Pentacyclic triterpenes and other constituents in propolis extract from Melipona beecheii collected in Yucatan, México
Autor(a) principal: | |
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Data de Publicação: | 2019 |
Outros Autores: | , , , , , |
Tipo de documento: | Artigo |
Idioma: | eng |
Título da fonte: | Revista Brasileira de Farmacognosia (Online) |
Texto Completo: | http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0102-695X2019000300358 |
Resumo: | ABSTRACT Thirteen pentacyclic triterpenes, methyl 3-oxours-12-en-23-oate, marsformosanone, taraxerone, β-amyrenone, α-amyrenone, lupenone, 24-methylencycloartan-3-one, moretenol acetate, β-amyrin acetate, germanicol acetate, 24-methylencycloartanyl acetate, β-amyrin, and α-amyrin were identified in a chloroform-methanol propolis extract from Melipona beecheii. Additionally, were identified in this propolis, hexadecanoic acid, methyl ester, octadecanoic acid, methyl ester and 1-triacontanol. The purification of the propolis extract was carried out using different chromatographic techniques, including vacuum liquid chromatography, gravity column chromatography and gel filtration chromatography Sephadex LH-20. The identification of the metabolites was performed using mass spectrometry. |
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Pentacyclic triterpenes and other constituents in propolis extract from Melipona beecheii collected in Yucatan, MéxicoStingless beePropolisPentacyclic triterpenesβ-Amyrin acetateGermanicol acetateLupenoneABSTRACT Thirteen pentacyclic triterpenes, methyl 3-oxours-12-en-23-oate, marsformosanone, taraxerone, β-amyrenone, α-amyrenone, lupenone, 24-methylencycloartan-3-one, moretenol acetate, β-amyrin acetate, germanicol acetate, 24-methylencycloartanyl acetate, β-amyrin, and α-amyrin were identified in a chloroform-methanol propolis extract from Melipona beecheii. Additionally, were identified in this propolis, hexadecanoic acid, methyl ester, octadecanoic acid, methyl ester and 1-triacontanol. The purification of the propolis extract was carried out using different chromatographic techniques, including vacuum liquid chromatography, gravity column chromatography and gel filtration chromatography Sephadex LH-20. The identification of the metabolites was performed using mass spectrometry.Sociedade Brasileira de Farmacognosia2019-06-01info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersiontext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S0102-695X2019000300358Revista Brasileira de Farmacognosia v.29 n.3 2019reponame:Revista Brasileira de Farmacognosia (Online)instname:Sociedade Brasileira de Farmacognosia (SBFgnosia)instacron:SBFGNOSIA10.1016/j.bjp.2019.01.006info:eu-repo/semantics/openAccessYam-Puc,AlejandroSantana-Hernández,Aarón A.Yah-Nahuat,Pamela N.Ramón-Sierra,Jesús M.Cáceres-Farfán,Mirbella R.Borges-Argáez,Rocío L.Ortiz-Vázquez,Elizabetheng2019-08-22T00:00:00Zoai:scielo:S0102-695X2019000300358Revistahttp://www.sbfgnosia.org.br/revista/https://old.scielo.br/oai/scielo-oai.phprbgnosia@ltf.ufpb.br1981-528X0102-695Xopendoar:2019-08-22T00:00Revista Brasileira de Farmacognosia (Online) - Sociedade Brasileira de Farmacognosia (SBFgnosia)false |
dc.title.none.fl_str_mv |
Pentacyclic triterpenes and other constituents in propolis extract from Melipona beecheii collected in Yucatan, México |
title |
Pentacyclic triterpenes and other constituents in propolis extract from Melipona beecheii collected in Yucatan, México |
spellingShingle |
Pentacyclic triterpenes and other constituents in propolis extract from Melipona beecheii collected in Yucatan, México Yam-Puc,Alejandro Stingless bee Propolis Pentacyclic triterpenes β-Amyrin acetate Germanicol acetate Lupenone |
