The Effect of Nitrogen Flow Rate on the Loadbearing Capacity from Nano- to Macro-Hardness of Austenitic Stainless Steels Magnetron Sputtering-Coated with Stainless Steel Films
Autor(a) principal: | |
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Data de Publicação: | 2020 |
Outros Autores: | , |
Tipo de documento: | Artigo |
Idioma: | eng |
Título da fonte: | Materials research (São Carlos. Online) |
Texto Completo: | http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392020000300223 |
Resumo: | UNS S31603 stainless steel (SS) substrates were covered by reactive magnetron-sputtering with protective SS coatings of the same steel specification. A mechanical characterization study (through nano-, micro- and macro-hardness tests) of samples obtained under two different sputtering conditions and varying the N2 gas flow rate was carried out. This contribution aimed at appraising the effects of varying the nitrogen flow rate on hardness, elastic modulus, and susceptibility to indentation-induced crack formation of the coated SSs. Nitrogen-free samples displayed body-centered cubic (BCC) films with 9.0-9.4 GPa hardness and 203-206 GPa elastic modulus, while their susceptibility to indentation-induced cracking varied between superior and moderated among the two sets of sputtering conditions studied. Samples alloyed with 4-6 N at-% displayed a predominantly face-centered cubic (FCC) structure, 9.4 GPa hardness, 196-218 GPa elastic modulus, and superior resistance to crack formation. Samples with 11.5-22.0 N at-% were fully composed of the FCC structure, displayed 12.4-15.2 GPa hardness, 188-193 GPa elastic modulus, and moderated resistance to indentation-induced crack formation. Samples with 47.0 N at-% displayed FCC compound nitride structure, for which hardness and elastic modulus were 8.1 GPa and 139 GPa, respectively. These samples displayed low resistance to crack formation. |
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The Effect of Nitrogen Flow Rate on the Loadbearing Capacity from Nano- to Macro-Hardness of Austenitic Stainless Steels Magnetron Sputtering-Coated with Stainless Steel Filmsstainless steelsS-phaseloadbearing capacitysteel filmscomposite hardnessfragile failureUNS S31603 stainless steel (SS) substrates were covered by reactive magnetron-sputtering with protective SS coatings of the same steel specification. A mechanical characterization study (through nano-, micro- and macro-hardness tests) of samples obtained under two different sputtering conditions and varying the N2 gas flow rate was carried out. This contribution aimed at appraising the effects of varying the nitrogen flow rate on hardness, elastic modulus, and susceptibility to indentation-induced crack formation of the coated SSs. Nitrogen-free samples displayed body-centered cubic (BCC) films with 9.0-9.4 GPa hardness and 203-206 GPa elastic modulus, while their susceptibility to indentation-induced cracking varied between superior and moderated among the two sets of sputtering conditions studied. Samples alloyed with 4-6 N at-% displayed a predominantly face-centered cubic (FCC) structure, 9.4 GPa hardness, 196-218 GPa elastic modulus, and superior resistance to crack formation. Samples with 11.5-22.0 N at-% were fully composed of the FCC structure, displayed 12.4-15.2 GPa hardness, 188-193 GPa elastic modulus, and moderated resistance to indentation-induced crack formation. Samples with 47.0 N at-% displayed FCC compound nitride structure, for which hardness and elastic modulus were 8.1 GPa and 139 GPa, respectively. These samples displayed low resistance to crack formation.ABM, ABC, ABPol2020-01-01info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersiontext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392020000300223Materials Research v.23 n.3 2020reponame:Materials research (São Carlos. Online)instname:Universidade Federal de São Carlos (UFSCAR)instacron:ABM ABC ABPOL10.1590/1980-5373-mr-2019-0453info:eu-repo/semantics/openAccessGarzón,Carlos M.Vergara,Giovanny A.Recco,Abel A. C.eng2020-09-25T00:00:00Zoai:scielo:S1516-14392020000300223Revistahttp://www.scielo.br/mrPUBhttps://old.scielo.br/oai/scielo-oai.phpdedz@power.ufscar.br1980-53731516-1439opendoar:2020-09-25T00:00Materials research (São Carlos. Online) - Universidade Federal de São Carlos (UFSCAR)false |
dc.title.none.fl_str_mv |
The Effect of Nitrogen Flow Rate on the Loadbearing Capacity from Nano- to Macro-Hardness of Austenitic Stainless Steels Magnetron Sputtering-Coated with Stainless Steel Films |
title |
