A??a?? oil as an alternative in the synthesis and coating of iron oxide nanoparticles
Autor(a) principal: | |
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Data de Publicação: | 2020 |
Outros Autores: | , , , , , , |
Tipo de documento: | Artigo de conferência |
Título da fonte: | Repositório Institucional do IPEN |
Texto Completo: | http://repositorio.ipen.br/handle/123456789/30632 |
Resumo: | In the last decades, nanotechnology studies have attracted the attention of researchers from various fields, engineering, chemistry, physics, medicine, environment. Medicine, nanomedicine, the major advances in the diagnosis and therapies of diseases, such as magnetic resonance imaging and the treatment of cancer by hyperthermia, respectively. Nanomaterials for such biomedical applications should have size control of less than 20 nm, crystal structure and well-defined morphology. Thus, as nanoparticles of iron oxide (Fe3O4) is one of the materials most studied for such applications. Thus, iron oxide nanoparticles were synthesized by variation of the thermal decomposition method, which is described as one of the best quality nanoparticle synthesis tools. During the synthesis, we used a??a?? oil, rich in fatty acids, palmitoleic, linoleic and palmitic, as a process of synthesis and coating of nanoparticles, making them biocompatible. The a??a?? oil was made by the supercritical extraction method, where the product can be obtained pure, free of solvents. The samples were characterized by X-ray diffraction (XRD) and the magnetite phase (Fe3O4) was identify through the position of the intensity peaks. The nanoparticles present spherical morphology with a diameter of 3 to 10 nm, observed through transmission electron microscopy (TEM) images. In addition, neutron analysis (NAA) determined that the samples had a concentration of 74.93% Fe3O4 and a remaining database is related to the coating of sample nanoparticles as potentiated for biomedical applications. |
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2020-01-10T18:21:42Z2020-01-10T18:21:42ZOctober 21-25, 2019http://repositorio.ipen.br/handle/123456789/306320000-0003-2197-35920000-0002-4499-5949In the last decades, nanotechnology studies have attracted the attention of researchers from various fields, engineering, chemistry, physics, medicine, environment. Medicine, nanomedicine, the major advances in the diagnosis and therapies of diseases, such as magnetic resonance imaging and the treatment of cancer by hyperthermia, respectively. Nanomaterials for such biomedical applications should have size control of less than 20 nm, crystal structure and well-defined morphology. Thus, as nanoparticles of iron oxide (Fe3O4) is one of the materials most studied for such applications. Thus, iron oxide nanoparticles were synthesized by variation of the thermal decomposition method, which is described as one of the best quality nanoparticle synthesis tools. During the synthesis, we used a??a?? oil, rich in fatty acids, palmitoleic, linoleic and palmitic, as a process of synthesis and coating of nanoparticles, making them biocompatible. The a??a?? oil was made by the supercritical extraction method, where the product can be obtained pure, free of solvents. The samples were characterized by X-ray diffraction (XRD) and the magnetite phase (Fe3O4) was identify through the position of the intensity peaks. The nanoparticles present spherical morphology with a diameter of 3 to 10 nm, observed through transmission electron microscopy (TEM) images. In addition, neutron analysis (NAA) determined that the samples had a concentration of 74.93% Fe3O4 and a remaining database is related to the coating of sample nanoparticles as potentiated for biomedical applications.Submitted by Celia Satomi Uehara (celia.u-topservice@ipen.br) on 2020-01-10T18:21:42Z No. of bitstreams: 1 26281.pdf: 278567 bytes, checksum: 00d7f07b6bffb821e79e9ca85424438e (MD5)Made available in DSpace on 2020-01-10T18:21:42Z (GMT). No. of bitstreams: 1 26281.pdf: 278567 bytes, checksum: 00d7f07b6bffb821e79e9ca85424438e (MD5)2437-2442Associa????o Brasileira de Energia Nuclearbiologycoatingsconcentration ratiograin sizeiron oxidesmedicinemorphologynanoparticlesneutron activation analysistransmission electron microscopyvegetable oilsA??a?? oil as an alternative in the synthesis and coating of iron oxide nanoparticlesinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/conferenceObjectINACIRio de JaneiroSantos, SP14371178600600PAES, SUANE C.CORREA, BRUNO S.SENA, CLEIDILANECOSTA, MESSIAS S.CABRERA-PASCA, GABRIEL A.CARBONARI, ARTUR W.SAIKI, MITIKOINTERNATIONAL NUCLEAR ATLANTIC CONFERENCEinfo:eu-repo/semantics/openAccessreponame:Repositório Institucional do IPENinstname:Instituto