Fe-Doping Effect on the Bi3Ni Superconductor Microstructure
Autor(a) principal: | |
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Data de Publicação: | 2017 |
Outros Autores: | , , , , , , |
Tipo de documento: | Artigo |
Idioma: | eng |
Título da fonte: | Materials research (São Carlos. Online) |
Texto Completo: | http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392017000300601 |
Resumo: | The substitution effects of Fe ion on the structure of the intermetallic Bi3Ni1-xFex (0 ≤ x ≤ 0.10) superconductor were studied. The morphology of samples consists of an inhomogeneous laminar slab-like microstructure. The main phase corresponds to Bi3Ni1-xFex with an orthorhombic structure (Pnma), but with very small quantities of impurities of BiNi and Bi as revealed by X-ray diffraction. SEM and AFM reveal that the Bi3Ni1-xFex phase consists of two regions. One region is Bi richer and Ni and Fe poorer than the other region. Raman spectroscopy revealed two phonon modes at room temperature. No significant changes were observed in the spectra with Fe doping and in different regions of the Bi3Ni1-xFex phase. Superconductivity is observed below a transition temperature TC = 4 K and regardless of iron doping. |
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Materials research (São Carlos. Online) |
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Fe-Doping Effect on the Bi3Ni Superconductor MicrostructureBi3NiSuperconductorIntermetallic alloysIronThe substitution effects of Fe ion on the structure of the intermetallic Bi3Ni1-xFex (0 ≤ x ≤ 0.10) superconductor were studied. The morphology of samples consists of an inhomogeneous laminar slab-like microstructure. The main phase corresponds to Bi3Ni1-xFex with an orthorhombic structure (Pnma), but with very small quantities of impurities of BiNi and Bi as revealed by X-ray diffraction. SEM and AFM reveal that the Bi3Ni1-xFex phase consists of two regions. One region is Bi richer and Ni and Fe poorer than the other region. Raman spectroscopy revealed two phonon modes at room temperature. No significant changes were observed in the spectra with Fe doping and in different regions of the Bi3Ni1-xFex phase. Superconductivity is observed below a transition temperature TC = 4 K and regardless of iron doping.ABM, ABC, ABPol2017-06-01info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersiontext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392017000300601Materials Research v.20 n.3 2017reponame:Materials research (São Carlos. Online)instname:Universidade Federal de São Carlos (UFSCAR)instacron:ABM ABC ABPOL10.1590/1980-5373-mr-2016-0538info:eu-repo/semantics/openAccessGonsalves,Silvio HenriqueMonteiro,João Frederico Haas LeandroLeal,Adriane Consuelo Da SilvaAndrade,André Vitor Chaves deSouza,Gelson Biscaia deSiqueira,Ezequiel CostaSerbena,Francisco CarlosJurelo,Alcione Robertoeng2017-06-23T00:00:00Zoai:scielo:S1516-14392017000300601Revistahttp://www.scielo.br/mrPUBhttps://old.scielo.br/oai/scielo-oai.phpdedz@power.ufscar.br1980-53731516-1439opendoar:2017-06-23T00:00Materials research (São Carlos. Online) - Universidade Federal de São Carlos (UFSCAR)false |
dc.title.none.fl_str_mv |
Fe-Doping Effect on the Bi3Ni Superconductor Microstructure |
title |
Fe-Doping Effect on the Bi3Ni Superconductor Microstructure |
spellingShingle |
Fe-Doping Effect on the Bi3Ni Superconductor Microstructure Gonsalves,Silvio Henrique Bi3Ni Superconductor Intermetallic alloys Iron |
title_short |
Fe-Doping Effect on the Bi3Ni Superconductor Microstructure |
title_full |
Fe-Doping Effect on the Bi3Ni Superconductor Microstructure |
title_fullStr |
Fe-Doping Effect on the Bi3Ni Superconductor Microstructure |
title_full_unstemmed |
Fe-Doping Effect on the Bi3Ni Superconductor Microstructure |
title_sort |
Fe-Doping Effect on the Bi3Ni Superconductor Microstructure |
author |
Gonsalves,Silvio Henrique |
author_facet |
Gonsalves,Silvio Henrique Monteiro,João Frederico Haas Leandro Leal,Adriane Consuelo Da Silva Andrade,André Vitor Chaves de Souza,Gelson Biscaia de Siqueira,Ezequiel Costa Serbena,Francisco Carlos Jurelo,Alcione Roberto |
author_role |
author |
author2 |
Monteiro,João Frederico Haas Leandro Leal,Adriane Consuelo Da Silva Andrade,André Vitor Chaves de Souza,Gelson Biscaia de Siqueira,Ezequiel Costa Serbena,Francisco Carlos Jurelo,Alcione Roberto |
author2_role |
author author author author author author author |
dc.contributor.author.fl_str_mv |
Gonsalves,Silvio Henrique Monteiro,João Frederico Haas Leandro Leal,Adriane Consuelo Da Silva Andrade,André Vitor Chaves de Souza,Gelson Biscaia de Siqueira,Ezequiel Costa Serbena,Francisco Carlos Jurelo,Alcione Roberto |
dc.subject.por.fl_str_mv |
Bi3Ni Superconductor Intermetallic alloys Iron |
topic |
Bi3Ni Superconductor Intermetallic alloys Iron |
description |
The substitution effects of Fe ion on the structure of the intermetallic Bi3Ni1-xFex (0 ≤ x ≤ 0.10) superconductor were studied. The morphology of samples consists of an inhomogeneous laminar slab-like microstructure. The main phase corresponds to Bi3Ni1-xFex with an orthorhombic structure (Pnma), but with very small quantities of impurities of BiNi and Bi as revealed by X-ray diffraction. SEM and AFM reveal that the Bi3Ni1-xFex phase consists of two regions. One region is Bi richer and Ni and Fe poorer than the other region. Raman spectroscopy revealed two phonon modes at room temperature. No significant changes were observed in the spectra with Fe doping and in different regions of the Bi3Ni1-xFex phase. Superconductivity is observed below a transition temperature TC = 4 K and regardless of iron doping. |
publishDate |
2017 |
dc.date.none.fl_str_mv |
2017-06-01 |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392017000300601 |
url |
http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392017000300601 |
dc.language.iso.fl_str_mv |
eng |
language |
eng |
dc.relation.none.fl_str_mv |
10.1590/1980-5373-mr-2016-0538 |
dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess |
eu_rights_str_mv |
openAccess |
dc.format.none.fl_str_mv |
text/html |
dc.publisher.none.fl_str_mv |
ABM, ABC, ABPol |
publisher.none.fl_str_mv |
ABM, ABC, ABPol |
dc.source.none.fl_str_mv |
Materials Research v.20 n.3 2017 reponame:Materials research (São Carlos. Online) instname:Universidade Federal de São Carlos (UFSCAR) instacron:ABM ABC ABPOL |
instname_str |
Universidade Federal de São Carlos (UFSCAR) |
instacron_str |
ABM ABC ABPOL |
institution |
ABM ABC ABPOL |
reponame_str |
Materials research (São Carlos. Online) |
collection |
Materials research (São Carlos. Online) |
repository.name.fl_str_mv |
Materials research (São Carlos. Online) - Universidade Federal de São Carlos (UFSCAR) |
repository.mail.fl_str_mv |
dedz@power.ufscar.br |
_version_ |
1754212670657003520 |