO4 0.5 mol.L-1 solution and NH4OH 6.0 mol.L-1 alkaline medium for pH control, maintained between 6.0 and 9.0. The reaction occurred at a temperature of 100ºC at different test times. The obtained HAp was characterized by several techniques, such as FTIR, which identified the SO4(2-) groups characteristic for the Gypsum block, and the PO4(3-) groups that are attributed to the biomaterial HAp, besides XRD and SEM, which made it possible to confirm a successful conversion of the material. Tests for mechanical resistance to compression (σc) were carried out for both materials as well.ABM, ABC, ABPol2014-08-01info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersiontext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392014000700008Materials Research v.17 suppl.1 2014reponame:Materials research (São Carlos. Online)instname:Universidade Federal de São Carlos (UFSCAR)instacron:ABM ABC ABPOL10.1590/S1516-14392014005000062info:eu-repo/semantics/openAccessBarbosa,Amanda AlvesFerraz,Andréa de VasconcelosDantas,Alan ChristieOlivier,Nelson Cárdenaseng2015-11-06T00:00:00Zoai:scielo:S1516-14392014000700008Revistahttp://www.scielo.br/mrPUBhttps://old.scielo.br/oai/scielo-oai.phpdedz@power.ufscar.br1980-53731516-1439opendoar:2015-11-06T00:00Materials research (São Carlos. Online) - Universidade Federal de São Carlos (UFSCAR)false
dc.title.none.fl_str_mv The production of hydroxyapatite prototypes from solid bodies of gypsum/polyvinyl alcohol composites
title The production of hydroxyapatite prototypes from solid bodies of gypsum/polyvinyl alcohol composites
spellingShingle The production of hydroxyapatite prototypes from solid bodies of gypsum/polyvinyl alcohol composites
Barbosa,Amanda Alves
hydroxyapatite
gypsum
PVA
prototypes
title_short The production of hydroxyapatite prototypes from solid bodies of gypsum/polyvinyl alcohol composites
title_full The production of hydroxyapatite prototypes from solid bodies of gypsum/polyvinyl alcohol composites
title_fullStr The production of hydroxyapatite prototypes from solid bodies of gypsum/polyvinyl alcohol composites
title_full_unstemmed The production of hydroxyapatite prototypes from solid bodies of gypsum/polyvinyl alcohol composites
title_sort The production of hydroxyapatite prototypes from solid bodies of gypsum/polyvinyl alcohol composites
author Barbosa,Amanda Alves
author_facet Barbosa,Amanda Alves
Ferraz,Andréa de Vasconcelos
Dantas,Alan Christie
Olivier,Nelson Cárdenas
author_role author
author2 Ferraz,Andréa de Vasconcelos
Dantas,Alan Christie
Olivier,Nelson Cárdenas
author2_role author
author
author
dc.contributor.author.fl_str_mv Barbosa,Amanda Alves
Ferraz,Andréa de Vasconcelos
Dantas,Alan Christie
Olivier,Nelson Cárdenas
dc.subject.por.fl_str_mv hydroxyapatite
gypsum
PVA
prototypes
topic hydroxyapatite
gypsum
PVA
prototypes
description Prototypes of porous hydroxyapatite (HAp) were produced from Gypsum/PVA composite, using a mass proportion of 15% polymer. The material was obtained by means of chemical conversion in (NH4)2HPO4 0.5 mol.L-1 solution and NH4OH 6.0 mol.L-1 alkaline medium for pH control, maintained between 6.0 and 9.0. The reaction occurred at a temperature of 100ºC at different test times. The obtained HAp was characterized by several techniques, such as FTIR, which identified the SO4(2-) groups characteristic for the Gypsum block, and the PO4(3-) groups that are attributed to the biomaterial HAp, besides XRD and SEM, which made it possible to confirm a successful conversion of the material. Tests for mechanical resistance to compression (σc) were carried out for both materials as well.
publishDate 2014
dc.date.none.fl_str_mv 2014-08-01
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392014000700008
url http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392014000700008
dc.language.iso.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv 10.1590/S1516-14392014005000062
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv text/html
dc.publisher.none.fl_str_mv ABM, ABC, ABPol
publisher.none.fl_str_mv ABM, ABC, ABPol
dc.source.none.fl_str_mv Materials Research v.17 suppl.1 2014
reponame:Materials research (São Carlos. Online)
instname:Universidade Federal de São Carlos (UFSCAR)
instacron:ABM ABC ABPOL
instname_str Universidade Federal de São Carlos (UFSCAR)
instacron_str ABM ABC ABPOL
institution ABM ABC ABPOL
reponame_str Materials research (São Carlos. Online)
collection Materials research (São Carlos. Online)
repository.name.fl_str_mv Materials research (São Carlos. Online) - Universidade Federal de São Carlos (UFSCAR)
repository.mail.fl_str_mv dedz@power.ufscar.br
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