Synthesis and characterization of a linker for primary amines used in the solid phase organic synthesis of spermidine

Detalhes bibliográficos
Autor(a) principal: Silva,Emerson T. da
Data de Publicação: 2011
Outros Autores: Gil,Rosane A. S. San, Caldarelli,Stefano, Ziarelli,Fabio, Lima,Edson L. S.
Tipo de documento: Artigo
Idioma: eng
Título da fonte: Journal of the Brazilian Chemical Society (Online)
Texto Completo: http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532011000100011
Resumo: A linker resin for the synthesis of functionalized spermidine in good yield is described, along with its characterization by infrared (IR), 13C solid-state nuclear magnetic resonance with cross polarization and magic angle spinning (13C CPMAS NMR) and ¹H high resolution magic angle spinning nuclear magnetic resonance (¹H HRMAS NMR. This linker has been regenerated after cleavage of spermidine and re-used without loss of efficiency.
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spelling Synthesis and characterization of a linker for primary amines used in the solid phase organic synthesis of spermidinepolyamines13C CPMAS NMRHRMAS NMRsolid phase organic synthesisspermidineA linker resin for the synthesis of functionalized spermidine in good yield is described, along with its characterization by infrared (IR), 13C solid-state nuclear magnetic resonance with cross polarization and magic angle spinning (13C CPMAS NMR) and ¹H high resolution magic angle spinning nuclear magnetic resonance (¹H HRMAS NMR. This linker has been regenerated after cleavage of spermidine and re-used without loss of efficiency.Sociedade Brasileira de Química2011-01-01info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersiontext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532011000100011Journal of the Brazilian Chemical Society v.22 n.1 2011reponame:Journal of the Brazilian Chemical Society (Online)instname:Sociedade Brasileira de Química (SBQ)instacron:SBQ10.1590/S0103-50532011000100011info:eu-repo/semantics/openAccessSilva,Emerson T. daGil,Rosane A. S. SanCaldarelli,StefanoZiarelli,FabioLima,Edson L. S.eng2011-01-26T00:00:00Zoai:scielo:S0103-50532011000100011Revistahttp://jbcs.sbq.org.brONGhttps://old.scielo.br/oai/scielo-oai.php||office@jbcs.sbq.org.br1678-47900103-5053opendoar:2011-01-26T00:00Journal of the Brazilian Chemical Society (Online) - Sociedade Brasileira de Química (SBQ)false
dc.title.none.fl_str_mv Synthesis and characterization of a linker for primary amines used in the solid phase organic synthesis of spermidine
title Synthesis and characterization of a linker for primary amines used in the solid phase organic synthesis of spermidine
spellingShingle Synthesis and characterization of a linker for primary amines used in the solid phase organic synthesis of spermidine
Silva,Emerson T. da
polyamines
13C CPMAS NMR
HRMAS NMR
solid phase organic synthesis
spermidine
title_short Synthesis and characterization of a linker for primary amines used in the solid phase organic synthesis of spermidine
title_full Synthesis and characterization of a linker for primary amines used in the solid phase organic synthesis of spermidine
title_fullStr Synthesis and characterization of a linker for primary amines used in the solid phase organic synthesis of spermidine
title_full_unstemmed Synthesis and characterization of a linker for primary amines used in the solid phase organic synthesis of spermidine
title_sort Synthesis and characterization of a linker for primary amines used in the solid phase organic synthesis of spermidine
author Silva,Emerson T. da
author_facet Silva,Emerson T. da
Gil,Rosane A. S. San
Caldarelli,Stefano
Ziarelli,Fabio
Lima,Edson L. S.
author_role author
author2 Gil,Rosane A. S. San
Caldarelli,Stefano
Ziarelli,Fabio
Lima,Edson L. S.
author2_role author
author
author
author
dc.contributor.author.fl_str_mv Silva,Emerson T. da
Gil,Rosane A. S. San
Caldarelli,Stefano
Ziarelli,Fabio
Lima,Edson L. S.
dc.subject.por.fl_str_mv polyamines
13C CPMAS NMR
HRMAS NMR
solid phase organic synthesis
spermidine
topic polyamines
13C CPMAS NMR
HRMAS NMR
solid phase organic synthesis
spermidine
description A linker resin for the synthesis of functionalized spermidine in good yield is described, along with its characterization by infrared (IR), 13C solid-state nuclear magnetic resonance with cross polarization and magic angle spinning (13C CPMAS NMR) and ¹H high resolution magic angle spinning nuclear magnetic resonance (¹H HRMAS NMR. This linker has been regenerated after cleavage of spermidine and re-used without loss of efficiency.
publishDate 2011
dc.date.none.fl_str_mv 2011-01-01
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532011000100011
url http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532011000100011
dc.language.iso.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv 10.1590/S0103-50532011000100011
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv text/html
dc.publisher.none.fl_str_mv Sociedade Brasileira de Química
publisher.none.fl_str_mv Sociedade Brasileira de Química
dc.source.none.fl_str_mv Journal of the Brazilian Chemical Society v.22 n.1 2011
reponame:Journal of the Brazilian Chemical Society (Online)
instname:Sociedade Brasileira de Química (SBQ)
instacron:SBQ
instname_str Sociedade Brasileira de Química (SBQ)
instacron_str SBQ
institution SBQ
reponame_str Journal of the Brazilian Chemical Society (Online)
collection Journal of the Brazilian Chemical Society (Online)
repository.name.fl_str_mv Journal of the Brazilian Chemical Society (Online) - Sociedade Brasileira de Química (SBQ)
repository.mail.fl_str_mv ||office@jbcs.sbq.org.br
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