Análise das viabilidades da obtenção de um biofilme a partir do colágeno de frango
Autor(a) principal: | |
---|---|
Data de Publicação: | 2018 |
Tipo de documento: | Dissertação |
Idioma: | por |
Título da fonte: | Biblioteca Digital de Teses e Dissertações da Uninove |
Texto Completo: | http://bibliotecatede.uninove.br/handle/tede/1947 |
Resumo: | The present work aims to analyze the feasibility of obtaining a biofilm from the extraction of collagen from the feet of chicken. In this sense, a factorial design varying the acetic acid concentration, time and temperature of the collagen extraction was used. The optimization of the system was done by response surface analysis with a confidence level of 95% using the ANOVA methodology. After obtaining the collagen, the films were made from a solution of chicken collagen with glycerin or propylene glycol. Biofilms were tested for swelling and water vapor transmission to assure quality and evaluate the prospects for degradation and degree of hydration. It was also evaluated the cost value of raw materials for the production of a pack with 12 units of these biofilms. The dried and pulverized material was found to have a yellow coloration and a composition of more than 78% protein. The extraction yield varied from 1.7 to 8.5% of collagen on the initial mass of the chicken feet and the optimization showed that it is possible to obtain yields above 8.0% when using the acetic acid concentration between 3,000 and 3.682%, the operating time between 1 and 3h and the temperature between 70 and 76.82 ° C. The results of swelling and water vapor transmission tests ensured the quality of products with respect to degradation and degree of hydration. The cost analysis showed that in order to produce a package with 12 biofilm units, the cost of raw material involved was R $ 0.04 (US $ 0.01) and that methylparaben accounted for 75% of the costs, followed by plasticizer (glycerine and / or propylene glycol) with approximately 20% of the total cost of the formulation. Thus, this work demonstrated that biofilms produced from chicken collagen are technically and economically viable. |
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Santana, José Carlos CurveloSantana, José Carlos CurveloSouza, Roberto Rodrigues deBerssaneti, Fernando Tobalhttp://lattes.cnpq.br/1864225011246309Gardim, Roberta Bezerra2018-12-27T18:39:42Z2018-09-27Gardim, Roberta Bezerra. Análise das viabilidades da obtenção de um biofilme a partir do colágeno de frango. 2018. 85 f. Dissertação( Programa de Mestrado em Engenharia de Produção) - Universidade Nove de Julho, São Paulo.http://bibliotecatede.uninove.br/handle/tede/1947The present work aims to analyze the feasibility of obtaining a biofilm from the extraction of collagen from the feet of chicken. In this sense, a factorial design varying the acetic acid concentration, time and temperature of the collagen extraction was used. The optimization of the system was done by response surface analysis with a confidence level of 95% using the ANOVA methodology. After obtaining the collagen, the films were made from a solution of chicken collagen with glycerin or propylene glycol. Biofilms were tested for swelling and water vapor transmission to assure quality and evaluate the prospects for degradation and degree of hydration. It was also evaluated the cost value of raw materials