Analysis of the microstructural evolution of composite of Tungsten with lignin kraft

Detalhes bibliográficos
Autor(a) principal: SOUZA, A.C.
Data de Publicação: 2020
Outros Autores: ROSSI, J.L., FERNANDES, H.B., GOUVEA, A.F.G., ENCONTRO CIENT??FICO DE F??SICA APLICADA, 8.
Tipo de documento: Artigo de conferência
Título da fonte: Repositório Institucional do IPEN
Texto Completo: http://repositorio.ipen.br/handle/123456789/31218
Resumo: In materials science and engineering, there is a demand in new materials for radiation shielding in the transport of radiopharmaceuticals used in the diagnosis and therapy of cancer, justifying the interest in developing this work. The obtained lignin kraft and tungsten form the precursors used for metal-organic composite. Tungsten metal has diverse applications in the nuclear sector presents an enormous mechanical strength and an excellent cross section with thermal neutrons. The aim of this study is to analyse the microstructural evolution of metal-organic composite using the kraft lignin and tungsten, using analysis of scanning electron microscopy (SEM), microhardness test and x-ray diffraction (XRD). Microscopic analysis showed the granulometry of the precursors separate and composite morphology, observing the formation of alpha (??) and beta (??) phases and absence of oxidation process for different heat treatment temperatures. The spectra of x-ray diffraction identified the structures of each phase formed and micro hardness measures showed an increase of mechanical resistance with temperature. The results of the microstructural characterization of metal-organic composite, will contribute in the next steps of attenuation measurements of gamma radiation.
id IPEN_36aa5ba5b4bb78fd97a98cc1f5279f4b
oai_identifier_str oai:repositorio.ipen.br:123456789/31218
network_acronym_str IPEN
network_name_str Repositório Institucional do IPEN
repository_id_str 4510
spelling 2020-06-01T14:16:22Z2020-06-01T14:16:22Z4-7 de setembro, 2017http://repositorio.ipen.br/handle/123456789/3121810.5151/phypro-viii-efa-190000-0002-8304-9939In materials science and engineering, there is a demand in new materials for radiation shielding in the transport of radiopharmaceuticals used in the diagnosis and therapy of cancer, justifying the interest in developing this work. The obtained lignin kraft and tungsten form the precursors used for metal-organic composite. Tungsten metal has diverse applications in the nuclear sector presents an enormous mechanical strength and an excellent cross section with thermal neutrons. The aim of this study is to analyse the microstructural evolution of metal-organic composite using the kraft lignin and tungsten, using analysis of scanning electron microscopy (SEM), microhardness test and x-ray diffraction (XRD). Microscopic analysis showed the granulometry of the precursors separate and composite morphology, observing the formation of alpha (??) and beta (??) phases and absence of oxidation process for different heat treatment temperatures. The spectra of x-ray diffraction identified the structures of each phase formed and micro hardness measures showed an increase of mechanical resistance with temperature. The results of the microstructural characterization of metal-organic composite, will contribute in the next steps of attenuation measurements of gamma radiation.Submitted by Pedro Silva Filho (pfsilva@ipen.br) on 2020-06-01T14:16:22Z No. of bitstreams: 1 26997.pdf: 571982 bytes, checksum: d19da1f189e5dd3000f713b47f975675 (MD5)Made available in DSpace on 2020-06-01T14:16:22Z (GMT). No. of bitstreams: 1 26997.pdf: 571982 bytes, checksum: d19da1f189e5dd3000f713b47f975675 (MD5)76-78Blucher ProceedingsAnalysis of the microstructural evolution of composite of Tungsten with lignin kraftinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/conferenceObjectECFANS??o Paulo, SPVit??ria, ES502600SOUZA, A.C.ROSSI, J.L.FERNANDES, H.B.GOUVEA, A.F.G.ENCONTRO CIENT??FICO DE F??SICA APLICADA, 8.info:eu-repo/semantics/openAccessreponame:Repositório Institucional do IPENinstname:Instituto de Pesquisas Energéticas e Nucleares (IPEN)instacron:IPEN269972017ROSSI, J.L.20-06Anais502ROSSI, J.L.:502:730:NORIGINAL26997.pdf26997.pdfapplication/pdf571982http://repositorio.ipen.br/bitstream/123456789/31218/1/26997.pdfd19da1f189e5dd3000f713b47f975675MD51LICENSElicense.txtlicense.txttext/plain; charset=utf-81748http://repositorio.ipen.br/bitstream/123456789/31218/2/license.txt8a4605be74aa9ea9d79846c1fba20a33MD52123456789/312182020-06-01 14:16:22.238oai:repositorio.ipen.br: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Repositório InstitucionalPUBhttp://repositorio.ipen.br/oai/requestbibl@ipen.bropendoar:45102020-06-01T14:16:22Repositório Institucional do IPEN - Instituto de Pesquisas Energéticas e Nucleares (IPEN)false
dc.title.pt_BR.fl_str_mv Analysis of the microstructural evolution of composite of Tungsten with lignin kraft
title Analysis of the microstructural evolution of composite of Tungsten with lignin kraft
spellingShingle Analysis of the microstructural evolution of composite of Tungsten with lignin kraft
SOUZA, A.C.
