Co-precipitation synthesis of (Zn-Mn)-co-doped magnetite nanoparticles and their application in magnetic hyperthermia
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Data de Publicação: | 2019 |
Outros Autores: | , |
Tipo de documento: | Artigo |
Título da fonte: | Repositório da Produção Científica e Intelectual da Unicamp |
Texto Completo: | https://hdl.handle.net/20.500.12733/1670943 |
Resumo: | Agradecimentos: We gratefully acknowledge CAPES, CNPq, FAPESP, and INOMAT for the financial support, Brazilian Nanotechnology National Laboratory for HR-TEM measurements performed in a JEOL JEM-2100 microscope and Prof. Fanny Béron from IFGW-UNICAMP for magnetic measurements |
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Co-precipitation synthesis of (Zn-Mn)-co-doped magnetite nanoparticles and their application in magnetic hyperthermiaFerritaFebreMedições magnéticasFerriteFeverMagnetic measurementsOxide materialsPrecipitationArtigo originalAgradecimentos: We gratefully acknowledge CAPES, CNPq, FAPESP, and INOMAT for the financial support, Brazilian Nanotechnology National Laboratory for HR-TEM measurements performed in a JEOL JEM-2100 microscope and Prof. Fanny Béron from IFGW-UNICAMP for magnetic measurementsAbstract: In this work, a series of zinc- and manganese-co-doped magnetite nanoparticles was synthesized by co-precipitation method and their magnetization and magnetic hyperthermia properties were evaluated according to the degree of doping. The syntheses of the magnetic nanoparticles were carried out in the presence of polyethyleneglycol (PEG) at 353?K using aqueous medium. Several samples was synthesized with nominal composition of (ZnxMn1-xFe0.6)Fe2O4, x = (0-0.4). All samples were characterized by XRD and pure spinel structure like was observed, having about 13?nm diameter and truncated octahedral morphology. The magnetometry measures showed that the Zn and/or Mn additions in the magnetite structure contributed to enhance of the saturation magnetization as expected with the highest value of saturation magnetization for Zn-Mn equivalent doped magnetite. The magnetic hyperthermia properties were evaluated in aqueous media at pH 5 for 10 min in a 25 mT and 112 kHz alternating magnetic field and it was observed that manganese-only doped sample reached the highest hyperthermia rate, while Zn doping decreased hyperthermia property. The intrinsic loss power (ILP) values varies from 0.2 to 1.0 nHm2 kg-1 with Mn doping values increasing and the magnetic hyperthermia effect was assigned mainly to the Néel-Brownian relaxation processCONSELHO NACIONAL DE DESENVOLVIMENTO CIENTÍFICO E TECNOLÓGICO - CNPQCOORDENAÇÃO DE APERFEIÇOAMENTO DE PESSOAL DE NÍVEL SUPERIOR - CAPESFUNDAÇÃO DE AMPARO À PESQUISA DO ESTADO DE SÃO PAULO - FAPESPFechadoUNIVERSIDADE ESTADUAL DE CAMPINASMassoni, Laura Bissoli de Mello, 1987-Sígoli, Fernando Aparecido, 1972-Mazali, Italo Odone, 1972-2019info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/articleapplication/pdfhttps://hdl.handle.net/20.500.12733/1670943MASSONI, Laura Bissoli de Mello; SÍGOLI, Fernando Aparecido; MAZALI, Italo Odone. Co-precipitation synthesis of (Zn-Mn)-co-doped magnetite nanoparticles and their application in magnetic hyperthermia. Journal of alloys and compounds. An interdisciplinary journal of materials science and solid-state chemistry and physics. Amsterdam : Elsevier, 2019.. Vol. 779 (Mar., 2019), p. 698-705. Disponível em: https://hdl.handle.net/20.500.12733/1670943. Acesso em: 24 mai. 2023.Inglêshttps://repositorio.unicamp.br/acervo/detalhe/1228150reponame:Repositório da Produção Científica e Intelectual da Unicampinstname:Universidade Estadual de Campinas (UNICAMP)instacron:UNICAMPinfo:eu-repo/semantics/openAccess2022-04-01T10:45:33Zoai:https://www.repositorio.unicamp.br/:1228150Repositório InstitucionalPUBhttp://repositorio.unicamp.br/oai/requestreposip@unicamp.bropendoar:2022-04-01T10:45:33Repositório da Produção Científica e Intelectual da Unicamp - Universidade Estadual de Campinas (UNICAMP)false |
dc.title.none.fl_str_mv |
Co-precipitation synthesis of (Zn-Mn)-co-doped magnetite nanoparticles and their application in magnetic hyperthermia |
title |