for the production of a pack with 12 units of these biofilms. The dried and pulverized material was found to have a yellow coloration and a composition of more than 78% protein. The extraction yield varied from 1.7 to 8.5% of collagen on the initial mass of the chicken feet and the optimization showed that it is possible to obtain yields above 8.0% when using the acetic acid concentration between 3,000 and 3.682%, the operating time between 1 and 3h and the temperature between 70 and 76.82 ° C. The results of swelling and water vapor transmission tests ensured the quality of products with respect to degradation and degree of hydration. The cost analysis showed that in order to produce a package with 12 biofilm units, the cost of raw material involved was R $ 0.04 (US $ 0.01) and that methylparaben accounted for 75% of the costs, followed by plasticizer (glycerine and / or propylene glycol) with approximately 20% of the total cost of the formulation. Thus, this work demonstrated that biofilms produced from chicken collagen are technically and economically viable.O presente trabalho visa analisar as viabilidades da obtenção de um biofilme a partir da extração do colágeno dos pés de frango. Neste sentido, um planejamento fatorial variando a concentração do ácido acético, tempo e temperatura de extração do colágeno foi utilizado. A otimização do sistema foi feita por análise de superfície de resposta com grau de confiança de 95% pela metodologia ANOVA. Após a obtenção do colágeno, as películas foram feitas a partir de uma solução de colágeno de frango com glicerina ou propilenoglicol. Nos biofilmes foram realizados testes de intumescimento e transmissão de vapor d´água para garantir a qualidade e avaliar as perspectivas de degradação e o grau de hidratação. Também foi avaliado o valor de custos das matérias-primas para produção de uma embalagem com 12 unidades desses biofilmes. Verificou-se que o material seco e pulverizado apresentou uma coloração amarela e uma composição com mais de 78% de proteínas. O rendimento da extração variou de 1,7 até 8,5% de colágeno sobre a massa inicial dos pés de frango e a otimização mostrou que é possível obter rendimentos acima dos 8,0% quando se utiliza a concentração do ácido acético entre 3,000 e 3,682 %, o tempo de operação entre 1 e 3h e a temperatura entre 70 e 76,82°C. Os resultados dos testes de intumescimento e transmissão de vapor d´água garantiram a qualidade dos produtos com relação à degradação e grau de hidratação. A análise de custos mostrou que para se produzir um pacote com 12 unidades de biofilme o custo de matéria-prima envolvida ficou em R$ 0,04 (US$0,01) e que o metilparabeno foi responsável por 75% dos custos, seguido pelo plastificante (glicerina e/ou propilenoglicol) com aproximadamente 20% do custo total da formulação. Assim, este trabalho demonstrou que os biofilmes produzidos a partir do colágeno de frango são viáveis tecnicamente e economicamente.Submitted by Nadir Basilio (nadirsb@uninove.br) on 2018-12-27T18:39:42Z No. of bitstreams: 1 Roberta Bezerra Gardim.pdf: 1468956 bytes, checksum: 380e03b6aa66268dd5e2774f84910e24 (MD5)Made available in DSpace on 2018-12-27T18:39:42Z (GMT). No. of bitstreams: 1 Roberta Bezerra Gardim.pdf: 1468956 bytes, checksum: 380e03b6aa66268dd5e2774f84910e24 (MD5) Previous issue date: 2018-09-27application/pdfporUniversidade Nove de