Young’s modulus and hardness of multiphase CaZrO3 -MgO ceramics by micro and nanoindentation
Autor(a) principal: | |
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Data de Publicação: | 2017 |
Outros Autores: | , , , , |
Tipo de documento: | Artigo |
Idioma: | eng |
Título da fonte: | Repositório Científico de Acesso Aberto de Portugal (Repositórios Cientìficos) |
Texto Completo: | http://hdl.handle.net/10400.6/12447 |
Resumo: | The aim of this work is to determine the values of the hardness and elastic modulus of the phases present in CaZrO3-MgO-ZrO2 composites and to analyse their contribution to the composite properties. Two materials previously developed with the same major phases (CaZrO3, MgO and c-ZrO2) present in different volume fractions and grain size have been analysed. The hardness and Young´s modulus of each phase determined by nanoindentation are independent from the specific composite and coincident with nanoindentation values for single phase bulk materials. The contribution of the individual phases to Young´s modulus of the multiphase materials is in agreement with calculations using the nanoindentation values and the Voight upper limit of the “rule of mixtures”. Scale dependence due to microcracking has been observed for microhardness values of the composites and differences between calculations and experimental values are related to this effect. |
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Young’s modulus and hardness of multiphase CaZrO3 -MgO ceramics by micro and nanoindentationYoung’s modulusCaZrO3HardnessCa-ZrO2NanoindentationThe aim of this work is to determine the values of the hardness and elastic modulus of the phases present in CaZrO3-MgO-ZrO2 composites and to analyse their contribution to the composite properties. Two materials previously developed with the same major phases (CaZrO3, MgO and c-ZrO2) present in different volume fractions and grain size have been analysed. The hardness and Young´s modulus of each phase determined by nanoindentation are independent from the specific composite and coincident with nanoindentation values for single phase bulk materials. The contribution of the individual phases to Young´s modulus of the multiphase materials is in agreement with calculations using the nanoindentation values and the Voight upper limit of the “rule of mixtures”. Scale dependence due to microcracking has been observed for microhardness values of the composites and differences between calculations and experimental values are related to this effect.This work was performed in the frame of the CYTEDnetwork HOREF(312RT0453)and was supported by the Spanish Government underprojectMAT2013-48426-C2-1-R.AbílioP.Silvaacknowledges thefinancialsupportofJECSTrustthroughmobilityContract201597 and Instituto de Cerámica y Vidrio–CSIC.ElsevieruBibliorumSilva, Abílio P.Booth, FernandoGarrido, LilianaAglietti, EstebanPena, PilarBaudin, Carmen2022-12-05T11:32:53Z2017-11-062017-11-06T00:00:00Zinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/articleapplication/pdfhttp://hdl.handle.net/10400.6/12447eng10.1016/j.jeurceramsoc.2017.11.007info:eu-repo/semantics/openAccessreponame:Repositório Científico de Acesso Aberto de Portugal (Repositórios Cientìficos)instname:Agência para a Sociedade do Conhecimento (UMIC) - FCT - Sociedade da Informaçãoinstacron:RCAAP2023-12-15T09:45:36Zoai:ubibliorum.ubi.pt:10400.6/12447Portal AgregadorONGhttps://www.rcaap.pt/oai/openaireopendoar:71602024-03-20T00:47:26.462813Repositório Científico de Acesso Aberto de Portugal (Repositórios Cientìficos) - Agência para a Sociedade do Conhecimento (UMIC) - FCT - Sociedade da Informaçãofalse |
dc.title.none.fl_str_mv |
Young’s modulus and hardness of multiphase CaZrO3 -MgO ceramics by micro and nanoindentation |
title |
