Comparative study between natural and synthetic Hydroxyapatite: structural, morphological and bioactivity properties
Autor(a) principal: | |
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Data de Publicação: | 2018 |
Outros Autores: | , , , |
Tipo de documento: | Artigo |
Idioma: | eng |
Título da fonte: | Matéria (Rio de Janeiro. Online) |
Texto Completo: | http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1517-70762018000400408 |
Resumo: | ABSTRACT In this work, a study of hydroxyapatite (HAp) powders obtained using both, porcine bones and chemical precursors was carried put. In the case of HAp obtained by means of porcine bones, physical processes as cooking, washing and milling were developed, for removing the organic material from the bones; after that, the powders were submitted to a thermal treatment at 800 °C, during 12 h. This procedure was carried out without adding chemical alkalines that are harmful for the environment and the human health. On the other hand, HAp powders were also synthetized using the chemical precipitation method widely reported, showing successful results. Moreover, both kind of powders were characterized using x ray diffraction, Fourier transformer infrared spectroscopy, scanning electron microscopy and energy dispersive spectroscopy. Furthermore, the bioactivity of the materials was determined using the simulated biological fluid (SBF) method. Results showed that the natural HAp exhibited better crystallographic properties. Moreover, according to these results, HAp obtained from porcine bones contains traces of elements as Na and Mg that are favorable for the bioactivity, according to the materials behavior when they are immersed in SBF. |
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Comparative study between natural and synthetic Hydroxyapatite: structural, morphological and bioactivity propertiesHydroxyapatiteporcine boneschemical precipitationsimulated biological fluidABSTRACT In this work, a study of hydroxyapatite (HAp) powders obtained using both, porcine bones and chemical precursors was carried put. In the case of HAp obtained by means of porcine bones, physical processes as cooking, washing and milling were developed, for removing the organic material from the bones; after that, the powders were submitted to a thermal treatment at 800 °C, during 12 h. This procedure was carried out without adding chemical alkalines that are harmful for the environment and the human health. On the other hand, HAp powders were also synthetized using the chemical precipitation method widely reported, showing successful results. Moreover, both kind of powders were characterized using x ray diffraction, Fourier transformer infrared spectroscopy, scanning electron microscopy and energy dispersive spectroscopy. Furthermore, the bioactivity of the materials was determined using the simulated biological fluid (SBF) method. Results showed that the natural HAp exhibited better crystallographic properties. Moreover, according to these results, HAp obtained from porcine bones contains traces of elements as Na and Mg that are favorable for the bioactivity, according to the materials behavior when they are immersed in SBF.Laboratório de Hidrogênio, Coppe - Universidade Federal do Rio de Janeiroem cooperação com a Associação Brasileira do Hidrogênio, ABH22018-01-01info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersiontext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S1517-70762018000400408Matéria (Rio de Janeiro) v.23 n.4 2018reponame:Matéria (Rio de Janeiro. Online)instname:Matéria (Rio de Janeiro. Online)instacron:RLAM10.1590/s1517-707620180004.0551info:eu-repo/semantics/openAccessSossa,Paola Andrea ForeroGiraldo,Belarmino SeguraGarcia,Beatriz Clemencia GalvizParra,Elisabeth RestrepoArango,Pedro Jose Arangoeng2018-12-03T00:00:00Zoai:scielo:S1517-70762018000400408Revistahttp://www.materia.coppe.ufrj.br/https://old.scielo.br/oai/scielo-oai.php||materia@labh2.coppe.ufrj.br1517-70761517-7076opendoar:2018-12-03T00:00Matéria (Rio de Janeiro. Online) - Matéria (Rio de Janeiro. Online)false |
dc.title.none.fl_str_mv |
Comparative study between natural and synthetic Hydroxyapatite: structural, morphological and bioactivity properties |
title |
Comparative study between natural and synthetic Hydroxyapatite: structural, morphological and bioactivity properties |
