Comparison of High Performance Liquid Chromatography with Fluorescence Detector and with Tandem Mass Spectrometry methods for detection and quantification of Ochratoxin A in green and roasted coffee beans
| Autor(a) principal: | |
|---|---|
| Data de Publicação: | 2013 |
| Outros Autores: | , , , , , |
| Tipo de documento: | Artigo |
| Idioma: | eng |
| Título da fonte: | Repositório Institucional da FIOCRUZ (ARCA) |
| Texto Completo: | https://www.arca.fiocruz.br/handle/icict/8625 http://dx.doi.org/10.1590/S1516-89132013000600004 |
Resumo: | Instituto Nacional de Metrologia, Qualidade e Tecnologia. Diretoria de Metrologia Cientifíca e Industrial. Divisão de Metrologia Química. Duque de Caxias, RJ, Brasil. |
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Bandeira, Raquel Duarte da Costa CunhaUekane, Thais MatsueCunha, Carolina Passos daRodrigues, Janaína MarquesCruz, Marcus Henrique Campino de LaGodoy, Ronoel Luiz de OliveiraFioravante, Andreia de Lima2014-10-17T18:58:19Z2014-10-17T18:58:19Z2013BANDEIRA, R. D. C. C. et al. Comparison of High Performance Liquid Chromatography with Fluorescence Detector and with Tandem Mass Spectrometry methods for detection and quantification of Ochratoxin A in green and roasted coffee beans. Brazilian Archives of Biological Technology, Curitiba, v. 56, n. 6, p. 911-920. nov./dez. 2013.1516-8913https://www.arca.fiocruz.br/handle/icict/8625http://dx.doi.org/10.1590/S1516-89132013000600004engInstituto de Tecnologia do ParanáComparison of High Performance Liquid Chromatography with Fluorescence Detector and with Tandem Mass Spectrometry methods for detection and quantification of Ochratoxin A in green and roasted coffee beansinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/articleInstituto Nacional de Metrologia, Qualidade e Tecnologia. Diretoria de Metrologia Cientifíca e Industrial. Divisão de Metrologia Química. Duque de Caxias, RJ, Brasil.Instituto Nacional de Metrologia, Qualidade e Tecnologia. Diretoria de Metrologia Cientifíca e Industrial. Divisão de Metrologia Química. Duque de Caxias, RJ, Brasil.Instituto Nacional de Metrologia, Qualidade e Tecnologia. Diretoria de Metrologia Cientifíca e Industrial. Divisão de Metrologia Química. Duque de Caxias, RJ, Brasil.Instituto Nacional de Metrologia, Qualidade e Tecnologia. Diretoria de Metrologia Cientifíca e Industrial. Divisão de Metrologia Química. Duque de Caxias, RJ, Brasil.Fundação Oswaldo Cruz. Instituto Nacional de Controle de Qualidade em Saúde. Comissão do Programa de Ensaio de Proficiência de Produtos Sujeitos ao Regime de Vigilância Sanitária. Rio de Janeiro, RJ, Brasil.Embrapa Agroindustria de Alimentos. Rio de Janeiro, RJ, Brasil.Instituto Nacional de Metrologia, Qualidade e Tecnologia. Diretoria de Metrologia Cientifíca e Industrial. Divisão de Metrologia Química. Duque de Caxias, RJ, Brasil.Two analytical methods for the determination and confirmation of ochratoxin A (OTA) in green and roasted coffee samples were compared. Sample extraction and clean-up were based on liquid–liquid phase extraction and immunoaffinity column. The detection of OTA was carried out with the high performance liquid chromatography (HPLC) combined either with fluorescence detection (FLD), or positive electrospray ionization (ESI+) coupled with tandem mass spectrometry (MS–MS). The results obtained with the LC-ESI-MS/MS were specific and more sensitive, with the advantages in terms of unambiguous analyte identification, when compared with the HPLC-FLD.HPLC-FLDLC-MS/MSGreen CoffeeRoasted CoffeeOchratoxinsCromatografia Líquida de Alta PressãoEspectrometria de MassasCaféRoasted CoffeeOcratoxinasinfo:eu-repo/semantics/openAccessreponame:Repositório Institucional da FIOCRUZ (ARCA)instname:Fundação Oswaldo Cruz (FIOCRUZ)instacron:FIOCRUZLICENSElicense.txtlicense.txttext/plain; charset=utf-81914https://www.arca.fiocruz.br/bitstream/icict/8625/1/license.txt7d48279ffeed55da8dfe2f8e81f3b81fMD51ORIGINALBraz Arch Biol Technol_56_911-920.pdfBraz Arch Biol Technol_56_911-920.pdfapplication/pdf222047https://www.arca.fiocruz.br/bitstream/icict/8625/2/Braz%20Arch%20Biol%20Technol_56_911-920.pdf7812cf22f62960742e5b058d4f6a1274MD52TEXTBraz Arch Biol Technol_56_911-920.pdf.txtBraz Arch Biol Technol_56_911-920.pdf.txtExtracted texttext/plain38580https://www.arca.fiocruz.br/bitstream/icict/8625/3/Braz%20Arch%20Biol%20Technol_56_911-920.pdf.txt8a32c687bb5dc22175fb898d3e942ac3MD53icict/86252018-04-06 08:43:53.685oai:www.arca.fiocruz.br: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ório InstitucionalPUBhttps://www.arca.fiocruz.br/oai/requestrepositorio.arca@fiocruz.bropendoar:21352018-04-06T11:43:53Repositório Institucional da FIOCRUZ (ARCA) - Fundação Oswaldo Cruz (FIOCRUZ)false |
| dc.title.en.fl_str_mv |
Comparison of High Performance Liquid Chromatography with Fluorescence Detector and with Tandem Mass Spectrometry methods for detection and quantification of Ochratoxin A in green and roasted coffee beans |
| title |
