Characterization of reverse martensitic transformation in cold-rolled austenitic 316 stainless steel

Detalhes bibliográficos
Autor(a) principal: Fava,Javier
Data de Publicação: 2018
Outros Autores: Spinosa,Cristina, Ruch,Marta, Carabedo,Fernando, Landau,Mónica, Cosarinsky,Guillermo, Savin,Adriana, Steigmann,Rozina, Craus,Mihail Liviu
Tipo de documento: Artigo
Idioma: eng
Título da fonte: Matéria (Rio de Janeiro. Online)
Texto Completo: http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1517-70762018000200523
Resumo: ABSTRACT In this work the reversion of the strain-induced ?’-martensite to ?’-austenite was studied in a series of AISI 316 stainless steels (SS) specimens. The samples were submitted to 63% reduction in thickness by rolling at a temperature of -70ºC, to achieve high martensite content. The reversion of martensite to austenite was made by means of isochronic, isothermal heat treatments at temperatures between 200 and 900ºC, so as to induce partial martensite-austenite phase transformation. The samples were studied by optical and electronic microscopy, X-ray diffraction, magnetization measurements, microhardness, and electromagnetic non destructive methods: feritscope, conductivity measurements using Van der Pauw’s technique, and magnetic permeability assessments by an eddy current inverse method. The metalography study showed an ?’ lath martensite type structure and a similar one for the reverted austenite (?’). Magnetization measurements and magnetic permeability showed that the reversion is active between 400 and 800°C. From the magnetic saturation measurements, a new calibration curve for the assessment of %?’ through the feritscope readings was obtained. The results of the different techniques were com-pared, in order to assess the scope of the studied techniques in the characterization of rolled SS products, and in the evaluation of progress of reversion reaction.
id RLAM-1_23aceeed0c74d3bf8929fce1da9f22bc
oai_identifier_str oai:scielo:S1517-70762018000200523
network_acronym_str RLAM-1
network_name_str Matéria (Rio de Janeiro. Online)
repository_id_str
spelling Characterization of reverse martensitic transformation in cold-rolled austenitic 316 stainless steelMartensitereversionausteniticeddy current.ABSTRACT In this work the reversion of the strain-induced ?’-martensite to ?’-austenite was studied in a series of AISI 316 stainless steels (SS) specimens. The samples were submitted to 63% reduction in thickness by rolling at a temperature of -70ºC, to achieve high martensite content. The reversion of martensite to austenite was made by means of isochronic, isothermal heat treatments at temperatures between 200 and 900ºC, so as to induce partial martensite-austenite phase transformation. The samples were studied by optical and electronic microscopy, X-ray diffraction, magnetization measurements, microhardness, and electromagnetic non destructive methods: feritscope, conductivity measurements using Van der Pauw’s technique, and magnetic permeability assessments by an eddy current inverse method. The metalography study showed an ?’ lath martensite type structure and a similar one for the reverted austenite (?’). Magnetization measurements and magnetic permeability showed that the reversion is active between 400 and 800°C. From the magnetic saturation measurements, a new calibration curve for the assessment of %?’ through the feritscope readings was obtained. The results of the different techniques were com-pared, in order to assess the scope of the studied techniques in the characterization of rolled SS products, and in the evaluation of progress of reversion reaction.Laboratório de Hidrogênio, Coppe - Universidade Federal do Rio de Janeiroem cooperação com a Associação Brasileira do Hidrogênio, ABH22018-01-01info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersiontext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S1517-70762018000200523Matéria (Rio de Janeiro) v.23 n.2 2018reponame:Matéria (Rio de Janeiro. Online)instname:Matéria (Rio de Janeiro. Online)instacron:RLAM10.1590/s1517-707620180002.04info:eu-repo/semantics/openAccessFava,JavierSpinosa,CristinaRuch,MartaCarabedo,FernandoLandau,MónicaCosarinsky,GuillermoSavin,AdrianaSteigmann,RozinaCraus,Mihail Liviueng2018-07-19T00:00:00Zoai:scielo:S1517-70762018000200523Revistahttp://www.materia.coppe.ufrj.br/https://old.scielo.br/oai/scielo-oai.php||materia@labh2.coppe.ufrj.br1517-70761517-7076opendoar:2018-07-19T00:00Matéria (Rio de Janeiro. Online) - Matéria (Rio de Janeiro. Online)false
dc.title.none.fl_str_mv Characterization of reverse martensitic transformation in cold-rolled austenitic 316 stainless steel
title Characterization of reverse martensitic transformation in cold-rolled austenitic 316 stainless steel
spellingShingle Characterization of reverse martensitic transformation in cold-rolled austenitic 316 stainless steel
Fava,Javier
Martensite
reversion
austenitic
eddy current.