title_short Analysis of the microstructural evolution of composite of Tungsten with lignin kraft
title_full Analysis of the microstructural evolution of composite of Tungsten with lignin kraft
title_fullStr Analysis of the microstructural evolution of composite of Tungsten with lignin kraft
title_full_unstemmed Analysis of the microstructural evolution of composite of Tungsten with lignin kraft
title_sort Analysis of the microstructural evolution of composite of Tungsten with lignin kraft
author SOUZA, A.C.
author_facet SOUZA, A.C.
ROSSI, J.L.
FERNANDES, H.B.
GOUVEA, A.F.G.
ENCONTRO CIENT??FICO DE F??SICA APLICADA, 8.
author_role author
author2 ROSSI, J.L.
FERNANDES, H.B.
GOUVEA, A.F.G.
ENCONTRO CIENT??FICO DE F??SICA APLICADA, 8.
author2_role author
author
author
author
dc.contributor.author.fl_str_mv SOUZA, A.C.
ROSSI, J.L.
FERNANDES, H.B.
GOUVEA, A.F.G.
ENCONTRO CIENT??FICO DE F??SICA APLICADA, 8.
description In materials science and engineering, there is a demand in new materials for radiation shielding in the transport of radiopharmaceuticals used in the diagnosis and therapy of cancer, justifying the interest in developing this work. The obtained lignin kraft and tungsten form the precursors used for metal-organic composite. Tungsten metal has diverse applications in the nuclear sector presents an enormous mechanical strength and an excellent cross section with thermal neutrons. The aim of this study is to analyse the microstructural evolution of metal-organic composite using the kraft lignin and tungsten, using analysis of scanning electron microscopy (SEM), microhardness test and x-ray diffraction (XRD). Microscopic analysis showed the granulometry of the precursors separate and composite morphology, observing the formation of alpha (??) and beta (??) phases and absence of oxidation process for different heat treatment temperatures. The spectra of x-ray diffraction identified the structures of each phase formed and micro hardness measures showed an increase of mechanical resistance with temperature. The results of the microstructural characterization of metal-organic composite, will contribute in the next steps of attenuation measurements of gamma radiation.
publishDate 2020
dc.date.evento.pt_BR.fl_str_mv 4-7 de setembro, 2017
dc.date.accessioned.fl_str_mv 2020-06-01T14:16:22Z
dc.date.available.fl_str_mv 2020-06-01T14:16:22Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/conferenceObject
format conferenceObject
status_str publishedVersion
dc.identifier.uri.fl_str_mv http://repositorio.ipen.br/handle/123456789/31218
dc.identifier.doi.pt_BR.fl_str_mv 10.5151/phypro-viii-efa-19
dc.identifier.orcid.pt_BR.fl_str_mv 0000-0002-8304-9939
url http://repositorio.ipen.br/handle/123456789/31218
identifier_str_mv 10.5151/phypro-viii-efa-19
0000-0002-8304-9939
dc.relation.authority.fl_str_mv 502
dc.relation.confidence.fl_str_mv 600
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv 76-78
dc.coverage.pt_BR.fl_str_mv N
dc.publisher.none.fl_str_mv Blucher Proceedings
publisher.none.fl_str_mv Blucher Proceedings
dc.source.none.fl_str_mv reponame:Repositório Institucional do IPEN
instname:Instituto de Pesquisas Energéticas e Nucleares (IPEN)
instacron:IPEN
instname_str Instituto de Pesquisas Energéticas e Nucleares (IPEN)
instacron_str IPEN
institution IPEN
reponame_str Repositório Institucional do IPEN
collection Repositório Institucional do IPEN
bitstream.url.fl_str_mv http://repositorio.ipen.br/bitstream/123456789/31218/1/26997.pdf
http://repositorio.ipen.br/bitstream/123456789/31218/2/license.txt
bitstream.checksum.fl_str_mv d19da1f189e5dd3000f713b47f975675
8a4605be74aa9ea9d79846c1fba20a33
bitstream.checksumAlgorithm.fl_str_mv MD5
MD5
repository.name.fl_str_mv Repositório Institucional do IPEN - Instituto de Pesquisas Energéticas e Nucleares (IPEN)
repository.mail.fl_str_mv bibl@ipen.br
_version_ 1767254252041797632