Comparison of High Performance Liquid Chromatography with Fluorescence Detector and with Tandem Mass Spectrometry methods for detection and quantification of Ochratoxin A in green and roasted coffee beans |
| spellingShingle |
Comparison of High Performance Liquid Chromatography with Fluorescence Detector and with Tandem Mass Spectrometry methods for detection and quantification of Ochratoxin A in green and roasted coffee beans Bandeira, Raquel Duarte da Costa Cunha HPLC-FLD LC-MS/MS Green Coffee Roasted Coffee Ochratoxins Cromatografia Líquida de Alta Pressão Espectrometria de Massas Café Roasted Coffee Ocratoxinas |
| title_short |
Comparison of High Performance Liquid Chromatography with Fluorescence Detector and with Tandem Mass Spectrometry methods for detection and quantification of Ochratoxin A in green and roasted coffee beans |
| title_full |
Comparison of High Performance Liquid Chromatography with Fluorescence Detector and with Tandem Mass Spectrometry methods for detection and quantification of Ochratoxin A in green and roasted coffee beans |
| title_fullStr |
Comparison of High Performance Liquid Chromatography with Fluorescence Detector and with Tandem Mass Spectrometry methods for detection and quantification of Ochratoxin A in green and roasted coffee beans |
| title_full_unstemmed |
Comparison of High Performance Liquid Chromatography with Fluorescence Detector and with Tandem Mass Spectrometry methods for detection and quantification of Ochratoxin A in green and roasted coffee beans |
| title_sort |
Comparison of High Performance Liquid Chromatography with Fluorescence Detector and with Tandem Mass Spectrometry methods for detection and quantification of Ochratoxin A in green and roasted coffee beans |
| author |
Bandeira, Raquel Duarte da Costa Cunha |
| author_facet |
Bandeira, Raquel Duarte da Costa Cunha Uekane, Thais Matsue Cunha, Carolina Passos da Rodrigues, Janaína Marques Cruz, Marcus Henrique Campino de La Godoy, Ronoel Luiz de Oliveira Fioravante, Andreia de Lima |
| author_role |
author |
| author2 |
Uekane, Thais Matsue Cunha, Carolina Passos da Rodrigues, Janaína Marques Cruz, Marcus Henrique Campino de La Godoy, Ronoel Luiz de Oliveira Fioravante, Andreia de Lima |
| author2_role |
author author author author author author |
| dc.contributor.author.fl_str_mv |
Bandeira, Raquel Duarte da Costa Cunha Uekane, Thais Matsue Cunha, Carolina Passos da Rodrigues, Janaína Marques Cruz, Marcus Henrique Campino de La Godoy, Ronoel Luiz de Oliveira Fioravante, Andreia de Lima |
| dc.subject.en.en.fl_str_mv |
HPLC-FLD LC-MS/MS Green Coffee Roasted Coffee Ochratoxins |
| topic |
HPLC-FLD LC-MS/MS Green Coffee Roasted Coffee Ochratoxins Cromatografia Líquida de Alta Pressão Espectrometria de Massas Café Roasted Coffee Ocratoxinas |
| dc.subject.decs.pt_BR.fl_str_mv |
Cromatografia Líquida de Alta Pressão Espectrometria de Massas Café Roasted Coffee Ocratoxinas |
| description |
Instituto Nacional de Metrologia, Qualidade e Tecnologia. Diretoria de Metrologia Cientifíca e Industrial. Divisão de Metrologia Química. Duque de Caxias, RJ, Brasil. |
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2013 |
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2013 |
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2014-10-17T18:58:19Z |
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2014-10-17T18:58:19Z |
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info:eu-repo/semantics/publishedVersion |
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info:eu-repo/semantics/article |
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BANDEIRA, R. D. C. C. et al. Comparison of High Performance Liquid Chromatography with Fluorescence Detector and with Tandem Mass Spectrometry methods for detection and quantification of Ochratoxin A in green and roasted coffee beans. Brazilian Archives of Biological Technology, Curitiba, v. 56, n. 6, p. 911-920. nov./dez. 2013. |
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https://www.arca.fiocruz.br/handle/icict/8625 |
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1516-8913 |
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http://dx.doi.org/10.1590/S1516-89132013000600004 |
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BANDEIRA, R. D. C. C. et al. Comparison of High Performance Liquid Chromatography with Fluorescence Detector and with Tandem Mass Spectrometry methods for detection and quantification of Ochratoxin A in green and roasted coffee beans. Brazilian Archives of Biological Technology, Curitiba, v. 56, n. 6, p. 911-920. nov./dez. 2013. 1516-8913 |
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https://www.arca.fiocruz.br/handle/icict/8625 http://dx.doi.org/10.1590/S1516-89132013000600004 |
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Instituto de Tecnologia do Paraná |
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Instituto de Tecnologia do Paraná |
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