Synthesis and characterization of TiO2 films obtained by sol-gel method
Main Author: | |
---|---|
Publication Date: | 2018 |
Other Authors: | , , , , |
Format: | Conference object |
Source: | Repositório Institucional do IPEN |
Download full: | http://repositorio.ipen.br/handle/123456789/29216 |
Summary: | Borosilicate coated titanium dioxide thin films were produced by the sol-gel method. The films were calcinated at 450??C for 20 minutes for crystalization. X-ray diffration analyses show that before the heat treatment the film was amorphous and after that it crystallized in anatase phase presenting mean grain size of 34 nm and RMS roughness of 8 nm. The crystallized film was used as photocatalist in the degradation of methyl orange dye presenting an efficiency of 25% after 2h under UV light. |
id |
IPEN_7ecf8c387ead5d18e609f4a8abc9b267 |
---|---|
oai_identifier_str |
oai:repositorio.ipen.br:123456789/29216 |
network_acronym_str |
IPEN |
network_name_str |
Repositório Institucional do IPEN |
repository_id_str |
4510 |
spelling |
2018-09-27T13:00:08Z2018-09-27T13:00:08ZNovember 27-30, 2017http://repositorio.ipen.br/handle/123456789/29216Borosilicate coated titanium dioxide thin films were produced by the sol-gel method. The films were calcinated at 450??C for 20 minutes for crystalization. X-ray diffration analyses show that before the heat treatment the film was amorphous and after that it crystallized in anatase phase presenting mean grain size of 34 nm and RMS roughness of 8 nm. The crystallized film was used as photocatalist in the degradation of methyl orange dye presenting an efficiency of 25% after 2h under UV light.Submitted by Marco Antonio Oliveira da Silva (maosilva@ipen.br) on 2018-09-27T13:00:08Z No. of bitstreams: 1 25005.pdf: 1077975 bytes, checksum: 8c71aa2e969dd56540fa23b68c7d2c19 (MD5)Made available in DSpace on 2018-09-27T13:00:08Z (GMT). No. of bitstreams: 1 25005.pdf: 1077975 bytes, checksum: 8c71aa2e969dd56540fa23b68c7d2c19 (MD5)Synthesis and characterization of TiO2 films obtained by sol-gel methodinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/conferenceObjectPANNANOIGuaruj??, SPSZURKALO, MARGARIDAOLIVEIRA, EDUARDO C. deCORREA, OLANDIR V.BENTO, RODRIGO T.PILLIS, MARINA F.PAN AMERICAN CONGRESS OF NANOTECHNOLOGY, 1stinfo:eu-repo/semantics/openAccessreponame:Repositório Institucional do IPENinstname:Instituto de Pesquisas Energéticas e Nucleares (IPEN)instacron:IPEN250052017SZURKALO, MARGARIDAOLIVEIRA, EDUARDO C. deCORREA, OLANDIR V.BENTO, RODRIGO T.PILLIS, MARINA F.18-09Proceedings60391459148814417758SZURKALO, MARGARIDA:6039:730:SOLIVEIRA, EDUARDO C. DE:14591:730:NCORREA, OLANDIR V.:488:730:NBENTO, RODRIGO T.:14417:730:NPILLIS, MARINA F.:758:730:NORIGINAL25005.pdf25005.pdfapplication/pdf1077975http://repositorio.ipen.br/bitstream/123456789/29216/1/25005.pdf8c71aa2e969dd56540fa23b68c7d2c19MD51LICENSElicense.txtlicense.txttext/plain; charset=utf-81748http://repositorio.ipen.br/bitstream/123456789/29216/2/license.txt8a4605be74aa9ea9d79846c1fba20a33MD52123456789/292162018-09-27 13:00:08.526oai:repositorio.ipen.br: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Repositório InstitucionalPUBhttp://repositorio.ipen.br/oai/requestbibl@ipen.bropendoar:45102018-09-27T13:00:08Repositório Institucional do IPEN - Instituto de Pesquisas Energéticas e Nucleares (IPEN)false |
