Some triterpenic compounds in extracts of Cecropia and Bauhinia species for different sampling years.
Autor(a) principal: | |
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Data de Publicação: | 2018 |
Outros Autores: | , , , , |
Tipo de documento: | Artigo |
Idioma: | eng |
Título da fonte: | Repositório Institucional da EMBRAPA (Repository Open Access to Scientific Information from EMBRAPA - Alice) |
Texto Completo: | http://www.alice.cnptia.embrapa.br/alice/handle/doc/1087842 https://doi.org/10.1016/j.bjp.2017.11.005 |
Resumo: | The aim of this paper is to provide an overview on the chemical composition of triterpenes in widespreadused folk medicine species, through the development and validation of eleven compounds using HPLC-UV detection. The compounds were separated using isocratic elution, on a reverse phase column (KinetexC18, 250 mm × 4.6 mm, 5 m) with mobile phase consisted of acetonitrile:tetrahydrofuran (90:10, v/v),flow-rate of 0.5 ml/min and detection in 210 nm. Diverse validation parameters were successfully eval-uated. The samples of Bauhinia variegata L., B. variegata var. candida Voigt, Fabaceae, Cecropia palmataWilld. and C. obtusa Trécul, Urticaceae, collected in 2012, 2013 and 2014 from Amazon were treated withtwo different solvents (ethyl acetate and chloroform) and analyzed by the proposed method. Stigmas-terol, lupeol, -sitosterol, -amirin and -amirin were found in all the studied plants. Highlighting thepresence of oleanolic acid, maslinic acid in C. obtusa and C. palmata extracts, erythrodiol only in C. pal-mata, stigmasteol in B. variegata and -amirin in B. variegata var. candida. Overall, ethyl acetate showedbetter performance as the extractor solvent than chloroform. Moreover, it could be used for the qualitycontrol of medicinal plants and to assess potential marker compounds. |
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Some triterpenic compounds in extracts of Cecropia and Bauhinia species for different sampling years.Composição QuímicaPlanta MedicinalThe aim of this paper is to provide an overview on the chemical composition of triterpenes in widespreadused folk medicine species, through the development and validation of eleven compounds using HPLC-UV detection. The compounds were separated using isocratic elution, on a reverse phase column (KinetexC18, 250 mm × 4.6 mm, 5 m) with mobile phase consisted of acetonitrile:tetrahydrofuran (90:10, v/v),flow-rate of 0.5 ml/min and detection in 210 nm. Diverse validation parameters were successfully eval-uated. The samples of Bauhinia variegata L., B. variegata var. candida Voigt, Fabaceae, Cecropia palmataWilld. and C. obtusa Trécul, Urticaceae, collected in 2012, 2013 and 2014 from Amazon were treated withtwo different solvents (ethyl acetate and chloroform) and analyzed by the proposed method. Stigmas-terol, lupeol, -sitosterol, -amirin and -amirin were found in all the studied plants. Highlighting thepresence of oleanolic acid, maslinic acid in C. obtusa and C. palmata extracts, erythrodiol only in C. pal-mata, stigmasteol in B. variegata and -amirin in B. variegata var. candida. Overall, ethyl acetate showedbetter performance as the extractor solvent than chloroform. Moreover, it could be used for the qualitycontrol of medicinal plants and to assess potential marker compounds.Marcella Emilia Pietra Schmidt, PÓS-GRADUANDA UFSM; Fernanda Brum Pires, POS-GRADUANDA UFSM; Lucas Paines Bressan, PÓS-GRADUANDO UFSM; Fábio Vieira da Silva Junior, PÓS-GRADUANDO UFSM; OSMAR ALVES LAMEIRA, CPATU; Marcelo Barcellos da Rosa, PÓS-GRADUANDO UFSM.SCHMIDT, M. E. P.PIRES, F. B.BRESSAN, L. P.SILVA JUNIOR, F. V. daLAMEIRA, O. A.ROSA, M. B. da2018-02-20T00:35:50Z2018-02-20T00:35:50Z2018-02-1920182018-05-02T11:11:11Zinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/articleRevista Brasileira de Farmacognosia, v. 28, n. 1, p. 21-26, Jan./Feb. 2018.http://www.alice.cnptia.embrapa.br/alice/handle/doc/1087842https://doi.org/10.1016/j.bjp.2017.11.005enginfo:eu-repo/semantics/openAccessreponame:Repositório Institucional da EMBRAPA (Repository Open Access to Scientific Information from EMBRAPA - Alice)instname:Empresa Brasileira de Pesquisa Agropecuária (Embrapa)instacron:EMBRAPA2018-02-20T00:35:57Zoai:www.alice.cnptia.embrapa.br:doc/1087842Repositório InstitucionalPUBhttps://www.alice.cnptia.embrapa.br/oai/requestopendoar:21542018-02-20T00:35:57falseRepositório InstitucionalPUBhttps://www.alice.cnptia.embrapa.br/oai/requestcg-riaa@embrapa.bropendoar:21542018-02-20T00:35:57Repositório Institucional da EMBRAPA (Repository Open Access to Scientific Information from EMBRAPA - Alice) - Empresa Brasileira de Pesquisa Agropecuária (Embrapa)false |
dc.title.none.fl_str_mv |
Some triterpenic compounds in extracts of Cecropia and Bauhinia species for different sampling years. |