title_short Characterization of reverse martensitic transformation in cold-rolled austenitic 316 stainless steel
title_full Characterization of reverse martensitic transformation in cold-rolled austenitic 316 stainless steel
title_fullStr Characterization of reverse martensitic transformation in cold-rolled austenitic 316 stainless steel
title_full_unstemmed Characterization of reverse martensitic transformation in cold-rolled austenitic 316 stainless steel
title_sort Characterization of reverse martensitic transformation in cold-rolled austenitic 316 stainless steel
author Fava,Javier
author_facet Fava,Javier
Spinosa,Cristina
Ruch,Marta
Carabedo,Fernando
Landau,Mónica
Cosarinsky,Guillermo
Savin,Adriana
Steigmann,Rozina
Craus,Mihail Liviu
author_role author
author2 Spinosa,Cristina
Ruch,Marta
Carabedo,Fernando
Landau,Mónica
Cosarinsky,Guillermo
Savin,Adriana
Steigmann,Rozina
Craus,Mihail Liviu
author2_role author
author
author
author
author
author
author
author
dc.contributor.author.fl_str_mv Fava,Javier
Spinosa,Cristina
Ruch,Marta
Carabedo,Fernando
Landau,Mónica
Cosarinsky,Guillermo
Savin,Adriana
Steigmann,Rozina
Craus,Mihail Liviu
dc.subject.por.fl_str_mv Martensite
reversion
austenitic
eddy current.
topic Martensite
reversion
austenitic
eddy current.
description ABSTRACT In this work the reversion of the strain-induced ?’-martensite to ?’-austenite was studied in a series of AISI 316 stainless steels (SS) specimens. The samples were submitted to 63% reduction in thickness by rolling at a temperature of -70ºC, to achieve high martensite content. The reversion of martensite to austenite was made by means of isochronic, isothermal heat treatments at temperatures between 200 and 900ºC, so as to induce partial martensite-austenite phase transformation. The samples were studied by optical and electronic microscopy, X-ray diffraction, magnetization measurements, microhardness, and electromagnetic non destructive methods: feritscope, conductivity measurements using Van der Pauw’s technique, and magnetic permeability assessments by an eddy current inverse method. The metalography study showed an ?’ lath martensite type structure and a similar one for the reverted austenite (?’). Magnetization measurements and magnetic permeability showed that the reversion is active between 400 and 800°C. From the magnetic saturation measurements, a new calibration curve for the assessment of %?’ through the feritscope readings was obtained. The results of the different techniques were com-pared, in order to assess the scope of the studied techniques in the characterization of rolled SS products, and in the evaluation of progress of reversion reaction.
publishDate 2018
dc.date.none.fl_str_mv 2018-01-01
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1517-70762018000200523
url http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1517-70762018000200523
dc.language.iso.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv 10.1590/s1517-707620180002.04
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv text/html
dc.publisher.none.fl_str_mv Laboratório de Hidrogênio, Coppe - Universidade Federal do Rio de Janeiro
em cooperação com a Associação Brasileira do Hidrogênio, ABH2
publisher.none.fl_str_mv Laboratório de Hidrogênio, Coppe - Universidade Federal do Rio de Janeiro
em cooperação com a Associação Brasileira do Hidrogênio, ABH2
dc.source.none.fl_str_mv Matéria (Rio de Janeiro) v.23 n.2 2018
reponame:Matéria (Rio de Janeiro. Online)
instname:Matéria (Rio de Janeiro. Online)
instacron:RLAM
instname_str Matéria (Rio de Janeiro. Online)
instacron_str RLAM
institution RLAM
reponame_str Matéria (Rio de Janeiro. Online)
collection Matéria (Rio de Janeiro. Online)
repository.name.fl_str_mv Matéria (Rio de Janeiro. Online) - Matéria (Rio de Janeiro. Online)
repository.mail.fl_str_mv ||materia@labh2.coppe.ufrj.br
_version_ 1752126690782347264