Chemical constituents from the stem of Brosimum potabile (Moraceae)
Autor(a) principal: | |
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Data de Publicação: | 2010 |
Outros Autores: | , , , , , |
Tipo de documento: | Artigo |
Idioma: | eng |
Título da fonte: | Acta Amazonica |
Texto Completo: | http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0044-59672010000400011 |
Resumo: | Three coumarins, 5-methoxypsoralene, xanthyletin, and (-)-marmesin, have been isolated from the ethanolic extract of the stem of the Amazonian plant Brosimum potabile. The structures were determined on the basis of NMR analyses and by comparison with spectroscopic data in the literature. The analysis of the hexane fractions by GC-MS in EIMS mode suggested the presence of (1-methylpentyl)-benzene; α,α-dimethyl-4-(1-methylethyl)-benzenemethanol; 1-methyl-3,5-bis(1-methylethyl)-benzene; urs-12-ene; chola-5,22-dien-3β-ol; cholesta-4,6-dien-3β-ol; sitosteryl 9(Z)-octadecenoate; cholesta-5,22-dien-3β-ol; cholesta-4,6,22-trien-3-one; and cholesta-4,22-dien-3-one. NMR data of other hexane fractions indicated the presence of 3β-acetoxy-lup-12,20(29)-diene; 3β-acetoxy-olean-12-ene; 3β-acetoxy-urs-12-ene; and adian-5-ene. All these compounds are first described in B. potabile. |
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Chemical constituents from the stem of Brosimum potabile (Moraceae)Brosimum potabilecoumarinspentacyclic triterpenesstructural characterization by NMR and GC/MSThree coumarins, 5-methoxypsoralene, xanthyletin, and (-)-marmesin, have been isolated from the ethanolic extract of the stem of the Amazonian plant Brosimum potabile. The structures were determined on the basis of NMR analyses and by comparison with spectroscopic data in the literature. The analysis of the hexane fractions by GC-MS in EIMS mode suggested the presence of (1-methylpentyl)-benzene; α,α-dimethyl-4-(1-methylethyl)-benzenemethanol; 1-methyl-3,5-bis(1-methylethyl)-benzene; urs-12-ene; chola-5,22-dien-3β-ol; cholesta-4,6-dien-3β-ol; sitosteryl 9(Z)-octadecenoate; cholesta-5,22-dien-3β-ol; cholesta-4,6,22-trien-3-one; and cholesta-4,22-dien-3-one. NMR data of other hexane fractions indicated the presence of 3β-acetoxy-lup-12,20(29)-diene; 3β-acetoxy-olean-12-ene; 3β-acetoxy-urs-12-ene; and adian-5-ene. All these compounds are first described in B. potabile.Instituto Nacional de Pesquisas da Amazônia2010-12-01info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersiontext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S0044-59672010000400011Acta Amazonica v.40 n.4 2010reponame:Acta Amazonicainstname:Instituto Nacional de Pesquisas da Amazônia (INPA)instacron:INPA10.1590/S0044-59672010000400011info:eu-repo/semantics/openAccessAbreu,Viviane Gomes da CostaSilva,Marilda Conceição daMagalhães,Rozângela ManfriniPiló-Veloso,DorilaXavier,Izelene Felício da SilvaOliveira,Patrícia MachadoAlcântra,Antônio Flávio de Carvalhoeng2011-01-03T00:00:00Zoai:scielo:S0044-59672010000400011Revistahttps://acta.inpa.gov.br/PUBhttps://old.scielo.br/oai/scielo-oai.phpacta@inpa.gov.br||acta@inpa.gov.br1809-43920044-5967opendoar:2011-01-03T00:00Acta Amazonica - Instituto Nacional de Pesquisas da Amazônia (INPA)false |
dc.title.none.fl_str_mv |
Chemical constituents from the stem of Brosimum potabile (Moraceae) |
title |
Chemical constituents from the stem of Brosimum potabile (Moraceae) |
spellingShingle |
Chemical constituents from the stem of Brosimum potabile (Moraceae) Abreu,Viviane Gomes da Costa Brosimum potabile coumarins pentacyclic triterpenes structural characterization by NMR and GC/MS |