title_short |
Pentacyclic triterpenes and other constituents in propolis extract from Melipona beecheii collected in Yucatan, México |
title_full |
Pentacyclic triterpenes and other constituents in propolis extract from Melipona beecheii collected in Yucatan, México |
title_fullStr |
Pentacyclic triterpenes and other constituents in propolis extract from Melipona beecheii collected in Yucatan, México |
title_full_unstemmed |
Pentacyclic triterpenes and other constituents in propolis extract from Melipona beecheii collected in Yucatan, México |
title_sort |
Pentacyclic triterpenes and other constituents in propolis extract from Melipona beecheii collected in Yucatan, México |
author |
Yam-Puc,Alejandro |
author_facet |
Yam-Puc,Alejandro Santana-Hernández,Aarón A. Yah-Nahuat,Pamela N. Ramón-Sierra,Jesús M. Cáceres-Farfán,Mirbella R. Borges-Argáez,Rocío L. Ortiz-Vázquez,Elizabeth |
author_role |
author |
author2 |
Santana-Hernández,Aarón A. Yah-Nahuat,Pamela N. Ramón-Sierra,Jesús M. Cáceres-Farfán,Mirbella R. Borges-Argáez,Rocío L. Ortiz-Vázquez,Elizabeth |
author2_role |
author author author author author author |
dc.contributor.author.fl_str_mv |
Yam-Puc,Alejandro Santana-Hernández,Aarón A. Yah-Nahuat,Pamela N. Ramón-Sierra,Jesús M. Cáceres-Farfán,Mirbella R. Borges-Argáez,Rocío L. Ortiz-Vázquez,Elizabeth |
dc.subject.por.fl_str_mv |
Stingless bee Propolis Pentacyclic triterpenes β-Amyrin acetate Germanicol acetate Lupenone |
topic |
Stingless bee Propolis Pentacyclic triterpenes β-Amyrin acetate Germanicol acetate Lupenone |
description |
ABSTRACT Thirteen pentacyclic triterpenes, methyl 3-oxours-12-en-23-oate, marsformosanone, taraxerone, β-amyrenone, α-amyrenone, lupenone, 24-methylencycloartan-3-one, moretenol acetate, β-amyrin acetate, germanicol acetate, 24-methylencycloartanyl acetate, β-amyrin, and α-amyrin were identified in a chloroform-methanol propolis extract from Melipona beecheii. Additionally, were identified in this propolis, hexadecanoic acid, methyl ester, octadecanoic acid, methyl ester and 1-triacontanol. The purification of the propolis extract was carried out using different chromatographic techniques, including vacuum liquid chromatography, gravity column chromatography and gel filtration chromatography Sephadex LH-20. The identification of the metabolites was performed using mass spectrometry. |
publishDate |
2019 |
dc.date.none.fl_str_mv |
2019-06-01 |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0102-695X2019000300358 |
url |
http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0102-695X2019000300358 |
dc.language.iso.fl_str_mv |
eng |
language |
eng |
dc.relation.none.fl_str_mv |
10.1016/j.bjp.2019.01.006 |
dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess |
eu_rights_str_mv |
openAccess |
dc.format.none.fl_str_mv |
text/html |
dc.publisher.none.fl_str_mv |
Sociedade Brasileira de Farmacognosia |
publisher.none.fl_str_mv |
Sociedade Brasileira de Farmacognosia |
dc.source.none.fl_str_mv |
Revista Brasileira de Farmacognosia v.29 n.3 2019 reponame:Revista Brasileira de Farmacognosia (Online) instname:Sociedade Brasileira de Farmacognosia (SBFgnosia) instacron:SBFGNOSIA |
instname_str |
Sociedade Brasileira de Farmacognosia (SBFgnosia) |
instacron_str |
SBFGNOSIA |
institution |
SBFGNOSIA |
reponame_str |
Revista Brasileira de Farmacognosia (Online) |
collection |
Revista Brasileira de Farmacognosia (Online) |
repository.name.fl_str_mv |
Revista Brasileira de Farmacognosia (Online) - Sociedade Brasileira de Farmacognosia (SBFgnosia) |
repository.mail.fl_str_mv |
rbgnosia@ltf.ufpb.br |
_version_ |
1752122471159431168 |