Effect of different precursors in the chemical synthesis of ZnO nanocrystals
Autor(a) principal: | |
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Data de Publicação: | 2011 |
Outros Autores: | , , , , , , , , |
Tipo de documento: | Artigo |
Idioma: | eng |
Título da fonte: | Materials research (São Carlos. Online) |
Texto Completo: | http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392011000200020 |
Resumo: | This work evaluates the effect of ZnCl2 and Zn(NO3)2.6H2O as precursors in the synthesis of ZnO nanocrystals. The materials were obtained at 90 ºC by a simple solochemical route. The resulting samples were characterized regarding phase composition, particle size and morphology, by means of XRD and TEM. The analysis have provided evidences that the material obtained applying Zn(NO3)2.6H2O as precursor has hexagonal crystalline structure, typical of the ZnO, and dimensions in the nanoscale. However, applying ZnCl2 as precursor results in a mixture of ZnO and Zn5(OH)8Cl2.H2O phases. For both precursors, the predominant morphology of the obtained ZnO nanocrystals was the rod-like structure. |
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Effect of different precursors in the chemical synthesis of ZnO nanocrystalsnanocrystalline materialszinc oxidesolochemical methodThis work evaluates the effect of ZnCl2 and Zn(NO3)2.6H2O as precursors in the synthesis of ZnO nanocrystals. The materials were obtained at 90 ºC by a simple solochemical route. The resulting samples were characterized regarding phase composition, particle size and morphology, by means of XRD and TEM. The analysis have provided evidences that the material obtained applying Zn(NO3)2.6H2O as precursor has hexagonal crystalline structure, typical of the ZnO, and dimensions in the nanoscale. However, applying ZnCl2 as precursor results in a mixture of ZnO and Zn5(OH)8Cl2.H2O phases. For both precursors, the predominant morphology of the obtained ZnO nanocrystals was the rod-like structure.ABM, ABC, ABPol2011-01-01info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersiontext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392011000200020Materials Research v.14 n.2 2011reponame:Materials research (São Carlos. Online)instname:Universidade Federal de São Carlos (UFSCAR)instacron:ABM ABC ABPOL10.1590/S1516-14392011005000035info:eu-repo/semantics/openAccessGusatti,MarivoneBarroso,Gilvan SérgioCampos,Carlos Eduardo Maduro deSouza,Daniel Aragão Ribeiro deRosário,Jeane de Almeida doLima,Raquel BohnMilioli,Camila CardosoSilva,Laura AbreuRiella,Humberto GracherKuhnen,Nivaldo Cabraleng2011-06-27T00:00:00Zoai:scielo:S1516-14392011000200020Revistahttp://www.scielo.br/mrPUBhttps://old.scielo.br/oai/scielo-oai.phpdedz@power.ufscar.br1980-53731516-1439opendoar:2011-06-27T00:00Materials research (São Carlos. Online) - Universidade Federal de São Carlos (UFSCAR)false |
dc.title.none.fl_str_mv |
Effect of different precursors in the chemical synthesis of ZnO nanocrystals |
title |
Effect of different precursors in the chemical synthesis of ZnO nanocrystals |
spellingShingle |
Effect of different precursors in the chemical synthesis of ZnO nanocrystals Gusatti,Marivone nanocrystalline materials zinc oxide solochemical method |
title_short |
Effect of different precursors in the chemical synthesis of ZnO nanocrystals |
title_full |
Effect of different precursors in the chemical synthesis of ZnO nanocrystals |
title_fullStr |
Effect of different precursors in the chemical synthesis of ZnO nanocrystals |
title_full_unstemmed |
Effect of different precursors in the chemical synthesis of ZnO nanocrystals |
title_sort |
Effect of different precursors in the chemical synthesis of ZnO nanocrystals |
author |
Gusatti,Marivone |
author_facet |
Gusatti,Marivone Barroso,Gilvan Sérgio Campos,Carlos Eduardo Maduro de Souza,Daniel Aragão Ribeiro de Rosário,Jeane de Almeida do Lima,Raquel Bohn Milioli,Camila Cardoso Silva,Laura Abreu Riella,Humberto Gracher Kuhnen,Nivaldo Cabral |
author_role |
author |
author2 |
Barroso,Gilvan Sérgio Campos,Carlos Eduardo Maduro de Souza,Daniel Aragão Ribeiro de Rosário,Jeane de Almeida do Lima,Raquel Bohn Milioli,Camila Cardoso Silva,Laura Abreu Riella,Humberto Gracher Kuhnen,Nivaldo Cabral |
author2_role |
author author author author author author author author author |
dc.contributor.author.fl_str_mv |
Gusatti,Marivone Barroso,Gilvan Sérgio Campos,Carlos Eduardo Maduro de Souza,Daniel Aragão Ribeiro de Rosário,Jeane de Almeida do Lima,Raquel Bohn Milioli,Camila Cardoso Silva,Laura Abreu Riella,Humberto Gracher Kuhnen,Nivaldo Cabral |
dc.subject.por.fl_str_mv |
nanocrystalline materials zinc oxide solochemical method |
topic |
nanocrystalline materials zinc oxide solochemical method |
description |
This work evaluates the effect of ZnCl2 and Zn(NO3)2.6H2O as precursors in the synthesis of ZnO nanocrystals. The materials were obtained at 90 ºC by a simple solochemical route. The resulting samples were characterized regarding phase composition, particle size and morphology, by means of XRD and TEM. The analysis have provided evidences that the material obtained applying Zn(NO3)2.6H2O as precursor has hexagonal crystalline structure, typical of the ZnO, and dimensions in the nanoscale. However, applying ZnCl2 as precursor results in a mixture of ZnO and Zn5(OH)8Cl2.H2O phases. For both precursors, the predominant morphology of the obtained ZnO nanocrystals was the rod-like structure. |
publishDate |
2011 |
dc.date.none.fl_str_mv |
2011-01-01 |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392011000200020 |
url |
http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392011000200020 |
dc.language.iso.fl_str_mv |
eng |
language |
eng |
dc.relation.none.fl_str_mv |
10.1590/S1516-14392011005000035 |
dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess |
eu_rights_str_mv |
openAccess |
dc.format.none.fl_str_mv |
text/html |
dc.publisher.none.fl_str_mv |
ABM, ABC, ABPol |
publisher.none.fl_str_mv |
ABM, ABC, ABPol |
dc.source.none.fl_str_mv |
Materials Research v.14 n.2 2011 reponame:Materials research (São Carlos. Online) instname:Universidade Federal de São Carlos (UFSCAR) instacron:ABM ABC ABPOL |
instname_str |
Universidade Federal de São Carlos (UFSCAR) |
instacron_str |
ABM ABC ABPOL |
institution |
ABM ABC ABPOL |
reponame_str |
Materials research (São Carlos. Online) |
collection |
Materials research (São Carlos. Online) |
repository.name.fl_str_mv |
Materials research (São Carlos. Online) - Universidade Federal de São Carlos (UFSCAR) |
repository.mail.fl_str_mv |
dedz@power.ufscar.br |
_version_ |
1754212660157612032 |