JulhoPrograma de Pós-Graduação de Mestrado e Doutorado em Engenharia de ProduçãoUNINOVEBrasilEngenhariapés de frangocolágeno de frangobiofilmegelatinaextração de colágenoextração de colágeno de frangocolágeno de frango péschicken feetchicken collagenbiofilmgelatincollagen extractioncollagen extraction from chickenchicken collagen feetENGENHARIAS::ENGENHARIA DE PRODUCAOAnálise das viabilidades da obtenção de um biofilme a partir do colágeno de frangoinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/masterThesis2551182063231974631600info:eu-repo/semantics/openAccessreponame:Biblioteca Digital de Teses e Dissertações da Uninoveinstname:Universidade Nove de Julho (UNINOVE)instacron:UNINOVEORIGINALRoberta Bezerra Gardim.pdfRoberta Bezerra Gardim.pdfapplication/pdf1468956http://localhost:8080/tede/bitstream/tede/1947/2/Roberta+Bezerra+Gardim.pdf380e03b6aa66268dd5e2774f84910e24MD52LICENSElicense.txtlicense.txttext/plain; charset=utf-82165http://localhost:8080/tede/bitstream/tede/1947/1/license.txtbd3efa91386c1718a7f26a329fdcb468MD51tede/19472021-10-08 18:31:56.365oai:localhost:tede/1947Tk9UQTogQ09MT1FVRSBBUVVJIEEgU1VBIFBSw5NQUklBIExJQ0VOw4dBCkVzdGEgbGljZW7Dp2EgZGUgZXhlbXBsbyDDqSBmb3JuZWNpZGEgYXBlbmFzIHBhcmEgZmlucyBpbmZvcm1hdGl2b3MuCgpMSUNFTsOHQSBERSBESVNUUklCVUnDh8ODTyBOw4NPLUVYQ0xVU0lWQQoKQ29tIGEgYXByZXNlbnRhw6fDo28gZGVzdGEgbGljZW7Dp2EsIHZvY8OqIChvIGF1dG9yIChlcykgb3UgbyB0aXR1bGFyIGRvcyBkaXJlaXRvcyBkZSBhdXRvcikgY29uY2VkZSDDoCBVbml2ZXJzaWRhZGUgClhYWCAoU2lnbGEgZGEgVW5pdmVyc2lkYWRlKSBvIGRpcmVpdG8gbsOjby1leGNsdXNpdm8gZGUgcmVwcm9kdXppciwgIHRyYWR1emlyIChjb25mb3JtZSBkZWZpbmlkbyBhYmFpeG8pLCBlL291IApkaXN0cmlidWlyIGEgc3VhIHRlc2Ugb3UgZGlzc2VydGHDp8OjbyAoaW5jbHVpbmRvIG8gcmVzdW1vKSBwb3IgdG9kbyBvIG11bmRvIG5vIGZvcm1hdG8gaW1wcmVzc28gZSBlbGV0csO0bmljbyBlIAplbSBxdWFscXVlciBtZWlvLCBpbmNsdWluZG8gb3MgZm9ybWF0b3Mgw6F1ZGlvIG91IHbDrWRlby4KClZvY8OqIGNvbmNvcmRhIHF1ZSBhIFNpZ2xhIGRlIFVuaXZlcnNpZGFkZSBwb2RlLCBzZW0gYWx0ZXJhciBvIGNvbnRlw7pkbywgdHJhbnNwb3IgYSBzdWEgdGVzZSBvdSBkaXNzZXJ0YcOnw6NvIApwYXJhIHF1YWxxdWVyIG1laW8gb3UgZm9ybWF0byBwYXJhIGZpbnMgZGUgcHJlc2VydmHDp8Ojby4KClZvY8OqIHRhbWLDqW0gY29uY29yZGEgcXVlIGEgU2lnbGEgZGUgVW5pdmVyc2lkYWRlIHBvZGUgbWFudGVyIG1haXMgZGUgdW1hIGPDs3BpYSBhIHN1YSB0ZXNlIG91IApkaXNzZXJ0YcOnw6NvIHBhcmEgZmlucyBkZSBzZWd1cmFuw6dhLCBiYWNrLXVwIGUgcHJlc2VydmHDp8Ojby4KClZvY8OqIGRlY2xhcmEgcXVlIGEgc3VhIHRlc2Ugb3UgZGlzc2VydGHDp8OjbyDDqSBvcmlnaW5hbCBlIHF1ZSB2b2PDqiB0ZW0gbyBwb2RlciBkZSBjb25jZWRlciBvcyBkaXJlaXRvcyBjb250aWRvcyAKbmVzdGEgbGljZW7Dp2EuIFZvY8OqIHRhbWLDqW0gZGVjbGFyYSBxdWUgbyBkZXDDs3NpdG8gZGEgc3VhIHRlc2Ugb3UgZGlzc2VydGHDp8OjbyBuw6NvLCBxdWUgc2VqYSBkZSBzZXUgCmNvbmhlY2ltZW50bywgaW5mcmluZ2UgZGlyZWl0b3MgYXV0b3JhaXMgZGUgbmluZ3XDqW0uCgpDYXNvIGEgc3VhIHRlc2Ugb3UgZGlzc2VydGHDp8OjbyBjb250ZW5oYSBtYXRlcmlhbCBxdWUgdm9jw6ogbsOjbyBwb3NzdWkgYSB0aXR1bGFyaWRhZGUgZG9zIGRpcmVpdG9zIGF1dG9yYWlzLCB2b2PDqiAKZGVjbGFyYSBxdWUgb2J0ZXZlIGEgcGVybWlzc8OjbyBpcnJlc3RyaXRhIGRvIGRldGVudG9yIGRvcyBkaXJlaXRvcyBhdXRvcmFpcyBwYXJhIGNvbmNlZGVyIMOgIFNpZ2xhIGRlIFVuaXZlcnNpZGFkZSAKb3MgZGlyZWl0b3MgYXByZXNlbnRhZG9zIG5lc3RhIGxpY2Vuw6dhLCBlIHF1ZSBlc3NlIG1hdGVyaWFsIGRlIHByb3ByaWVkYWRlIGRlIHRlcmNlaXJvcyBlc3TDoSBjbGFyYW1lbnRlIAppZGVudGlmaWNhZG8gZSByZWNvbmhlY2lkbyBubyB0ZXh0byBvdSBubyBjb250ZcO6ZG8gZGEgdGVzZSBvdSBkaXNzZXJ0YcOnw6NvIG9yYSBkZXBvc2l0YWRhLgoKQ0FTTyBBIFRFU0UgT1UgRElTU0VSVEHDh8ODTyBPUkEgREVQT1NJVEFEQSBURU5IQSBTSURPIFJFU1VMVEFETyBERSBVTSBQQVRST0PDjU5JTyBPVSAKQVBPSU8gREUgVU1BIEFHw4pOQ0lBIERFIEZPTUVOVE8gT1UgT1VUUk8gT1JHQU5JU01PIFFVRSBOw4NPIFNFSkEgQSBTSUdMQSBERSAKVU5JVkVSU0lEQURFLCBWT0PDiiBERUNMQVJBIFFVRSBSRVNQRUlUT1UgVE9ET1MgRSBRVUFJU1FVRVIgRElSRUlUT1MgREUgUkVWSVPDg08gQ09NTyAKVEFNQsOJTSBBUyBERU1BSVMgT0JSSUdBw4fDlUVTIEVYSUdJREFTIFBPUiBDT05UUkFUTyBPVSBBQ09SRE8uCgpBIFNpZ2xhIGRlIFVuaXZlcnNpZGFkZSBzZSBjb21wcm9tZXRlIGEgaWRlbnRpZmljYXIgY2xhcmFtZW50ZSBvIHNldSBub21lIChzKSBvdSBvKHMpIG5vbWUocykgZG8ocykgCmRldGVudG9yKGVzKSBkb3MgZGlyZWl0b3MgYXV0b3JhaXMgZGEgdGVzZSBvdSBkaXNzZXJ0YcOnw6NvLCBlIG7Do28gZmFyw6EgcXVhbHF1ZXIgYWx0ZXJhw6fDo28sIGFsw6ltIGRhcXVlbGFzIApjb25jZWRpZGFzIHBvciBlc3RhIGxpY2Vuw6dhLgo=Biblioteca Digital de Teses e Dissertaçõeshttp://bibliotecatede.uninove.br/PRIhttp://bibliotecatede.uninove.br/oai/requestbibliotecatede@uninove.br||bibliotecatede@uninove.bropendoar:2021-10-08T21:31:56Biblioteca Digital de Teses e Dissertações da Uninove - Universidade Nove de Julho (UNINOVE)false |
dc.title.por.fl_str_mv |
Análise das viabilidades da obtenção de um biofilme a partir do colágeno de frango |
title |
Análise das viabilidades da obtenção de um biofilme a partir do colágeno de frango |
spellingShingle |
Análise das viabilidades da obtenção de um biofilme a partir do colágeno de frango Gardim, Roberta Bezerra pés de frango colágeno de frango biofilme gelatina extração de colágeno extração de colágeno de frango colágeno de frango pés chicken feet chicken collagen biofilm gelatin collagen extraction collagen extraction from chicken chicken collagen feet ENGENHARIAS::ENGENHARIA DE PRODUCAO |
title_short |
Análise das viabilidades da obtenção de um biofilme a partir do colágeno de frango |
title_full |
Análise das viabilidades da obtenção de um biofilme a partir do colágeno de frango |
title_fullStr |
Análise das viabilidades da obtenção de um biofilme a partir do colágeno de frango |
title_full_unstemmed |
Análise das viabilidades da obtenção de um biofilme a partir do colágeno de frango |
title_sort |
Análise das viabilidades da obtenção de um biofilme a partir do colágeno de frango |
author |
Gardim, Roberta Bezerra |
author_facet |
Gardim, Roberta Bezerra |
author_role |
author |
dc.contributor.advisor1.fl_str_mv |
Santana, José Carlos Curvelo |
dc.contributor.referee1.fl_str_mv |
Santana, José Carlos Curvelo |
dc.contributor.referee2.fl_str_mv |
Souza, Roberto Rodrigues de |
dc.contributor.referee3.fl_str_mv |
Berssaneti, Fernando Tobal |
dc.contributor.authorLattes.fl_str_mv |
http://lattes.cnpq.br/1864225011246309 |
dc.contributor.author.fl_str_mv |
Gardim, Roberta Bezerra |
contributor_str_mv |
Santana, José Carlos Curvelo Santana, José Carlos Curvelo Souza, Roberto Rodrigues de Berssaneti, Fernando Tobal |
dc.subject.por.fl_str_mv |
pés de frango colágeno de frango biofilme gelatina extração de colágeno extração de colágeno de frango colágeno de frango pés |
topic |
pés de frango colágeno de frango biofilme gelatina extração de colágeno extração de colágeno de frango colágeno de frango pés chicken feet chicken collagen biofilm gelatin collagen extraction collagen extraction from chicken chicken collagen feet ENGENHARIAS::ENGENHARIA DE PRODUCAO |
dc.subject.eng.fl_str_mv |
chicken feet chicken collagen biofilm gelatin collagen extraction collagen extraction from chicken chicken collagen feet |
dc.subject.cnpq.fl_str_mv |
ENGENHARIAS::ENGENHARIA DE PRODUCAO |
description |