title_short |
Chemical constituents from the stem of Brosimum potabile (Moraceae) |
title_full |
Chemical constituents from the stem of Brosimum potabile (Moraceae) |
title_fullStr |
Chemical constituents from the stem of Brosimum potabile (Moraceae) |
title_full_unstemmed |
Chemical constituents from the stem of Brosimum potabile (Moraceae) |
title_sort |
Chemical constituents from the stem of Brosimum potabile (Moraceae) |
author |
Abreu,Viviane Gomes da Costa |
author_facet |
Abreu,Viviane Gomes da Costa Silva,Marilda Conceição da Magalhães,Rozângela Manfrini Piló-Veloso,Dorila Xavier,Izelene Felício da Silva Oliveira,Patrícia Machado Alcântra,Antônio Flávio de Carvalho |
author_role |
author |
author2 |
Silva,Marilda Conceição da Magalhães,Rozângela Manfrini Piló-Veloso,Dorila Xavier,Izelene Felício da Silva Oliveira,Patrícia Machado Alcântra,Antônio Flávio de Carvalho |
author2_role |
author author author author author author |
dc.contributor.author.fl_str_mv |
Abreu,Viviane Gomes da Costa Silva,Marilda Conceição da Magalhães,Rozângela Manfrini Piló-Veloso,Dorila Xavier,Izelene Felício da Silva Oliveira,Patrícia Machado Alcântra,Antônio Flávio de Carvalho |
dc.subject.por.fl_str_mv |
Brosimum potabile coumarins pentacyclic triterpenes structural characterization by NMR and GC/MS |
topic |
Brosimum potabile coumarins pentacyclic triterpenes structural characterization by NMR and GC/MS |
description |
Three coumarins, 5-methoxypsoralene, xanthyletin, and (-)-marmesin, have been isolated from the ethanolic extract of the stem of the Amazonian plant Brosimum potabile. The structures were determined on the basis of NMR analyses and by comparison with spectroscopic data in the literature. The analysis of the hexane fractions by GC-MS in EIMS mode suggested the presence of (1-methylpentyl)-benzene; α,α-dimethyl-4-(1-methylethyl)-benzenemethanol; 1-methyl-3,5-bis(1-methylethyl)-benzene; urs-12-ene; chola-5,22-dien-3β-ol; cholesta-4,6-dien-3β-ol; sitosteryl 9(Z)-octadecenoate; cholesta-5,22-dien-3β-ol; cholesta-4,6,22-trien-3-one; and cholesta-4,22-dien-3-one. NMR data of other hexane fractions indicated the presence of 3β-acetoxy-lup-12,20(29)-diene; 3β-acetoxy-olean-12-ene; 3β-acetoxy-urs-12-ene; and adian-5-ene. All these compounds are first described in B. potabile. |
publishDate |
2010 |
dc.date.none.fl_str_mv |
2010-12-01 |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0044-59672010000400011 |
url |
http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0044-59672010000400011 |
dc.language.iso.fl_str_mv |
eng |
language |
eng |
dc.relation.none.fl_str_mv |
10.1590/S0044-59672010000400011 |
dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess |
eu_rights_str_mv |
openAccess |
dc.format.none.fl_str_mv |
text/html |
dc.publisher.none.fl_str_mv |
Instituto Nacional de Pesquisas da Amazônia |
publisher.none.fl_str_mv |
Instituto Nacional de Pesquisas da Amazônia |
dc.source.none.fl_str_mv |
Acta Amazonica v.40 n.4 2010 reponame:Acta Amazonica instname:Instituto Nacional de Pesquisas da Amazônia (INPA) instacron:INPA |
instname_str |
Instituto Nacional de Pesquisas da Amazônia (INPA) |
instacron_str |
INPA |
institution |
INPA |
reponame_str |
Acta Amazonica |
collection |
Acta Amazonica |
repository.name.fl_str_mv |
Acta Amazonica - Instituto Nacional de Pesquisas da Amazônia (INPA) |
repository.mail.fl_str_mv |
acta@inpa.gov.br||acta@inpa.gov.br |
_version_ |
1752129838990229504 |