dc.title.pt_BR.fl_str_mv |
Synthesis and characterization of TiO2 films obtained by sol-gel method |
title |
Synthesis and characterization of TiO2 films obtained by sol-gel method |
spellingShingle |
Synthesis and characterization of TiO2 films obtained by sol-gel method SZURKALO, MARGARIDA |
title_short |
Synthesis and characterization of TiO2 films obtained by sol-gel method |
title_full |
Synthesis and characterization of TiO2 films obtained by sol-gel method |
title_fullStr |
Synthesis and characterization of TiO2 films obtained by sol-gel method |
title_full_unstemmed |
Synthesis and characterization of TiO2 films obtained by sol-gel method |
title_sort |
Synthesis and characterization of TiO2 films obtained by sol-gel method |
author |
SZURKALO, MARGARIDA |
author_facet |
SZURKALO, MARGARIDA OLIVEIRA, EDUARDO C. de CORREA, OLANDIR V. BENTO, RODRIGO T. PILLIS, MARINA F. PAN AMERICAN CONGRESS OF NANOTECHNOLOGY, 1st |
author_role |
author |
author2 |
OLIVEIRA, EDUARDO C. de CORREA, OLANDIR V. BENTO, RODRIGO T. PILLIS, MARINA F. PAN AMERICAN CONGRESS OF NANOTECHNOLOGY, 1st |
author2_role |
author author author author author |
dc.contributor.author.fl_str_mv |
SZURKALO, MARGARIDA OLIVEIRA, EDUARDO C. de CORREA, OLANDIR V. BENTO, RODRIGO T. PILLIS, MARINA F. PAN AMERICAN CONGRESS OF NANOTECHNOLOGY, 1st |
description |
Borosilicate coated titanium dioxide thin films were produced by the sol-gel method. The films were calcinated at 450??C for 20 minutes for crystalization. X-ray diffration analyses show that before the heat treatment the film was amorphous and after that it crystallized in anatase phase presenting mean grain size of 34 nm and RMS roughness of 8 nm. The crystallized film was used as photocatalist in the degradation of methyl orange dye presenting an efficiency of 25% after 2h under UV light. |
publishDate |
2018 |
dc.date.evento.pt_BR.fl_str_mv |
November 27-30, 2017 |
dc.date.accessioned.fl_str_mv |
2018-09-27T13:00:08Z |
dc.date.available.fl_str_mv |
2018-09-27T13:00:08Z |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/conferenceObject |
format |
conferenceObject |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
http://repositorio.ipen.br/handle/123456789/29216 |
url |
http://repositorio.ipen.br/handle/123456789/29216 |
dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess |
eu_rights_str_mv |
openAccess |
dc.coverage.pt_BR.fl_str_mv |
I |
dc.source.none.fl_str_mv |
reponame:Repositório Institucional do IPEN instname:Instituto de Pesquisas Energéticas e Nucleares (IPEN) instacron:IPEN |
instname_str |
Instituto de Pesquisas Energéticas e Nucleares (IPEN) |
instacron_str |
IPEN |
institution |
IPEN |
reponame_str |
Repositório Institucional do IPEN |
collection |
Repositório Institucional do IPEN |
bitstream.url.fl_str_mv |
http://repositorio.ipen.br/bitstream/123456789/29216/1/25005.pdf http://repositorio.ipen.br/bitstream/123456789/29216/2/license.txt |
bitstream.checksum.fl_str_mv |
8c71aa2e969dd56540fa23b68c7d2c19 8a4605be74aa9ea9d79846c1fba20a33 |
bitstream.checksumAlgorithm.fl_str_mv |
MD5 MD5 |
repository.name.fl_str_mv |
Repositório Institucional do IPEN - Instituto de Pesquisas Energéticas e Nucleares (IPEN) |
repository.mail.fl_str_mv |
bibl@ipen.br |
_version_ |
1767254246082740224 |