Co-precipitation synthesis of (Zn-Mn)-co-doped magnetite nanoparticles and their application in magnetic hyperthermia |
spellingShingle |
Co-precipitation synthesis of (Zn-Mn)-co-doped magnetite nanoparticles and their application in magnetic hyperthermia Massoni, Laura Bissoli de Mello, 1987- Ferrita Febre Medições magnéticas Ferrite Fever Magnetic measurements Oxide materials Precipitation Artigo original |
title_short |
Co-precipitation synthesis of (Zn-Mn)-co-doped magnetite nanoparticles and their application in magnetic hyperthermia |
title_full |
Co-precipitation synthesis of (Zn-Mn)-co-doped magnetite nanoparticles and their application in magnetic hyperthermia |
title_fullStr |
Co-precipitation synthesis of (Zn-Mn)-co-doped magnetite nanoparticles and their application in magnetic hyperthermia |
title_full_unstemmed |
Co-precipitation synthesis of (Zn-Mn)-co-doped magnetite nanoparticles and their application in magnetic hyperthermia |
title_sort |
Co-precipitation synthesis of (Zn-Mn)-co-doped magnetite nanoparticles and their application in magnetic hyperthermia |
author |
Massoni, Laura Bissoli de Mello, 1987- |
author_facet |
Massoni, Laura Bissoli de Mello, 1987- Sígoli, Fernando Aparecido, 1972- Mazali, Italo Odone, 1972- |
author_role |
author |
author2 |
Sígoli, Fernando Aparecido, 1972- Mazali, Italo Odone, 1972- |
author2_role |
author author |
dc.contributor.none.fl_str_mv |
UNIVERSIDADE ESTADUAL DE CAMPINAS |
dc.contributor.author.fl_str_mv |
Massoni, Laura Bissoli de Mello, 1987- Sígoli, Fernando Aparecido, 1972- Mazali, Italo Odone, 1972- |
dc.subject.por.fl_str_mv |
Ferrita Febre Medições magnéticas Ferrite Fever Magnetic measurements Oxide materials Precipitation Artigo original |
topic |
Ferrita Febre Medições magnéticas Ferrite Fever Magnetic measurements Oxide materials Precipitation Artigo original |
description |
Agradecimentos: We gratefully acknowledge CAPES, CNPq, FAPESP, and INOMAT for the financial support, Brazilian Nanotechnology National Laboratory for HR-TEM measurements performed in a JEOL JEM-2100 microscope and Prof. Fanny Béron from IFGW-UNICAMP for magnetic measurements |
publishDate |
2019 |
dc.date.none.fl_str_mv |
2019 |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
https://hdl.handle.net/20.500.12733/1670943 MASSONI, Laura Bissoli de Mello; SÍGOLI, Fernando Aparecido; MAZALI, Italo Odone. Co-precipitation synthesis of (Zn-Mn)-co-doped magnetite nanoparticles and their application in magnetic hyperthermia. Journal of alloys and compounds. An interdisciplinary journal of materials science and solid-state chemistry and physics. Amsterdam : Elsevier, 2019.. Vol. 779 (Mar., 2019), p. 698-705. Disponível em: https://hdl.handle.net/20.500.12733/1670943. Acesso em: 24 mai. 2023. |
url |
https://hdl.handle.net/20.500.12733/1670943 |
identifier_str_mv |
MASSONI, Laura Bissoli de Mello; SÍGOLI, Fernando Aparecido; MAZALI, Italo Odone. Co-precipitation synthesis of (Zn-Mn)-co-doped magnetite nanoparticles and their application in magnetic hyperthermia. Journal of alloys and compounds. An interdisciplinary journal of materials science and solid-state chemistry and physics. Amsterdam : Elsevier, 2019.. Vol. 779 (Mar., 2019), p. 698-705. Disponível em: https://hdl.handle.net/20.500.12733/1670943. Acesso em: 24 mai. 2023. |
dc.language.iso.fl_str_mv |
Inglês |
language_invalid_str_mv |
Inglês |
dc.relation.none.fl_str_mv |
https://repositorio.unicamp.br/acervo/detalhe/1228150 |
dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess |
eu_rights_str_mv |
openAccess |
dc.format.none.fl_str_mv |
application/pdf |
dc.source.none.fl_str_mv |
reponame:Repositório da Produção Científica e Intelectual da Unicamp instname:Universidade Estadual de Campinas (UNICAMP) instacron:UNICAMP |
instname_str |
Universidade Estadual de Campinas (UNICAMP) |
instacron_str |
UNICAMP |
institution |
UNICAMP |
reponame_str |
Repositório da Produção Científica e Intelectual da Unicamp |
collection |
Repositório da Produção Científica e Intelectual da Unicamp |
repository.name.fl_str_mv |
Repositório da Produção Científica e Intelectual da Unicamp - Universidade Estadual de Campinas (UNICAMP) |
repository.mail.fl_str_mv |
reposip@unicamp.br |
_version_ |
1766887318878158848 |