de Pesquisas Energéticas e Nucleares (IPEN)instacron:IPEN262812019SAIKI, MITIKOCARBONARI, ARTUR W.CORREA, BRUNO S.20-01Proceedings1178143715164SAIKI, MITIKO:1178:320:NCARBONARI, ARTUR W.:1437:310:NCORREA, BRUNO S.:15164:-1:NORIGINAL26281.pdf26281.pdfapplication/pdf278567http://repositorio.ipen.br/bitstream/123456789/30632/1/26281.pdf00d7f07b6bffb821e79e9ca85424438eMD51LICENSElicense.txtlicense.txttext/plain; charset=utf-81748http://repositorio.ipen.br/bitstream/123456789/30632/2/license.txt8a4605be74aa9ea9d79846c1fba20a33MD52123456789/306322022-05-30 19:18:52.735oai:repositorio.ipen.br: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Repositório InstitucionalPUBhttp://repositorio.ipen.br/oai/requestbibl@ipen.bropendoar:45102022-05-30T19:18:52Repositório Institucional do IPEN - Instituto de Pesquisas Energéticas e Nucleares (IPEN)false |
dc.title.pt_BR.fl_str_mv |
A??a?? oil as an alternative in the synthesis and coating of iron oxide nanoparticles |
title |
A??a?? oil as an alternative in the synthesis and coating of iron oxide nanoparticles |
spellingShingle |
A??a?? oil as an alternative in the synthesis and coating of iron oxide nanoparticles PAES, SUANE C. biology coatings concentration ratio grain size iron oxides medicine morphology nanoparticles neutron activation analysis transmission electron microscopy vegetable oils |
title_short |
A??a?? oil as an alternative in the synthesis and coating of iron oxide nanoparticles |
title_full |
A??a?? oil as an alternative in the synthesis and coating of iron oxide nanoparticles |
title_fullStr |
A??a?? oil as an alternative in the synthesis and coating of iron oxide nanoparticles |
title_full_unstemmed |
A??a?? oil as an alternative in the synthesis and coating of iron oxide nanoparticles |
title_sort |
A??a?? oil as an alternative in the synthesis and coating of iron oxide nanoparticles |
author |
PAES, SUANE C. |
author_facet |
PAES, SUANE C. CORREA, BRUNO S. SENA, CLEIDILANE COSTA, MESSIAS S. CABRERA-PASCA, GABRIEL A. CARBONARI, ARTUR W. SAIKI, MITIKO INTERNATIONAL NUCLEAR ATLANTIC CONFERENCE |
author_role |
author |
author2 |
CORREA, BRUNO S. SENA, CLEIDILANE COSTA, MESSIAS S. CABRERA-PASCA, GABRIEL A. CARBONARI, ARTUR W. SAIKI, MITIKO INTERNATIONAL NUCLEAR ATLANTIC CONFERENCE |
author2_role |
author author author author author author author |
dc.contributor.author.fl_str_mv |
PAES, SUANE C. CORREA, BRUNO S. SENA, CLEIDILANE COSTA, MESSIAS S. CABRERA-PASCA, GABRIEL A. CARBONARI, ARTUR W. SAIKI, MITIKO INTERNATIONAL NUCLEAR ATLANTIC CONFERENCE |
dc.subject.por.fl_str_mv |
biology coatings concentration ratio grain size iron oxides medicine morphology nanoparticles neutron activation analysis transmission electron microscopy vegetable oils |
topic |
biology coatings concentration ratio grain size iron oxides medicine morphology nanoparticles neutron activation analysis transmission electron microscopy vegetable oils |
description |
In the last decades, nanotechnology studies have attracted the attention of researchers from various fields, engineering, chemistry, physics, medicine, environment. Medicine, nanomedicine, the major advances in the diagnosis and therapies of diseases, such as magnetic resonance imaging and the treatment of cancer by hyperthermia, respectively. Nanomaterials for such biomedical applications should have size control of less than 20 nm, crystal structure and well-defined morphology. Thus, as nanoparticles of iron oxide (Fe3O4) is one of the materials most studied for such applications. Thus, iron oxide nanoparticles were synthesized by variation of the thermal decomposition method, which is described as one of the best quality nanoparticle synthesis tools. During the synthesis, we used a??a?? oil, rich in fatty acids, palmitoleic, linoleic and palmitic, as a process of synthesis and coating of nanoparticles, making them biocompatible. The a??a?? oil was made by the supercritical extraction method, where the product can be obtained pure, free of solvents. The samples were characterized by X-ray diffraction (XRD) and the magnetite phase (Fe3O4) was identify through the position of the intensity peaks. The nanoparticles present spherical morphology with a diameter of 3 to 10 nm, observed through transmission electron microscopy (TEM) images. In addition, neutron analysis (NAA) determined that the samples had a concentration of 74.93% Fe3O4 and a remaining database is related to the coating of sample nanoparticles as potentiated for biomedical applications. |
publishDate |
2020 |
dc.date.evento.pt_BR.fl_str_mv |
October 21-25, 2019 |
dc.date.accessioned.fl_str_mv |
2020-01-10T18:21:42Z |
dc.date.available.fl_str_mv |
2020-01-10T18:21:42Z |
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