Physicochemical characterization of Lavandula spp. honey with FT-Raman spectroscopy
Autor(a) principal: | |
---|---|
Data de Publicação: | 2018 |
Outros Autores: | , , |
Tipo de documento: | Artigo |
Idioma: | eng |
Título da fonte: | Repositório Científico de Acesso Aberto de Portugal (Repositórios Cientìficos) |
Texto Completo: | http://hdl.handle.net/10198/15374 |
Resumo: | This study aimed to evaluate the potential of FT-Raman spectroscopy in the prediction of the chemical composition of Lavandula spp. monofloral honey. Partial Least Squares (PLS) regression models were performed for the quantitative estimation and the results were correlated with those obtained using reference methods. Good calibration models were obtained for electrical conductivity, ash, total acidity, pH, reducing sugars, hydroxymethylfurfural (HMF), proline, diastase index, apparent sucrose, total flavonoids content and total phenol content. On the other hand, the model was less accurate for pH determination. The calibration models had high r 2 (ranging between 92.8% and 99.9%), high residual prediction deviation - RPD (ranging between 4.2 and 26.8) and low root mean square errors. These results confirm the hypothesis that FT-Raman is a useful technique for the quality control and chemical properties’ evaluation of Lavandula spp honey. Its application may allow improving the efficiency, speed and cost of the current laboratory analysis. |
id |
RCAP_b4c6f0def42c6b15c28a234ae16c11ae |
---|---|
oai_identifier_str |
oai:bibliotecadigital.ipb.pt:10198/15374 |
network_acronym_str |
RCAP |
network_name_str |
Repositório Científico de Acesso Aberto de Portugal (Repositórios Cientìficos) |
repository_id_str |
7160 |
spelling |
Physicochemical characterization of Lavandula spp. honey with FT-Raman spectroscopyChemical compositionFT-RamanHoneyLavandula spp.PLS regression modelsQuality controlThis study aimed to evaluate the potential of FT-Raman spectroscopy in the prediction of the chemical composition of Lavandula spp. monofloral honey. Partial Least Squares (PLS) regression models were performed for the quantitative estimation and the results were correlated with those obtained using reference methods. Good calibration models were obtained for electrical conductivity, ash, total acidity, pH, reducing sugars, hydroxymethylfurfural (HMF), proline, diastase index, apparent sucrose, total flavonoids content and total phenol content. On the other hand, the model was less accurate for pH determination. The calibration models had high r 2 (ranging between 92.8% and 99.9%), high residual prediction deviation - RPD (ranging between 4.2 and 26.8) and low root mean square errors. These results confirm the hypothesis that FT-Raman is a useful technique for the quality control and chemical properties’ evaluation of Lavandula spp honey. Its application may allow improving the efficiency, speed and cost of the current laboratory analysis.Acknowledgements: CEF is a research unit funded by Fundação para a Ciência e a Tecnologia I.P. (FCT), Portugal (UID/AGR/00239/2013). Centre of Molecular and Environmental Biology is a research unit funded by FCT, UID/BIA/04050/2013 (POCI-01–0145-FEDER-007569) and by the ERDF through the COMPETE2020 - Programa Operacional Competitividade e Internacionalização (POCI).Biblioteca Digital do IPBAnjos, OféliaSantos, António J.A.Paixão, VascoEstevinho, Leticia M.2018-01-31T10:00:00Z20182018-01-01T00:00:00Zinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/articleapplication/pdfhttp://hdl.handle.net/10198/15374engAnjos, Ofélia; Santos, António J.A.; Paixão, Vasco; Estevinho, Letícia M. (2018). Physicochemical characterization of Lavandula spp. honey with FT-Raman spectroscopy. Talanta. ISSN 0039-9140. 178, p. 43-480039-914010.1016/j.talanta.2017.08.099info:eu-repo/semantics/openAccessreponame:Repositório Científico de Acesso Aberto de Portugal (Repositórios Cientìficos)instname:Agência para a Sociedade do Conhecimento (UMIC) - FCT - Sociedade da Informaçãoinstacron:RCAAP2023-11-21T10:35:57Zoai:bibliotecadigital.ipb.pt:10198/15374Portal AgregadorONGhttps://www.rcaap.pt/oai/openaireopendoar:71602024-03-19T23:04:58.921534Repositório Científico de Acesso Aberto de Portugal (Repositórios Cientìficos) - Agência para a Sociedade do Conhecimento (UMIC) - FCT - Sociedade da Informaçãofalse |