spellingShingle |
Comparative study between natural and synthetic Hydroxyapatite: structural, morphological and bioactivity properties Sossa,Paola Andrea Forero Hydroxyapatite porcine bones chemical precipitation simulated biological fluid |
title_short |
Comparative study between natural and synthetic Hydroxyapatite: structural, morphological and bioactivity properties |
title_full |
Comparative study between natural and synthetic Hydroxyapatite: structural, morphological and bioactivity properties |
title_fullStr |
Comparative study between natural and synthetic Hydroxyapatite: structural, morphological and bioactivity properties |
title_full_unstemmed |
Comparative study between natural and synthetic Hydroxyapatite: structural, morphological and bioactivity properties |
title_sort |
Comparative study between natural and synthetic Hydroxyapatite: structural, morphological and bioactivity properties |
author |
Sossa,Paola Andrea Forero |
author_facet |
Sossa,Paola Andrea Forero Giraldo,Belarmino Segura Garcia,Beatriz Clemencia Galviz Parra,Elisabeth Restrepo Arango,Pedro Jose Arango |
author_role |
author |
author2 |
Giraldo,Belarmino Segura Garcia,Beatriz Clemencia Galviz Parra,Elisabeth Restrepo Arango,Pedro Jose Arango |
author2_role |
author author author author |
dc.contributor.author.fl_str_mv |
Sossa,Paola Andrea Forero Giraldo,Belarmino Segura Garcia,Beatriz Clemencia Galviz Parra,Elisabeth Restrepo Arango,Pedro Jose Arango |
dc.subject.por.fl_str_mv |
Hydroxyapatite porcine bones chemical precipitation simulated biological fluid |
topic |
Hydroxyapatite porcine bones chemical precipitation simulated biological fluid |
description |
ABSTRACT In this work, a study of hydroxyapatite (HAp) powders obtained using both, porcine bones and chemical precursors was carried put. In the case of HAp obtained by means of porcine bones, physical processes as cooking, washing and milling were developed, for removing the organic material from the bones; after that, the powders were submitted to a thermal treatment at 800 °C, during 12 h. This procedure was carried out without adding chemical alkalines that are harmful for the environment and the human health. On the other hand, HAp powders were also synthetized using the chemical precipitation method widely reported, showing successful results. Moreover, both kind of powders were characterized using x ray diffraction, Fourier transformer infrared spectroscopy, scanning electron microscopy and energy dispersive spectroscopy. Furthermore, the bioactivity of the materials was determined using the simulated biological fluid (SBF) method. Results showed that the natural HAp exhibited better crystallographic properties. Moreover, according to these results, HAp obtained from porcine bones contains traces of elements as Na and Mg that are favorable for the bioactivity, according to the materials behavior when they are immersed in SBF. |
publishDate |
2018 |
dc.date.none.fl_str_mv |
2018-01-01 |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1517-70762018000400408 |
url |
http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1517-70762018000400408 |
dc.language.iso.fl_str_mv |
eng |
language |
eng |
dc.relation.none.fl_str_mv |
10.1590/s1517-707620180004.0551 |
dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess |
eu_rights_str_mv |
openAccess |
dc.format.none.fl_str_mv |
text/html |
dc.publisher.none.fl_str_mv |
Laboratório de Hidrogênio, Coppe - Universidade Federal do Rio de Janeiro em cooperação com a Associação Brasileira do Hidrogênio, ABH2 |
publisher.none.fl_str_mv |
Laboratório de Hidrogênio, Coppe - Universidade Federal do Rio de Janeiro em cooperação com a Associação Brasileira do Hidrogênio, ABH2 |
dc.source.none.fl_str_mv |
Matéria (Rio de Janeiro) v.23 n.4 2018 reponame:Matéria (Rio de Janeiro. Online) instname:Matéria (Rio de Janeiro. Online) instacron:RLAM |
instname_str |
Matéria (Rio de Janeiro. Online) |
instacron_str |
RLAM |
institution |
RLAM |
reponame_str |
Matéria (Rio de Janeiro. Online) |
collection |
Matéria (Rio de Janeiro. Online) |
repository.name.fl_str_mv |
Matéria (Rio de Janeiro. Online) - Matéria (Rio de Janeiro. Online) |
repository.mail.fl_str_mv |
||materia@labh2.coppe.ufrj.br |
_version_ |
1752126691481747456 |