The making of black inks in an Arabic treatise by al-Qalalūsī dated from the 13th c.
| Autor(a) principal: | |
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| Data de Publicação: | 2023 |
| Outros Autores: | , , , , , , , , |
| Tipo de documento: | Artigo |
| Idioma: | eng |
| Título da fonte: | Repositório Científico de Acesso Aberto de Portugal (Repositórios Cientìficos) |
| Texto Completo: | http://hdl.handle.net/10362/153175 |
Resumo: | Funding Information: This research was funded by the Portuguese Science Foundation [Fundação para a Ciência e Tecnologia, Ministério da Educação e da Ciência (FCT/MCTES)], through doctoral programme CORES-PD/00253/2012. Recetas y conocimientos de la sociedad medieval para el siglo XXI | "Try it and you will see thats true. Recipes and konwledges from medieval society to 21th century", PID2019-108736 GB-I00, Ministerio de Ciencia e Innovación. N. Teixeira and V. Otero acknowledge R. J. Díaz Hidalgo, posdoctoral UCO 2020, La producción documental y libraría al Ándalus siglos XIII XV, Plan Propio de Investigación de la Universidad de Córdoba; Associate Laboratory for Green Chemistry- LAQV co-financed by the ERDF under the PT2020 Partnership Agreement (POCI-01–0145-FEDER-007265). Publisher Copyright: © 2023, The Author(s). |
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The making of black inks in an Arabic treatise by al-Qalalūsī dated from the 13th c.reproduction and characterisation of iron-gall ink recipesConservationIron gall inksRecipesTechnical literatureConservationChemistry (miscellaneous)ArchaeologyMaterials Science (miscellaneous)ArchaeologyComputer Science ApplicationsSpectroscopyFunding Information: This research was funded by the Portuguese Science Foundation [Fundação para a Ciência e Tecnologia, Ministério da Educação e da Ciência (FCT/MCTES)], through doctoral programme CORES-PD/00253/2012. Recetas y conocimientos de la sociedad medieval para el siglo XXI | "Try it and you will see thats true. Recipes and konwledges from medieval society to 21th century", PID2019-108736 GB-I00, Ministerio de Ciencia e Innovación. N. Teixeira and V. Otero acknowledge R. J. Díaz Hidalgo, posdoctoral UCO 2020, La producción documental y libraría al Ándalus siglos XIII XV, Plan Propio de Investigación de la Universidad de Córdoba; Associate Laboratory for Green Chemistry- LAQV co-financed by the ERDF under the PT2020 Partnership Agreement (POCI-01–0145-FEDER-007265). Publisher Copyright: © 2023, The Author(s).For the first time, this paper systematises the medieval preparation of black writing inks found in the important thirteenth century Andalusian technical treatise written by Muhammad ibn Idrīs ibn al-Qalalūsī (1210–1308). We present the Arabic version of this extraordinary text (‘The gifts of the wise men on the curiosities of the substances’), and its first English translation, as well as discuss key aspects of the processes that remain missing or are unclear indications. In this work, we studied the iron gall inks based on galls, where no other phenolic source is present. In this pedagogical treatise, the recipes for these black iron-gall inks are organised and classified by the gallnuts extraction method used: boiling (decoction), squeezing and infusion, with water being the only solvent used. The inks selected were reproduced and characterised through a multi-analytical approach. Quantification was performed by HPLC–DAD (high performance liquid chromatography with diode array detectors in the UV–VIS), showing that gallic acid is a minor compound in the gall extracts prepared following al-Qalalūsī instructions. In all the recipes, the higher concentration compounds in the gall extracts are the gallotannins pentagalloylglucose and hexagalloylglucose, ranging from 79 to 50% of the phenolic compounds. This supports the results of Raman and infrared spectroscopies. A comparison with medieval Iberian recipes was also done, which served to reinforce our previous results that show water as the sole solvent extracts with much lower yields than mixed solvents (water plus white wine or vinegar).DCR - Departamento de Conservação e RestauroLAQV@REQUIMTEVICARTE - Vidro e Cerâmica para as ArtesRUNDíaz Hidalgo, Rafael JavierCórdoba, RicardoGrigoryan, HermineVieira, MárciaMelo, Maria J.Nabais, PaulaOtero, VanessaTeixeira, NatérciaFani, SaraAl-Abbady, Hossam2023-05-25T22:19:53Z2023-122023-12-01T00:00:00Zinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/article14application/pdfhttp://hdl.handle.net/10362/153175eng2050-7445PURE: 61559133https://doi.org/10.1186/s40494-022-00823-1info:eu-repo/semantics/openAccessreponame:Repositório Científico de Acesso Aberto de Portugal (Repositórios Cientìficos)instname:Agência para a Sociedade do Conhecimento (UMIC) - FCT - Sociedade da Informaçãoinstacron:RCAAP2024-03-11T05:35:47Zoai:run.unl.pt:10362/153175Portal AgregadorONGhttps://www.rcaap.pt/oai/openaireopendoar:71602024-03-20T03:55:12.664397Repositório Científico de Acesso Aberto de Portugal (Repositórios Cientìficos) - Agência para a Sociedade do Conhecimento (UMIC) - FCT - Sociedade da Informaçãofalse |