dc.title.none.fl_str_mv |
Physicochemical characterization of Lavandula spp. honey with FT-Raman spectroscopy |
title |
Physicochemical characterization of Lavandula spp. honey with FT-Raman spectroscopy |
spellingShingle |
Physicochemical characterization of Lavandula spp. honey with FT-Raman spectroscopy Anjos, Ofélia Chemical composition FT-Raman Honey Lavandula spp. PLS regression models Quality control |
title_short |
Physicochemical characterization of Lavandula spp. honey with FT-Raman spectroscopy |
title_full |
Physicochemical characterization of Lavandula spp. honey with FT-Raman spectroscopy |
title_fullStr |
Physicochemical characterization of Lavandula spp. honey with FT-Raman spectroscopy |
title_full_unstemmed |
Physicochemical characterization of Lavandula spp. honey with FT-Raman spectroscopy |
title_sort |
Physicochemical characterization of Lavandula spp. honey with FT-Raman spectroscopy |
author |
Anjos, Ofélia |
author_facet |
Anjos, Ofélia Santos, António J.A. Paixão, Vasco Estevinho, Leticia M. |
author_role |
author |
author2 |
Santos, António J.A. Paixão, Vasco Estevinho, Leticia M. |
author2_role |
author author author |
dc.contributor.none.fl_str_mv |
Biblioteca Digital do IPB |
dc.contributor.author.fl_str_mv |
Anjos, Ofélia Santos, António J.A. Paixão, Vasco Estevinho, Leticia M. |
dc.subject.por.fl_str_mv |
Chemical composition FT-Raman Honey Lavandula spp. PLS regression models Quality control |
topic |
Chemical composition FT-Raman Honey Lavandula spp. PLS regression models Quality control |
description |
This study aimed to evaluate the potential of FT-Raman spectroscopy in the prediction of the chemical composition of Lavandula spp. monofloral honey. Partial Least Squares (PLS) regression models were performed for the quantitative estimation and the results were correlated with those obtained using reference methods. Good calibration models were obtained for electrical conductivity, ash, total acidity, pH, reducing sugars, hydroxymethylfurfural (HMF), proline, diastase index, apparent sucrose, total flavonoids content and total phenol content. On the other hand, the model was less accurate for pH determination. The calibration models had high r 2 (ranging between 92.8% and 99.9%), high residual prediction deviation - RPD (ranging between 4.2 and 26.8) and low root mean square errors. These results confirm the hypothesis that FT-Raman is a useful technique for the quality control and chemical properties’ evaluation of Lavandula spp honey. Its application may allow improving the efficiency, speed and cost of the current laboratory analysis. |
publishDate |
2018 |
dc.date.none.fl_str_mv |
2018-01-31T10:00:00Z 2018 2018-01-01T00:00:00Z |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
http://hdl.handle.net/10198/15374 |
url |
http://hdl.handle.net/10198/15374 |
dc.language.iso.fl_str_mv |
eng |
language |
eng |
dc.relation.none.fl_str_mv |
Anjos, Ofélia; Santos, António J.A.; Paixão, Vasco; Estevinho, Letícia M. (2018). Physicochemical characterization of Lavandula spp. honey with FT-Raman spectroscopy. Talanta. ISSN 0039-9140. 178, p. 43-48 0039-9140 10.1016/j.talanta.2017.08.099 |
dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess |
eu_rights_str_mv |
openAccess |
dc.format.none.fl_str_mv |
application/pdf |
dc.source.none.fl_str_mv |
reponame:Repositório Científico de Acesso Aberto de Portugal (Repositórios Cientìficos) instname:Agência para a Sociedade do Conhecimento (UMIC) - FCT - Sociedade da Informação instacron:RCAAP |
instname_str |
Agência para a Sociedade do Conhecimento (UMIC) - FCT - Sociedade da Informação |
instacron_str |
RCAAP |
institution |
RCAAP |
reponame_str |
Repositório Científico de Acesso Aberto de Portugal (Repositórios Cientìficos) |
collection |
Repositório Científico de Acesso Aberto de Portugal (Repositórios Cientìficos) |
repository.name.fl_str_mv |
Repositório Científico de Acesso Aberto de Portugal (Repositórios Cientìficos) - Agência para a Sociedade do Conhecimento (UMIC) - FCT - Sociedade da Informação |
repository.mail.fl_str_mv |
|
_version_ |
1817553399989665792 |