title |
Some triterpenic compounds in extracts of Cecropia and Bauhinia species for different sampling years. |
spellingShingle |
Some triterpenic compounds in extracts of Cecropia and Bauhinia species for different sampling years. SCHMIDT, M. E. P. Composição Química Planta Medicinal |
title_short |
Some triterpenic compounds in extracts of Cecropia and Bauhinia species for different sampling years. |
title_full |
Some triterpenic compounds in extracts of Cecropia and Bauhinia species for different sampling years. |
title_fullStr |
Some triterpenic compounds in extracts of Cecropia and Bauhinia species for different sampling years. |
title_full_unstemmed |
Some triterpenic compounds in extracts of Cecropia and Bauhinia species for different sampling years. |
title_sort |
Some triterpenic compounds in extracts of Cecropia and Bauhinia species for different sampling years. |
author |
SCHMIDT, M. E. P. |
author_facet |
SCHMIDT, M. E. P. PIRES, F. B. BRESSAN, L. P. SILVA JUNIOR, F. V. da LAMEIRA, O. A. ROSA, M. B. da |
author_role |
author |
author2 |
PIRES, F. B. BRESSAN, L. P. SILVA JUNIOR, F. V. da LAMEIRA, O. A. ROSA, M. B. da |
author2_role |
author author author author author |
dc.contributor.none.fl_str_mv |
Marcella Emilia Pietra Schmidt, PÓS-GRADUANDA UFSM; Fernanda Brum Pires, POS-GRADUANDA UFSM; Lucas Paines Bressan, PÓS-GRADUANDO UFSM; Fábio Vieira da Silva Junior, PÓS-GRADUANDO UFSM; OSMAR ALVES LAMEIRA, CPATU; Marcelo Barcellos da Rosa, PÓS-GRADUANDO UFSM. |
dc.contributor.author.fl_str_mv |
SCHMIDT, M. E. P. PIRES, F. B. BRESSAN, L. P. SILVA JUNIOR, F. V. da LAMEIRA, O. A. ROSA, M. B. da |
dc.subject.por.fl_str_mv |
Composição Química Planta Medicinal |
topic |
Composição Química Planta Medicinal |
description |
The aim of this paper is to provide an overview on the chemical composition of triterpenes in widespreadused folk medicine species, through the development and validation of eleven compounds using HPLC-UV detection. The compounds were separated using isocratic elution, on a reverse phase column (KinetexC18, 250 mm × 4.6 mm, 5 m) with mobile phase consisted of acetonitrile:tetrahydrofuran (90:10, v/v),flow-rate of 0.5 ml/min and detection in 210 nm. Diverse validation parameters were successfully eval-uated. The samples of Bauhinia variegata L., B. variegata var. candida Voigt, Fabaceae, Cecropia palmataWilld. and C. obtusa Trécul, Urticaceae, collected in 2012, 2013 and 2014 from Amazon were treated withtwo different solvents (ethyl acetate and chloroform) and analyzed by the proposed method. Stigmas-terol, lupeol, -sitosterol, -amirin and -amirin were found in all the studied plants. Highlighting thepresence of oleanolic acid, maslinic acid in C. obtusa and C. palmata extracts, erythrodiol only in C. pal-mata, stigmasteol in B. variegata and -amirin in B. variegata var. candida. Overall, ethyl acetate showedbetter performance as the extractor solvent than chloroform. Moreover, it could be used for the qualitycontrol of medicinal plants and to assess potential marker compounds. |
publishDate |
2018 |
dc.date.none.fl_str_mv |
2018-02-20T00:35:50Z 2018-02-20T00:35:50Z 2018-02-19 2018 2018-05-02T11:11:11Z |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/publishedVersion info:eu-repo/semantics/article |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
Revista Brasileira de Farmacognosia, v. 28, n. 1, p. 21-26, Jan./Feb. 2018. http://www.alice.cnptia.embrapa.br/alice/handle/doc/1087842 https://doi.org/10.1016/j.bjp.2017.11.005 |
identifier_str_mv |
Revista Brasileira de Farmacognosia, v. 28, n. 1, p. 21-26, Jan./Feb. 2018. |
url |
http://www.alice.cnptia.embrapa.br/alice/handle/doc/1087842 https://doi.org/10.1016/j.bjp.2017.11.005 |
dc.language.iso.fl_str_mv |
eng |
language |
eng |
dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess |
eu_rights_str_mv |
openAccess |
dc.source.none.fl_str_mv |
reponame:Repositório Institucional da EMBRAPA (Repository Open Access to Scientific Information from EMBRAPA - Alice) instname:Empresa Brasileira de Pesquisa Agropecuária (Embrapa) instacron:EMBRAPA |
instname_str |
Empresa Brasileira de Pesquisa Agropecuária (Embrapa) |
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EMBRAPA |
institution |
EMBRAPA |
reponame_str |
Repositório Institucional da EMBRAPA (Repository Open Access to Scientific Information from EMBRAPA - Alice) |
collection |
Repositório Institucional da EMBRAPA (Repository Open Access to Scientific Information from EMBRAPA - Alice) |
repository.name.fl_str_mv |
Repositório Institucional da EMBRAPA (Repository Open Access to Scientific Information from EMBRAPA - Alice) - Empresa Brasileira de Pesquisa Agropecuária (Embrapa) |
repository.mail.fl_str_mv |
cg-riaa@embrapa.br |
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1794503449829703680 |