Analysis of volatiles in fluid inclusions by direct online crushing mass spectrometry
Autor(a) principal: | |
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Data de Publicação: | 2011 |
Outros Autores: | , |
Tipo de documento: | Artigo |
Idioma: | eng |
Título da fonte: | Journal of the Brazilian Chemical Society (Online) |
Texto Completo: | http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532011000300005 |
Resumo: | A new tool has been increasingly used in organic geochemistry; it is the application of fluid inclusions hosted in minerals, mainly quartz, from rock samples recovered in basin wells. In this paper we develop a new practical screening method to identify the presence of petroleum in fluid inclusions from siliciclastic and carbonatic minerals. The method is called detection of petroleum inclusions and allows analyzing the presence of volatiles in oil fluid inclusions extracted by online crushing from cuttings samples. This method offers the advantage of working with solid samples, as a micro-scaled sealed vessel (MSSV) system. Moreover it is simple, relatively fast and presents a satisfactory reproducibility. For the successful analysis it is essential to carefully control the analytical procedures, including the cleaning of samples and blank runs. Results were compared with previously reported methods |
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Analysis of volatiles in fluid inclusions by direct online crushing mass spectrometryfluid inclusionspetroleummass spectrometryhydrocarbonsquartzA new tool has been increasingly used in organic geochemistry; it is the application of fluid inclusions hosted in minerals, mainly quartz, from rock samples recovered in basin wells. In this paper we develop a new practical screening method to identify the presence of petroleum in fluid inclusions from siliciclastic and carbonatic minerals. The method is called detection of petroleum inclusions and allows analyzing the presence of volatiles in oil fluid inclusions extracted by online crushing from cuttings samples. This method offers the advantage of working with solid samples, as a micro-scaled sealed vessel (MSSV) system. Moreover it is simple, relatively fast and presents a satisfactory reproducibility. For the successful analysis it is essential to carefully control the analytical procedures, including the cleaning of samples and blank runs. Results were compared with previously reported methodsSociedade Brasileira de Química2011-03-01info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersiontext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532011000300005Journal of the Brazilian Chemical Society v.22 n.3 2011reponame:Journal of the Brazilian Chemical Society (Online)instname:Sociedade Brasileira de Química (SBQ)instacron:SBQ10.1590/S0103-50532011000300005info:eu-repo/semantics/openAccessJorge,SandraCoelho,Carlos E. SAquino-Neto,Francisco Radler deeng2011-03-25T00:00:00Zoai:scielo:S0103-50532011000300005Revistahttp://jbcs.sbq.org.brONGhttps://old.scielo.br/oai/scielo-oai.php||office@jbcs.sbq.org.br1678-47900103-5053opendoar:2011-03-25T00:00Journal of the Brazilian Chemical Society (Online) - Sociedade Brasileira de Química (SBQ)false |
dc.title.none.fl_str_mv |
Analysis of volatiles in fluid inclusions by direct online crushing mass spectrometry |
title |
Analysis of volatiles in fluid inclusions by direct online crushing mass spectrometry |
spellingShingle |
Analysis of volatiles in fluid inclusions by direct online crushing mass spectrometry Jorge,Sandra fluid inclusions petroleum mass spectrometry hydrocarbons quartz |
title_short |
Analysis of volatiles in fluid inclusions by direct online crushing mass spectrometry |
title_full |
Analysis of volatiles in fluid inclusions by direct online crushing mass spectrometry |
title_fullStr |
Analysis of volatiles in fluid inclusions by direct online crushing mass spectrometry |
title_full_unstemmed |
Analysis of volatiles in fluid inclusions by direct online crushing mass spectrometry |
title_sort |
Analysis of volatiles in fluid inclusions by direct online crushing mass spectrometry |
author |
Jorge,Sandra |
author_facet |
Jorge,Sandra Coelho,Carlos E. S Aquino-Neto,Francisco Radler de |
author_role |
author |
author2 |
Coelho,Carlos E. S Aquino-Neto,Francisco Radler de |
author2_role |
author author |
dc.contributor.author.fl_str_mv |
Jorge,Sandra Coelho,Carlos E. S Aquino-Neto,Francisco Radler de |
dc.subject.por.fl_str_mv |
fluid inclusions petroleum mass spectrometry hydrocarbons quartz |
topic |
fluid inclusions petroleum mass spectrometry hydrocarbons quartz |
description |
A new tool has been increasingly used in organic geochemistry; it is the application of fluid inclusions hosted in minerals, mainly quartz, from rock samples recovered in basin wells. In this paper we develop a new practical screening method to identify the presence of petroleum in fluid inclusions from siliciclastic and carbonatic minerals. The method is called detection of petroleum inclusions and allows analyzing the presence of volatiles in oil fluid inclusions extracted by online crushing from cuttings samples. This method offers the advantage of working with solid samples, as a micro-scaled sealed vessel (MSSV) system. Moreover it is simple, relatively fast and presents a satisfactory reproducibility. For the successful analysis it is essential to carefully control the analytical procedures, including the cleaning of samples and blank runs. Results were compared with previously reported methods |
publishDate |
2011 |
dc.date.none.fl_str_mv |
2011-03-01 |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532011000300005 |
url |
http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532011000300005 |
dc.language.iso.fl_str_mv |
eng |
language |
eng |
dc.relation.none.fl_str_mv |
10.1590/S0103-50532011000300005 |
dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess |
eu_rights_str_mv |
openAccess |
dc.format.none.fl_str_mv |
text/html |
dc.publisher.none.fl_str_mv |
Sociedade Brasileira de Química |
publisher.none.fl_str_mv |
Sociedade Brasileira de Química |
dc.source.none.fl_str_mv |
Journal of the Brazilian Chemical Society v.22 n.3 2011 reponame:Journal of the Brazilian Chemical Society (Online) instname:Sociedade Brasileira de Química (SBQ) instacron:SBQ |
instname_str |
Sociedade Brasileira de Química (SBQ) |
instacron_str |
SBQ |
institution |
SBQ |
reponame_str |
Journal of the Brazilian Chemical Society (Online) |
collection |
Journal of the Brazilian Chemical Society (Online) |
repository.name.fl_str_mv |
Journal of the Brazilian Chemical Society (Online) - Sociedade Brasileira de Química (SBQ) |
repository.mail.fl_str_mv |
||office@jbcs.sbq.org.br |
_version_ |
1750318171921842176 |