Synthesis, characterization and antibacterial activity of novel poly(silyl ether)s based on palm and soy oils

Detalhes bibliográficos
Autor(a) principal: Mohammed,Issam Ahmed
Data de Publicação: 2018
Outros Autores: Shahabuddin,Syed, Khanam,Rashmin, Saidur,Rahman
Tipo de documento: Artigo
Idioma: eng
Título da fonte: Polímeros (São Carlos. Online)
Texto Completo: http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0104-14282018000500406
Resumo: Abstract In this research, palm oil and soy oil were used as a natural polyol to prepare novel poly(silyl ether)s. Palm oil and soy oil were first converted to monoglyceride by one step via alcoholysis process in the presence of 0.1% CaO as a catalyst. The monoglycerides were characterized by Fourier transform infrared spectrometer (FT-IR), nuclear magnetic resonance (NMR) and iodine test. The novel poly(silyl ether)s were prepared via polycondensation reaction between dimethyldichlorosilane with monoglycerides based on palm and soy oils, respectively. FT-IR, NMR and silicone-29 (29Si NMR) were used to confirm and determine the presence of silicone in the synthesized polymers. Thermal behavior was studied by thermogravimetric analysis (TGA) and differential scanning calorimetry (DSC). Antibacterial activity of the polymers was screened against three different strains of bacteria, namely Escherichia coli E266, Staphylococcus aureus S276 and Salmonella choleeraesuis 10708.
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spelling Synthesis, characterization and antibacterial activity of novel poly(silyl ether)s based on palm and soy oilsantibacterialdimethydichlorosilanepalm oilpoly(silyl ethers)polyolsoy oilAbstract In this research, palm oil and soy oil were used as a natural polyol to prepare novel poly(silyl ether)s. Palm oil and soy oil were first converted to monoglyceride by one step via alcoholysis process in the presence of 0.1% CaO as a catalyst. The monoglycerides were characterized by Fourier transform infrared spectrometer (FT-IR), nuclear magnetic resonance (NMR) and iodine test. The novel poly(silyl ether)s were prepared via polycondensation reaction between dimethyldichlorosilane with monoglycerides based on palm and soy oils, respectively. FT-IR, NMR and silicone-29 (29Si NMR) were used to confirm and determine the presence of silicone in the synthesized polymers. Thermal behavior was studied by thermogravimetric analysis (TGA) and differential scanning calorimetry (DSC). Antibacterial activity of the polymers was screened against three different strains of bacteria, namely Escherichia coli E266, Staphylococcus aureus S276 and Salmonella choleeraesuis 10708.Associação Brasileira de Polímeros2018-12-01info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersiontext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S0104-14282018000500406Polímeros v.28 n.5 2018reponame:Polímeros (São Carlos. Online)instname:Associação Brasileira de Polímeros (ABPol)instacron:ABPO10.1590/0104-1428.10317info:eu-repo/semantics/openAccessMohammed,Issam AhmedShahabuddin,SyedKhanam,RashminSaidur,Rahmaneng2019-01-21T00:00:00Zoai:scielo:S0104-14282018000500406Revistahttp://www.scielo.br/pohttps://old.scielo.br/oai/scielo-oai.php||revista@abpol.org.br1678-51690104-1428opendoar:2019-01-21T00:00Polímeros (São Carlos. Online) - Associação Brasileira de Polímeros (ABPol)false
dc.title.none.fl_str_mv Synthesis, characterization and antibacterial activity of novel poly(silyl ether)s based on palm and soy oils
title Synthesis, characterization and antibacterial activity of novel poly(silyl ether)s based on palm and soy oils
spellingShingle Synthesis, characterization and antibacterial activity of novel poly(silyl ether)s based on palm and soy oils
Mohammed,Issam Ahmed
antibacterial
dimethydichlorosilane
palm oil
poly(silyl ethers)
polyol
soy oil
title_short Synthesis, characterization and antibacterial activity of novel poly(silyl ether)s based on palm and soy oils
title_full Synthesis, characterization and antibacterial activity of novel poly(silyl ether)s based on palm and soy oils
title_fullStr Synthesis, characterization and antibacterial activity of novel poly(silyl ether)s based on palm and soy oils
title_full_unstemmed Synthesis, characterization and antibacterial activity of novel poly(silyl ether)s based on palm and soy oils
title_sort Synthesis, characterization and antibacterial activity of novel poly(silyl ether)s based on palm and soy oils
author Mohammed,Issam Ahmed
author_facet Mohammed,Issam Ahmed
Shahabuddin,Syed
Khanam,Rashmin
Saidur,Rahman
author_role author
author2 Shahabuddin,Syed
Khanam,Rashmin
Saidur,Rahman
author2_role author
author
author
dc.contributor.author.fl_str_mv Mohammed,Issam Ahmed
Shahabuddin,Syed
Khanam,Rashmin
Saidur,Rahman
dc.subject.por.fl_str_mv antibacterial
dimethydichlorosilane
palm oil
poly(silyl ethers)
polyol
soy oil
topic antibacterial
dimethydichlorosilane
palm oil
poly(silyl ethers)
polyol
soy oil
description Abstract In this research, palm oil and soy oil were used as a natural polyol to prepare novel poly(silyl ether)s. Palm oil and soy oil were first converted to monoglyceride by one step via alcoholysis process in the presence of 0.1% CaO as a catalyst. The monoglycerides were characterized by Fourier transform infrared spectrometer (FT-IR), nuclear magnetic resonance (NMR) and iodine test. The novel poly(silyl ether)s were prepared via polycondensation reaction between dimethyldichlorosilane with monoglycerides based on palm and soy oils, respectively. FT-IR, NMR and silicone-29 (29Si NMR) were used to confirm and determine the presence of silicone in the synthesized polymers. Thermal behavior was studied by thermogravimetric analysis (TGA) and differential scanning calorimetry (DSC). Antibacterial activity of the polymers was screened against three different strains of bacteria, namely Escherichia coli E266, Staphylococcus aureus S276 and Salmonella choleeraesuis 10708.
publishDate 2018
dc.date.none.fl_str_mv 2018-12-01
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0104-14282018000500406
url http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0104-14282018000500406
dc.language.iso.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv 10.1590/0104-1428.10317
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv text/html
dc.publisher.none.fl_str_mv Associação Brasileira de Polímeros
publisher.none.fl_str_mv Associação Brasileira de Polímeros
dc.source.none.fl_str_mv Polímeros v.28 n.5 2018
reponame:Polímeros (São Carlos. Online)
instname:Associação Brasileira de Polímeros (ABPol)
instacron:ABPO
instname_str Associação Brasileira de Polímeros (ABPol)
instacron_str ABPO
institution ABPO
reponame_str Polímeros (São Carlos. Online)
collection Polímeros (São Carlos. Online)
repository.name.fl_str_mv Polímeros (São Carlos. Online) - Associação Brasileira de Polímeros (ABPol)
repository.mail.fl_str_mv ||revista@abpol.org.br
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