The present work aims to analyze the feasibility of obtaining a biofilm from the extraction of collagen from the feet of chicken. In this sense, a factorial design varying the acetic acid concentration, time and temperature of the collagen extraction was used. The optimization of the system was done by response surface analysis with a confidence level of 95% using the ANOVA methodology. After obtaining the collagen, the films were made from a solution of chicken collagen with glycerin or propylene glycol. Biofilms were tested for swelling and water vapor transmission to assure quality and evaluate the prospects for degradation and degree of hydration. It was also evaluated the cost value of raw materials for the production of a pack with 12 units of these biofilms. The dried and pulverized material was found to have a yellow coloration and a composition of more than 78% protein. The extraction yield varied from 1.7 to 8.5% of collagen on the initial mass of the chicken feet and the optimization showed that it is possible to obtain yields above 8.0% when using the acetic acid concentration between 3,000 and 3.682%, the operating time between 1 and 3h and the temperature between 70 and 76.82 ° C. The results of swelling and water vapor transmission tests ensured the quality of products with respect to degradation and degree of hydration. The cost analysis showed that in order to produce a package with 12 biofilm units, the cost of raw material involved was R $ 0.04 (US $ 0.01) and that methylparaben accounted for 75% of the costs, followed by plasticizer (glycerine and / or propylene glycol) with approximately 20% of the total cost of the formulation. Thus, this work demonstrated that biofilms produced from chicken collagen are technically and economically viable. |
publishDate |
2018 |
dc.date.accessioned.fl_str_mv |
2018-12-27T18:39:42Z |
dc.date.issued.fl_str_mv |
2018-09-27 |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/masterThesis |
format |
masterThesis |
status_str |
publishedVersion |
dc.identifier.citation.fl_str_mv |
Gardim, Roberta Bezerra. Análise das viabilidades da obtenção de um biofilme a partir do colágeno de frango. 2018. 85 f. Dissertação( Programa de Mestrado em Engenharia de Produção) - Universidade Nove de Julho, São Paulo. |
dc.identifier.uri.fl_str_mv |
http://bibliotecatede.uninove.br/handle/tede/1947 |
identifier_str_mv |
Gardim, Roberta Bezerra. Análise das viabilidades da obtenção de um biofilme a partir do colágeno de frango. 2018. 85 f. Dissertação( Programa de Mestrado em Engenharia de Produção) - Universidade Nove de Julho, São Paulo. |
url |
http://bibliotecatede.uninove.br/handle/tede/1947 |
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por |
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2551182063231974631 |
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600 |
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openAccess |
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Universidade Nove de Julho |
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Programa de Pós-Graduação de Mestrado e Doutorado em Engenharia de Produção |
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UNINOVE |
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Engenharia |
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Universidade Nove de Julho |
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