Young’s modulus and hardness of multiphase CaZrO3 -MgO ceramics by micro and nanoindentation |
spellingShingle |
Young’s modulus and hardness of multiphase CaZrO3 -MgO ceramics by micro and nanoindentation Silva, Abílio P. Young’s modulus CaZrO3 Hardness Ca-ZrO2 Nanoindentation |
title_short |
Young’s modulus and hardness of multiphase CaZrO3 -MgO ceramics by micro and nanoindentation |
title_full |
Young’s modulus and hardness of multiphase CaZrO3 -MgO ceramics by micro and nanoindentation |
title_fullStr |
Young’s modulus and hardness of multiphase CaZrO3 -MgO ceramics by micro and nanoindentation |
title_full_unstemmed |
Young’s modulus and hardness of multiphase CaZrO3 -MgO ceramics by micro and nanoindentation |
title_sort |
Young’s modulus and hardness of multiphase CaZrO3 -MgO ceramics by micro and nanoindentation |
author |
Silva, Abílio P. |
author_facet |
Silva, Abílio P. Booth, Fernando Garrido, Liliana Aglietti, Esteban Pena, Pilar Baudin, Carmen |
author_role |
author |
author2 |
Booth, Fernando Garrido, Liliana Aglietti, Esteban Pena, Pilar Baudin, Carmen |
author2_role |
author author author author author |
dc.contributor.none.fl_str_mv |
uBibliorum |
dc.contributor.author.fl_str_mv |
Silva, Abílio P. Booth, Fernando Garrido, Liliana Aglietti, Esteban Pena, Pilar Baudin, Carmen |
dc.subject.por.fl_str_mv |
Young’s modulus CaZrO3 Hardness Ca-ZrO2 Nanoindentation |
topic |
Young’s modulus CaZrO3 Hardness Ca-ZrO2 Nanoindentation |
description |
The aim of this work is to determine the values of the hardness and elastic modulus of the phases present in CaZrO3-MgO-ZrO2 composites and to analyse their contribution to the composite properties. Two materials previously developed with the same major phases (CaZrO3, MgO and c-ZrO2) present in different volume fractions and grain size have been analysed. The hardness and Young´s modulus of each phase determined by nanoindentation are independent from the specific composite and coincident with nanoindentation values for single phase bulk materials. The contribution of the individual phases to Young´s modulus of the multiphase materials is in agreement with calculations using the nanoindentation values and the Voight upper limit of the “rule of mixtures”. Scale dependence due to microcracking has been observed for microhardness values of the composites and differences between calculations and experimental values are related to this effect. |
publishDate |
2017 |
dc.date.none.fl_str_mv |
2017-11-06 2017-11-06T00:00:00Z 2022-12-05T11:32:53Z |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
http://hdl.handle.net/10400.6/12447 |
url |
http://hdl.handle.net/10400.6/12447 |
dc.language.iso.fl_str_mv |
eng |
language |
eng |
dc.relation.none.fl_str_mv |
10.1016/j.jeurceramsoc.2017.11.007 |
dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess |
eu_rights_str_mv |
openAccess |
dc.format.none.fl_str_mv |
application/pdf |
dc.publisher.none.fl_str_mv |
Elsevier |
publisher.none.fl_str_mv |
Elsevier |
dc.source.none.fl_str_mv |
reponame:Repositório Científico de Acesso Aberto de Portugal (Repositórios Cientìficos) instname:Agência para a Sociedade do Conhecimento (UMIC) - FCT - Sociedade da Informação instacron:RCAAP |
instname_str |
Agência para a Sociedade do Conhecimento (UMIC) - FCT - Sociedade da Informação |
instacron_str |
RCAAP |
institution |
RCAAP |
reponame_str |
Repositório Científico de Acesso Aberto de Portugal (Repositórios Cientìficos) |
collection |
Repositório Científico de Acesso Aberto de Portugal (Repositórios Cientìficos) |
repository.name.fl_str_mv |
Repositório Científico de Acesso Aberto de Portugal (Repositórios Cientìficos) - Agência para a Sociedade do Conhecimento (UMIC) - FCT - Sociedade da Informação |
repository.mail.fl_str_mv |
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1799136369725931520 |