Gd2O2S:Eu3+ Nanophosphors: Microwave Synthesis and X-ray Imaging Detector Application

Detalhes bibliográficos
Autor(a) principal: Rahim,Sapizah
Data de Publicação: 2019
Outros Autores: Hasim,Muhammad Hassyakirin, Ayob,Muhammad Taqiyuddin Mawardi, Rahman,Irman Abdul, Salleh,Khairul Anuar Mohd, Radiman,Shahidan
Tipo de documento: Artigo
Idioma: eng
Título da fonte: Materials research (São Carlos. Online)
Texto Completo: http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392019000600234
Resumo: Red-emitting Gd2O2S:Eu3+ nanophosphors were successfully prepared using a microwave irradiation method followed by hydrogenation treatment. The optimum calcination temperature (900 ºC) was determined by thermogravimetric-differential scanning calorimetry. The X-ray diffraction results showed that all the samples consisted of the pure hexagonal Gd2O2S:Eu3+ phase. The field emission scanning electron microscopy images showed that the Gd2O2S:Eu3+ nanophosphors were spherical, and their average particle diameter increased parallel with the microwave irradiation power. The photoluminescence spectra (under 325-nm excitation) of the samples exhibited red emission corresponding to the 5D0→7F2 transition of Eu3+ ions. A Gd2O2S:Eu3+ nanophosphor screen film was fabricated using the particle-binder sedimentation method. The result shows that the luminance of the Gd2O2S:Eu3+ nanophosphor screen film increased with an increase in the X-ray energy. Hence, this film would become one of the potential candidate for future imaging applications.
id ABMABCABPOL-1_a30c0e395a50e46de15bdead0949be57
oai_identifier_str oai:scielo:S1516-14392019000600234
network_acronym_str ABMABCABPOL-1
network_name_str Materials research (São Carlos. Online)
repository_id_str
spelling Gd2O2S:Eu3+ Nanophosphors: Microwave Synthesis and X-ray Imaging Detector ApplicationGd2O2S:Eu3+ nanophosphorsmicrowaveluminescentimaging detectorRed-emitting Gd2O2S:Eu3+ nanophosphors were successfully prepared using a microwave irradiation method followed by hydrogenation treatment. The optimum calcination temperature (900 ºC) was determined by thermogravimetric-differential scanning calorimetry. The X-ray diffraction results showed that all the samples consisted of the pure hexagonal Gd2O2S:Eu3+ phase. The field emission scanning electron microscopy images showed that the Gd2O2S:Eu3+ nanophosphors were spherical, and their average particle diameter increased parallel with the microwave irradiation power. The photoluminescence spectra (under 325-nm excitation) of the samples exhibited red emission corresponding to the 5D0→7F2 transition of Eu3+ ions. A Gd2O2S:Eu3+ nanophosphor screen film was fabricated using the particle-binder sedimentation method. The result shows that the luminance of the Gd2O2S:Eu3+ nanophosphor screen film increased with an increase in the X-ray energy. Hence, this film would become one of the potential candidate for future imaging applications.ABM, ABC, ABPol2019-01-01info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersiontext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392019000600234Materials Research v.22 n.6 2019reponame:Materials research (São Carlos. Online)instname:Universidade Federal de São Carlos (UFSCAR)instacron:ABM ABC ABPOL10.1590/1980-5373-mr-2019-0383info:eu-repo/semantics/openAccessRahim,SapizahHasim,Muhammad HassyakirinAyob,Muhammad Taqiyuddin MawardiRahman,Irman AbdulSalleh,Khairul Anuar MohdRadiman,Shahidaneng2020-03-06T00:00:00Zoai:scielo:S1516-14392019000600234Revistahttp://www.scielo.br/mrPUBhttps://old.scielo.br/oai/scielo-oai.phpdedz@power.ufscar.br1980-53731516-1439opendoar:2020-03-06T00:00Materials research (São Carlos. Online) - Universidade Federal de São Carlos (UFSCAR)false
