Thermogravimetric and magneticproperties of Ni1-X Zn xFe2O4 nanoparticles synthesized by coprecipitation

Detalhes bibliográficos
Autor(a) principal: Velmurugan,Kandasamy
Data de Publicação: 2009
Outros Autores: Venkatachalapathy,Vellaiyappan Sangli Karuppanan, Sendhilnathan,Sechassalom
Tipo de documento: Artigo
Idioma: eng
Título da fonte: Materials research (São Carlos. Online)
Texto Completo: http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392009000400025
Resumo: Ni1-xZn xFe2O4 (x = 0 to 1) nanoparticles of size less than 9 nm were prepared by a chemical coprecipitation method which could be used for ferrofluid preparation. XRD, VSM and DTA-TG (STA) were used to study the effect of variation in Zn substitution and its influence on particle size, magnetic properties such as M S, H C and Curie temperature, as well as on the water content. ICP was used to estimate Ni, Zn and Fe concentrations. The average crystallite size (DaveXR) of the particles was found to decrease from 8.95 to 6.92 nm with increasing zinc substitution. The lattice constant (a o) increased with increasing zinc substitution. The specific saturation magnetization (M S) of the particles was measured at room temperature. Magnetic parameters such as M S, Hc, and Mr were found to decrease with increasing zinc substitution. Estimation of the water content, which varies the Zn concentration, plays a vital role for the correct determination of cation contents. The Curie temperature was found to decrease with increasing zinc substitution.
id ABMABCABPOL-1_f6f7b17e91daf8c531bdb73c6c602fe6
oai_identifier_str oai:scielo:S1516-14392009000400025
network_acronym_str ABMABCABPOL-1
network_name_str Materials research (São Carlos. Online)
repository_id_str
spelling Thermogravimetric and magneticproperties of Ni1-X Zn xFe2O4 nanoparticles synthesized by coprecipitationcoprecipitationfine particlesnanoferritesspinelNi1-xZn xFe2O4 (x = 0 to 1) nanoparticles of size less than 9 nm were prepared by a chemical coprecipitation method which could be used for ferrofluid preparation. XRD, VSM and DTA-TG (STA) were used to study the effect of variation in Zn substitution and its influence on particle size, magnetic properties such as M S, H C and Curie temperature, as well as on the water content. ICP was used to estimate Ni, Zn and Fe concentrations. The average crystallite size (DaveXR) of the particles was found to decrease from 8.95 to 6.92 nm with increasing zinc substitution. The lattice constant (a o) increased with increasing zinc substitution. The specific saturation magnetization (M S) of the particles was measured at room temperature. Magnetic parameters such as M S, Hc, and Mr were found to decrease with increasing zinc substitution. Estimation of the water content, which varies the Zn concentration, plays a vital role for the correct determination of cation contents. The Curie temperature was found to decrease with increasing zinc substitution.ABM, ABC, ABPol2009-01-01info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersiontext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392009000400025Materials Research v.12 n.4 2009reponame:Materials research (São Carlos. Online)instname:Universidade Federal de São Carlos (UFSCAR)instacron:ABM ABC ABPOL10.1590/S1516-14392009000400025info:eu-repo/semantics/openAccessVelmurugan,KandasamyVenkatachalapathy,Vellaiyappan Sangli KaruppananSendhilnathan,Sechassalomeng2010-01-29T00:00:00Zoai:scielo:S1516-14392009000400025Revistahttp://www.scielo.br/mrPUBhttps://old.scielo.br/oai/scielo-oai.phpdedz@power.ufscar.br1980-53731516-1439opendoar:2010-01-29T00:00Materials research (São Carlos. Online) - Universidade Federal de São Carlos (UFSCAR)false
dc.title.none.fl_str_mv Thermogravimetric and magneticproperties of Ni1-X Zn xFe2O4 nanoparticles synthesized by coprecipitation
title Thermogravimetric and magneticproperties of Ni1-X Zn xFe2O4 nanoparticles synthesized by coprecipitation
spellingShingle Thermogravimetric and magneticproperties of Ni1-X Zn xFe2O4 nanoparticles synthesized by coprecipitation
Velmurugan,Kandasamy
coprecipitation
fine particles
nanoferrites
spinel
title_short Thermogravimetric and magneticproperties of Ni1-X Zn xFe2O4 nanoparticles synthesized by coprecipitation
title_full Thermogravimetric and magneticproperties of Ni1-X Zn xFe2O4 nanoparticles synthesized by coprecipitation
title_fullStr Thermogravimetric and magneticproperties of Ni1-X Zn xFe2O4 nanoparticles synthesized by coprecipitation
title_full_unstemmed Thermogravimetric and magneticproperties of Ni1-X Zn xFe2O4 nanoparticles synthesized by coprecipitation
title_sort Thermogravimetric and magneticproperties of Ni1-X Zn xFe2O4 nanoparticles synthesized by coprecipitation
author Velmurugan,Kandasamy
author_facet Velmurugan,Kandasamy
Venkatachalapathy,Vellaiyappan Sangli Karuppanan
Sendhilnathan,Sechassalom
author_role author
author2 Venkatachalapathy,Vellaiyappan Sangli Karuppanan
Sendhilnathan,Sechassalom
author2_role author
author
dc.contributor.author.fl_str_mv Velmurugan,Kandasamy
Venkatachalapathy,Vellaiyappan Sangli Karuppanan
Sendhilnathan,Sechassalom
dc.subject.por.fl_str_mv coprecipitation
fine particles
nanoferrites
spinel
topic coprecipitation
fine particles
nanoferrites
spinel
description Ni1-xZn xFe2O4 (x = 0 to 1) nanoparticles of size less than 9 nm were prepared by a chemical coprecipitation method which could be used for ferrofluid preparation. XRD, VSM and DTA-TG (STA) were used to study the effect of variation in Zn substitution and its influence on particle size, magnetic properties such as M S, H C and Curie temperature, as well as on the water content. ICP was used to estimate Ni, Zn and Fe concentrations. The average crystallite size (DaveXR) of the particles was found to decrease from 8.95 to 6.92 nm with increasing zinc substitution. The lattice constant (a o) increased with increasing zinc substitution. The specific saturation magnetization (M S) of the particles was measured at room temperature. Magnetic parameters such as M S, Hc, and Mr were found to decrease with increasing zinc substitution. Estimation of the water content, which varies the Zn concentration, plays a vital role for the correct determination of cation contents. The Curie temperature was found to decrease with increasing zinc substitution.
publishDate 2009
dc.date.none.fl_str_mv 2009-01-01
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392009000400025
url http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392009000400025
dc.language.iso.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv 10.1590/S1516-14392009000400025
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv text/html
dc.publisher.none.fl_str_mv ABM, ABC, ABPol
publisher.none.fl_str_mv ABM, ABC, ABPol
dc.source.none.fl_str_mv Materials Research v.12 n.4 2009
reponame:Materials research (São Carlos. Online)
instname:Universidade Federal de São Carlos (UFSCAR)
instacron:ABM ABC ABPOL
instname_str Universidade Federal de São Carlos (UFSCAR)
instacron_str ABM ABC ABPOL
institution ABM ABC ABPOL
reponame_str Materials research (São Carlos. Online)
collection Materials research (São Carlos. Online)
repository.name.fl_str_mv Materials research (São Carlos. Online) - Universidade Federal de São Carlos (UFSCAR)
repository.mail.fl_str_mv dedz@power.ufscar.br
_version_ 1754212659346014208

Registros relacionados