Condensed Tannins from the bark of Guazuma ulmifolia Lam. (Sterculiaceae)
Autor(a) principal: | |
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Data de Publicação: | 2009 |
Outros Autores: | , , |
Tipo de documento: | Artigo |
Idioma: | eng |
Título da fonte: | Journal of the Brazilian Chemical Society (Online) |
Texto Completo: | http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532009000600016 |
Resumo: | From the bark of Guazuma ulmifolia Lam. (Sterculiaceae), nine compounds were isolated and identified: ent-catechin, epicatechin, ent-gallocatechin, epigallocatechin, epiafzelechin-(4β→8)-epicatechin, epicatechin-(4β→8)-catechin (procyanidin B1), epicatechin-(4β→8)-epicatechin (procyanidin B2), epicatechin-(4β→8)-epigallocatechin, and the new compound 4'-O-methyl-epiafzelechin. Their structures were elucidated on the basis of spectral and literature data. HPLC fingerprint analysis of the semipurified extract was performed on a C18 column, with a mixture of acetonitrile (0.05% trifluoroacetic acid):water (0.05% trifluoroacetic acid) (v/v) with a flow rate of 0.8 mL min-1. The sample injection volume was 100 µL and the wavelength was 210 nm. |
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Condensed Tannins from the bark of Guazuma ulmifolia Lam. (Sterculiaceae)Guazuma ulmifoliacondensed tanninsHPLCfingerprintFrom the bark of Guazuma ulmifolia Lam. (Sterculiaceae), nine compounds were isolated and identified: ent-catechin, epicatechin, ent-gallocatechin, epigallocatechin, epiafzelechin-(4β→8)-epicatechin, epicatechin-(4β→8)-catechin (procyanidin B1), epicatechin-(4β→8)-epicatechin (procyanidin B2), epicatechin-(4β→8)-epigallocatechin, and the new compound 4'-O-methyl-epiafzelechin. Their structures were elucidated on the basis of spectral and literature data. HPLC fingerprint analysis of the semipurified extract was performed on a C18 column, with a mixture of acetonitrile (0.05% trifluoroacetic acid):water (0.05% trifluoroacetic acid) (v/v) with a flow rate of 0.8 mL min-1. The sample injection volume was 100 µL and the wavelength was 210 nm.Sociedade Brasileira de Química2009-01-01info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersiontext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532009000600016Journal of the Brazilian Chemical Society v.20 n.6 2009reponame:Journal of the Brazilian Chemical Society (Online)instname:Sociedade Brasileira de Química (SBQ)instacron:SBQ10.1590/S0103-50532009000600016info:eu-repo/semantics/openAccessLopes,Gisely C.Rocha,Juliana C. B.Almeida,Glalber C. deMello,João C. P. deeng2009-08-04T00:00:00Zoai:scielo:S0103-50532009000600016Revistahttp://jbcs.sbq.org.brONGhttps://old.scielo.br/oai/scielo-oai.php||office@jbcs.sbq.org.br1678-47900103-5053opendoar:2009-08-04T00:00Journal of the Brazilian Chemical Society (Online) - Sociedade Brasileira de Química (SBQ)false |
dc.title.none.fl_str_mv |
Condensed Tannins from the bark of Guazuma ulmifolia Lam. (Sterculiaceae) |
title |
Condensed Tannins from the bark of Guazuma ulmifolia Lam. (Sterculiaceae) |
spellingShingle |
Condensed Tannins from the bark of Guazuma ulmifolia Lam. (Sterculiaceae) Lopes,Gisely C. Guazuma ulmifolia condensed tannins HPLC fingerprint |
title_short |
Condensed Tannins from the bark of Guazuma ulmifolia Lam. (Sterculiaceae) |
title_full |
Condensed Tannins from the bark of Guazuma ulmifolia Lam. (Sterculiaceae) |
title_fullStr |
Condensed Tannins from the bark of Guazuma ulmifolia Lam. (Sterculiaceae) |
title_full_unstemmed |
Condensed Tannins from the bark of Guazuma ulmifolia Lam. (Sterculiaceae) |
title_sort |
Condensed Tannins from the bark of Guazuma ulmifolia Lam. (Sterculiaceae) |
author |
Lopes,Gisely C. |
author_facet |
Lopes,Gisely C. Rocha,Juliana C. B. Almeida,Glalber C. de Mello,João C. P. de |
author_role |
author |
author2 |
Rocha,Juliana C. B. Almeida,Glalber C. de Mello,João C. P. de |
author2_role |
author author author |
dc.contributor.author.fl_str_mv |
Lopes,Gisely C. Rocha,Juliana C. B. Almeida,Glalber C. de Mello,João C. P. de |
dc.subject.por.fl_str_mv |
Guazuma ulmifolia condensed tannins HPLC fingerprint |
topic |
Guazuma ulmifolia condensed tannins HPLC fingerprint |
description |
From the bark of Guazuma ulmifolia Lam. (Sterculiaceae), nine compounds were isolated and identified: ent-catechin, epicatechin, ent-gallocatechin, epigallocatechin, epiafzelechin-(4β→8)-epicatechin, epicatechin-(4β→8)-catechin (procyanidin B1), epicatechin-(4β→8)-epicatechin (procyanidin B2), epicatechin-(4β→8)-epigallocatechin, and the new compound 4'-O-methyl-epiafzelechin. Their structures were elucidated on the basis of spectral and literature data. HPLC fingerprint analysis of the semipurified extract was performed on a C18 column, with a mixture of acetonitrile (0.05% trifluoroacetic acid):water (0.05% trifluoroacetic acid) (v/v) with a flow rate of 0.8 mL min-1. The sample injection volume was 100 µL and the wavelength was 210 nm. |
publishDate |
2009 |
dc.date.none.fl_str_mv |
2009-01-01 |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532009000600016 |
url |
http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532009000600016 |
dc.language.iso.fl_str_mv |
eng |
language |
eng |
dc.relation.none.fl_str_mv |
10.1590/S0103-50532009000600016 |
dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess |
eu_rights_str_mv |
openAccess |
dc.format.none.fl_str_mv |
text/html |
dc.publisher.none.fl_str_mv |
Sociedade Brasileira de Química |
publisher.none.fl_str_mv |
Sociedade Brasileira de Química |
dc.source.none.fl_str_mv |
Journal of the Brazilian Chemical Society v.20 n.6 2009 reponame:Journal of the Brazilian Chemical Society (Online) instname:Sociedade Brasileira de Química (SBQ) instacron:SBQ |
instname_str |
Sociedade Brasileira de Química (SBQ) |
instacron_str |
SBQ |
institution |
SBQ |
reponame_str |
Journal of the Brazilian Chemical Society (Online) |
collection |
Journal of the Brazilian Chemical Society (Online) |
repository.name.fl_str_mv |
Journal of the Brazilian Chemical Society (Online) - Sociedade Brasileira de Química (SBQ) |
repository.mail.fl_str_mv |
||office@jbcs.sbq.org.br |
_version_ |
1750318169903333376 |