The Effect of Nitrogen Flow Rate on the Loadbearing Capacity from Nano- to Macro-Hardness of Austenitic Stainless Steels Magnetron Sputtering-Coated with Stainless Steel Films |
spellingShingle |
The Effect of Nitrogen Flow Rate on the Loadbearing Capacity from Nano- to Macro-Hardness of Austenitic Stainless Steels Magnetron Sputtering-Coated with Stainless Steel Films Garzón,Carlos M. stainless steels S-phase loadbearing capacity steel films composite hardness fragile failure |
title_short |
The Effect of Nitrogen Flow Rate on the Loadbearing Capacity from Nano- to Macro-Hardness of Austenitic Stainless Steels Magnetron Sputtering-Coated with Stainless Steel Films |
title_full |
The Effect of Nitrogen Flow Rate on the Loadbearing Capacity from Nano- to Macro-Hardness of Austenitic Stainless Steels Magnetron Sputtering-Coated with Stainless Steel Films |
title_fullStr |
The Effect of Nitrogen Flow Rate on the Loadbearing Capacity from Nano- to Macro-Hardness of Austenitic Stainless Steels Magnetron Sputtering-Coated with Stainless Steel Films |
title_full_unstemmed |
The Effect of Nitrogen Flow Rate on the Loadbearing Capacity from Nano- to Macro-Hardness of Austenitic Stainless Steels Magnetron Sputtering-Coated with Stainless Steel Films |
title_sort |
The Effect of Nitrogen Flow Rate on the Loadbearing Capacity from Nano- to Macro-Hardness of Austenitic Stainless Steels Magnetron Sputtering-Coated with Stainless Steel Films |
author |
Garzón,Carlos M. |
author_facet |
Garzón,Carlos M. Vergara,Giovanny A. Recco,Abel A. C. |
author_role |
author |
author2 |
Vergara,Giovanny A. Recco,Abel A. C. |
author2_role |
author author |
dc.contributor.author.fl_str_mv |
Garzón,Carlos M. Vergara,Giovanny A. Recco,Abel A. C. |
dc.subject.por.fl_str_mv |
stainless steels S-phase loadbearing capacity steel films composite hardness fragile failure |
topic |
stainless steels S-phase loadbearing capacity steel films composite hardness fragile failure |
description |
UNS S31603 stainless steel (SS) substrates were covered by reactive magnetron-sputtering with protective SS coatings of the same steel specification. A mechanical characterization study (through nano-, micro- and macro-hardness tests) of samples obtained under two different sputtering conditions and varying the N2 gas flow rate was carried out. This contribution aimed at appraising the effects of varying the nitrogen flow rate on hardness, elastic modulus, and susceptibility to indentation-induced crack formation of the coated SSs. Nitrogen-free samples displayed body-centered cubic (BCC) films with 9.0-9.4 GPa hardness and 203-206 GPa elastic modulus, while their susceptibility to indentation-induced cracking varied between superior and moderated among the two sets of sputtering conditions studied. Samples alloyed with 4-6 N at-% displayed a predominantly face-centered cubic (FCC) structure, 9.4 GPa hardness, 196-218 GPa elastic modulus, and superior resistance to crack formation. Samples with 11.5-22.0 N at-% were fully composed of the FCC structure, displayed 12.4-15.2 GPa hardness, 188-193 GPa elastic modulus, and moderated resistance to indentation-induced crack formation. Samples with 47.0 N at-% displayed FCC compound nitride structure, for which hardness and elastic modulus were 8.1 GPa and 139 GPa, respectively. These samples displayed low resistance to crack formation. |
publishDate |
2020 |
dc.date.none.fl_str_mv |
2020-01-01 |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392020000300223 |
url |
http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392020000300223 |
dc.language.iso.fl_str_mv |
eng |
language |
eng |
dc.relation.none.fl_str_mv |
10.1590/1980-5373-mr-2019-0453 |
dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess |
eu_rights_str_mv |
openAccess |
dc.format.none.fl_str_mv |
text/html |
dc.publisher.none.fl_str_mv |
ABM, ABC, ABPol |
publisher.none.fl_str_mv |
ABM, ABC, ABPol |
dc.source.none.fl_str_mv |
Materials Research v.23 n.3 2020 reponame:Materials research (São Carlos. Online) instname:Universidade Federal de São Carlos (UFSCAR) instacron:ABM ABC ABPOL |
instname_str |
Universidade Federal de São Carlos (UFSCAR) |
instacron_str |
ABM ABC ABPOL |
institution |
ABM ABC ABPOL |
reponame_str |
Materials research (São Carlos. Online) |
collection |
Materials research (São Carlos. Online) |
repository.name.fl_str_mv |
Materials research (São Carlos. Online) - Universidade Federal de São Carlos (UFSCAR) |
repository.mail.fl_str_mv |
dedz@power.ufscar.br |
_version_ |
1754212677322801152 |