| dc.title.none.fl_str_mv |
The making of black inks in an Arabic treatise by al-Qalalūsī dated from the 13th c. reproduction and characterisation of iron-gall ink recipes |
| title |
The making of black inks in an Arabic treatise by al-Qalalūsī dated from the 13th c. |
| spellingShingle |
The making of black inks in an Arabic treatise by al-Qalalūsī dated from the 13th c. Díaz Hidalgo, Rafael Javier Conservation Iron gall inks Recipes Technical literature Conservation Chemistry (miscellaneous) Archaeology Materials Science (miscellaneous) Archaeology Computer Science Applications Spectroscopy |
| title_short |
The making of black inks in an Arabic treatise by al-Qalalūsī dated from the 13th c. |
| title_full |
The making of black inks in an Arabic treatise by al-Qalalūsī dated from the 13th c. |
| title_fullStr |
The making of black inks in an Arabic treatise by al-Qalalūsī dated from the 13th c. |
| title_full_unstemmed |
The making of black inks in an Arabic treatise by al-Qalalūsī dated from the 13th c. |
| title_sort |
The making of black inks in an Arabic treatise by al-Qalalūsī dated from the 13th c. |
| author |
Díaz Hidalgo, Rafael Javier |
| author_facet |
Díaz Hidalgo, Rafael Javier Córdoba, Ricardo Grigoryan, Hermine Vieira, Márcia Melo, Maria J. Nabais, Paula Otero, Vanessa Teixeira, Natércia Fani, Sara Al-Abbady, Hossam |
| author_role |
author |
| author2 |
Córdoba, Ricardo Grigoryan, Hermine Vieira, Márcia Melo, Maria J. Nabais, Paula Otero, Vanessa Teixeira, Natércia Fani, Sara Al-Abbady, Hossam |
| author2_role |
author author author author author author author author author |
| dc.contributor.none.fl_str_mv |
DCR - Departamento de Conservação e Restauro LAQV@REQUIMTE VICARTE - Vidro e Cerâmica para as Artes RUN |
| dc.contributor.author.fl_str_mv |
Díaz Hidalgo, Rafael Javier Córdoba, Ricardo Grigoryan, Hermine Vieira, Márcia Melo, Maria J. Nabais, Paula Otero, Vanessa Teixeira, Natércia Fani, Sara Al-Abbady, Hossam |
| dc.subject.por.fl_str_mv |
Conservation Iron gall inks Recipes Technical literature Conservation Chemistry (miscellaneous) Archaeology Materials Science (miscellaneous) Archaeology Computer Science Applications Spectroscopy |
| topic |
Conservation Iron gall inks Recipes Technical literature Conservation Chemistry (miscellaneous) Archaeology Materials Science (miscellaneous) Archaeology Computer Science Applications Spectroscopy |
| description |
Funding Information: This research was funded by the Portuguese Science Foundation [Fundação para a Ciência e Tecnologia, Ministério da Educação e da Ciência (FCT/MCTES)], through doctoral programme CORES-PD/00253/2012. Recetas y conocimientos de la sociedad medieval para el siglo XXI | "Try it and you will see thats true. Recipes and konwledges from medieval society to 21th century", PID2019-108736 GB-I00, Ministerio de Ciencia e Innovación. N. Teixeira and V. Otero acknowledge R. J. Díaz Hidalgo, posdoctoral UCO 2020, La producción documental y libraría al Ándalus siglos XIII XV, Plan Propio de Investigación de la Universidad de Córdoba; Associate Laboratory for Green Chemistry- LAQV co-financed by the ERDF under the PT2020 Partnership Agreement (POCI-01–0145-FEDER-007265). Publisher Copyright: © 2023, The Author(s). |
| publishDate |
2023 |
| dc.date.none.fl_str_mv |
2023-05-25T22:19:53Z 2023-12 2023-12-01T00:00:00Z |
| dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
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info:eu-repo/semantics/article |
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article |
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publishedVersion |
| dc.identifier.uri.fl_str_mv |
http://hdl.handle.net/10362/153175 |
| url |
http://hdl.handle.net/10362/153175 |
| dc.language.iso.fl_str_mv |
eng |
| language |
eng |
| dc.relation.none.fl_str_mv |
2050-7445 PURE: 61559133 https://doi.org/10.1186/s40494-022-00823-1 |
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info:eu-repo/semantics/openAccess |
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openAccess |
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14 application/pdf |
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RCAAP |
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RCAAP |
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