Fish Bone as a Source of Raw Material for Synthesis of Calcium Phosphate

Detalhes bibliográficos
Autor(a) principal: Corrêa,Tarcília Henrique Amaral
Data de Publicação: 2019
Outros Autores: Holanda,José Nilson França
Tipo de documento: Artigo
Idioma: eng
Título da fonte: Materials research (São Carlos. Online)
Texto Completo: http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392019000700251
Resumo: Fish bone is rich in calcium carbonate, which makes it an alternative source of low cost calcium carbonate for the synthesis of calcium phosphate bioceramic for use in bone regeneration. The calcium phosphate bioceramic was prepared by a wet precipitation method with acid and base reactions. The synthesized bioceramic was characterized in terms of X-ray diffraction (XRD), scanning electron microscopy (SEM/EDS), thermogravimetric analysis (TGA), Fourier transform infrared spectroscopy (FTRI), average crystallite size and refinement by the Rietveld method for the quantification of crystalline phases. The results indicated the formation of a biphasic calcium phosphate bioceramic comprising 67.6 % of β-calcium pyrophosphate (β-CPP) and 32.1 % of β-tricalcium phosphate (β-TCP). This biphasic calcium phosphate bioceramic synthesized using fish bone waste presented nanostructured nature with an average crystallite size of 69.58 nm, which is very promising for biomedical applications.
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spelling Fish Bone as a Source of Raw Material for Synthesis of Calcium PhosphateCalcium phosphatebiphasic bioceramicfish bone wastenanocrystallitesFish bone is rich in calcium carbonate, which makes it an alternative source of low cost calcium carbonate for the synthesis of calcium phosphate bioceramic for use in bone regeneration. The calcium phosphate bioceramic was prepared by a wet precipitation method with acid and base reactions. The synthesized bioceramic was characterized in terms of X-ray diffraction (XRD), scanning electron microscopy (SEM/EDS), thermogravimetric analysis (TGA), Fourier transform infrared spectroscopy (FTRI), average crystallite size and refinement by the Rietveld method for the quantification of crystalline phases. The results indicated the formation of a biphasic calcium phosphate bioceramic comprising 67.6 % of β-calcium pyrophosphate (β-CPP) and 32.1 % of β-tricalcium phosphate (β-TCP). This biphasic calcium phosphate bioceramic synthesized using fish bone waste presented nanostructured nature with an average crystallite size of 69.58 nm, which is very promising for biomedical applications.ABM, ABC, ABPol2019-01-01info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersiontext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392019000700251Materials Research v.22 suppl.1 2019reponame:Materials research (São Carlos. Online)instname:Universidade Federal de São Carlos (UFSCAR)instacron:ABM ABC ABPOL10.1590/1980-5373-mr-2019-0486info:eu-repo/semantics/openAccessCorrêa,Tarcília Henrique AmaralHolanda,José Nilson Françaeng2019-10-24T00:00:00Zoai:scielo:S1516-14392019000700251Revistahttp://www.scielo.br/mrPUBhttps://old.scielo.br/oai/scielo-oai.phpdedz@power.ufscar.br1980-53731516-1439opendoar:2019-10-24T00:00Materials research (São Carlos. Online) - Universidade Federal de São Carlos (UFSCAR)false
dc.title.none.fl_str_mv Fish Bone as a Source of Raw Material for Synthesis of Calcium Phosphate
title Fish Bone as a Source of Raw Material for Synthesis of Calcium Phosphate
spellingShingle Fish Bone as a Source of Raw Material for Synthesis of Calcium Phosphate
Corrêa,Tarcília Henrique Amaral
Calcium phosphate
biphasic bioceramic
fish bone waste
nanocrystallites
title_short Fish Bone as a Source of Raw Material for Synthesis of Calcium Phosphate
title_full Fish Bone as a Source of Raw Material for Synthesis of Calcium Phosphate
title_fullStr Fish Bone as a Source of Raw Material for Synthesis of Calcium Phosphate
title_full_unstemmed Fish Bone as a Source of Raw Material for Synthesis of Calcium Phosphate
title_sort Fish Bone as a Source of Raw Material for Synthesis of Calcium Phosphate
author Corrêa,Tarcília Henrique Amaral
author_facet Corrêa,Tarcília Henrique Amaral
Holanda,José Nilson França
author_role author
author2 Holanda,José Nilson França
author2_role author
dc.contributor.author.fl_str_mv Corrêa,Tarcília Henrique Amaral
Holanda,José Nilson França
dc.subject.por.fl_str_mv Calcium phosphate
biphasic bioceramic
fish bone waste
nanocrystallites
topic Calcium phosphate
biphasic bioceramic
fish bone waste
nanocrystallites
description Fish bone is rich in calcium carbonate, which makes it an alternative source of low cost calcium carbonate for the synthesis of calcium phosphate bioceramic for use in bone regeneration. The calcium phosphate bioceramic was prepared by a wet precipitation method with acid and base reactions. The synthesized bioceramic was characterized in terms of X-ray diffraction (XRD), scanning electron microscopy (SEM/EDS), thermogravimetric analysis (TGA), Fourier transform infrared spectroscopy (FTRI), average crystallite size and refinement by the Rietveld method for the quantification of crystalline phases. The results indicated the formation of a biphasic calcium phosphate bioceramic comprising 67.6 % of β-calcium pyrophosphate (β-CPP) and 32.1 % of β-tricalcium phosphate (β-TCP). This biphasic calcium phosphate bioceramic synthesized using fish bone waste presented nanostructured nature with an average crystallite size of 69.58 nm, which is very promising for biomedical applications.
publishDate 2019
dc.date.none.fl_str_mv 2019-01-01
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392019000700251
url http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392019000700251
dc.language.iso.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv 10.1590/1980-5373-mr-2019-0486
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv text/html
dc.publisher.none.fl_str_mv ABM, ABC, ABPol
publisher.none.fl_str_mv ABM, ABC, ABPol
dc.source.none.fl_str_mv Materials Research v.22 suppl.1 2019
reponame:Materials research (São Carlos. Online)
instname:Universidade Federal de São Carlos (UFSCAR)
instacron:ABM ABC ABPOL
instname_str Universidade Federal de São Carlos (UFSCAR)
instacron_str ABM ABC ABPOL
institution ABM ABC ABPOL
reponame_str Materials research (São Carlos. Online)
collection Materials research (São Carlos. Online)
repository.name.fl_str_mv Materials research (São Carlos. Online) - Universidade Federal de São Carlos (UFSCAR)
repository.mail.fl_str_mv dedz@power.ufscar.br
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