dc.title.none.fl_str_mv Gd2O2S:Eu3+ Nanophosphors: Microwave Synthesis and X-ray Imaging Detector Application
title Gd2O2S:Eu3+ Nanophosphors: Microwave Synthesis and X-ray Imaging Detector Application
spellingShingle Gd2O2S:Eu3+ Nanophosphors: Microwave Synthesis and X-ray Imaging Detector Application
Rahim,Sapizah
Gd2O2S:Eu3+ nanophosphors
microwave
luminescent
imaging detector
title_short Gd2O2S:Eu3+ Nanophosphors: Microwave Synthesis and X-ray Imaging Detector Application
title_full Gd2O2S:Eu3+ Nanophosphors: Microwave Synthesis and X-ray Imaging Detector Application
title_fullStr Gd2O2S:Eu3+ Nanophosphors: Microwave Synthesis and X-ray Imaging Detector Application
title_full_unstemmed Gd2O2S:Eu3+ Nanophosphors: Microwave Synthesis and X-ray Imaging Detector Application
title_sort Gd2O2S:Eu3+ Nanophosphors: Microwave Synthesis and X-ray Imaging Detector Application
author Rahim,Sapizah
author_facet Rahim,Sapizah
Hasim,Muhammad Hassyakirin
Ayob,Muhammad Taqiyuddin Mawardi
Rahman,Irman Abdul
Salleh,Khairul Anuar Mohd
Radiman,Shahidan
author_role author
author2 Hasim,Muhammad Hassyakirin
Ayob,Muhammad Taqiyuddin Mawardi
Rahman,Irman Abdul
Salleh,Khairul Anuar Mohd
Radiman,Shahidan
author2_role author
author
author
author
author
dc.contributor.author.fl_str_mv Rahim,Sapizah
Hasim,Muhammad Hassyakirin
Ayob,Muhammad Taqiyuddin Mawardi
Rahman,Irman Abdul
Salleh,Khairul Anuar Mohd
Radiman,Shahidan
dc.subject.por.fl_str_mv Gd2O2S:Eu3+ nanophosphors
microwave
luminescent
imaging detector
topic Gd2O2S:Eu3+ nanophosphors
microwave
luminescent
imaging detector
description Red-emitting Gd2O2S:Eu3+ nanophosphors were successfully prepared using a microwave irradiation method followed by hydrogenation treatment. The optimum calcination temperature (900 ºC) was determined by thermogravimetric-differential scanning calorimetry. The X-ray diffraction results showed that all the samples consisted of the pure hexagonal Gd2O2S:Eu3+ phase. The field emission scanning electron microscopy images showed that the Gd2O2S:Eu3+ nanophosphors were spherical, and their average particle diameter increased parallel with the microwave irradiation power. The photoluminescence spectra (under 325-nm excitation) of the samples exhibited red emission corresponding to the 5D0→7F2 transition of Eu3+ ions. A Gd2O2S:Eu3+ nanophosphor screen film was fabricated using the particle-binder sedimentation method. The result shows that the luminance of the Gd2O2S:Eu3+ nanophosphor screen film increased with an increase in the X-ray energy. Hence, this film would become one of the potential candidate for future imaging applications.
publishDate 2019
dc.date.none.fl_str_mv 2019-01-01
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392019000600234
url http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392019000600234
dc.language.iso.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv 10.1590/1980-5373-mr-2019-0383
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv text/html
dc.publisher.none.fl_str_mv ABM, ABC, ABPol
publisher.none.fl_str_mv ABM, ABC, ABPol
dc.source.none.fl_str_mv Materials Research v.22 n.6 2019
reponame:Materials research (São Carlos. Online)
instname:Universidade Federal de São Carlos (UFSCAR)
instacron:ABM ABC ABPOL
instname_str Universidade Federal de São Carlos (UFSCAR)
instacron_str ABM ABC ABPOL
institution ABM ABC ABPOL
reponame_str Materials research (São Carlos. Online)
collection Materials research (São Carlos. Online)
repository.name.fl_str_mv Materials research (São Carlos. Online) - Universidade Federal de São Carlos (UFSCAR)
repository.mail.fl_str_mv dedz@power.ufscar.br
_version_ 1754212675523444736

Registros relacionados