Bagaço de cana-de-açúcar e raízes de alface empregados como biossorventes de íons metálicos em meio aquoso
Autor(a) principal: | |
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Data de Publicação: | 2017 |
Tipo de documento: | Dissertação |
Idioma: | por |
Título da fonte: | Repositório Institucional da UFSCAR |
Texto Completo: | https://repositorio.ufscar.br/handle/ufscar/9248 |
Resumo: | Sugarcane bagasse and hydroponic lettuce roots were used as biosorbents for Cu(II), Fe(II), Zn(II) and Mn(II) removal from mono and multielement solutions, as well as in lake water, at pH 5.5, in batch processes. These biomasses were studied in natura (lettuce roots, NLR, and sugarcane bagasse, NSB) and chemically modified with HNO3 (lettuce roots, MLR, and sugarcane bagasse, MSB). The results showed that higher adsorption efficiency was achieved with the modified biomass, with the exception of lettuce roots, which also presented similar efficiency when used in natura. The removal experimental quantities (qexp) in monoelement solution, calculated using the Langmuir isothermal model for Cu(II), Fe(II), Zn(II) and Mn(II) were respectively, 1.22, 1.08, 1.40 and 1.23 mg g-1 in NLR, and 1.69, 1.68, 1.09 and 1.48 mg g-1 in MLR and 0.58, 0.036, 0.40 e 0.24 mg g-1 in NSB, and 1.30, 1.41, 1.55 and 1.02 mg g-1 in MSB. The removal experimental quantities (qexp) in multielement solution containing Cu(II), Fe(II), Zn(II), and Mn(II) in multielement solution were 1.28, 1.41, 1.29 and 1.05 mg g-1 in NLR, and 1.30, 1.09, 1.72 e 1.64 mg g-1 in MLR, and 0.47, 0.58, 0.09 and 0.02 mg g-1 in NSB, and 1.30, 1.09, 1.06 and 1.62 mg g-1 in MSB, respectively. We used the isothermal models of Langmuir and Freundlich, however for multielement solutions the adsorption did not conform to the Freundlich isotherm. In the kinetic studies with modified biomasses, sorption was achieved in the first 5 minutes and reached equilibrium in 30 min. The O-H, C-O-C, C-C, C-H, and C=O groups were found in the characterization of the biomass sorption sites by Fourier transform infrared spectrometry (FTIR). In the determination of the biomass surface charges using blue methylene and red amaranth dyes, there was a predominance of negative charges. Modified biomasses were used in the adsorption of Cu(II), Fe(II), Zn(II), and Mn(II) in lake water, in which retention of 24.31, 14.50, 8.21, and 8.03 mg g-1 by MLR, and 13.15, 10.50, 5.14 and 6,10 mg g-1 by MSB was found, respectively. |
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Milani, Priscila AparecidaCarrilho, Elma Neide Vasconcelos Martinshttp://lattes.cnpq.br/5147872007117167http://lattes.cnpq.br/2420667904233275c0efcaf9-1125-4b98-a7fa-03f7560294132018-01-11T18:10:11Z2018-01-11T18:10:11Z2017-06-05MILANI, Priscila Aparecida. Bagaço de cana-de-açúcar e raízes de alface empregados como biossorventes de íons metálicos em meio aquoso. 2017. Dissertação (Mestrado em Agricultura e Ambiente) – Universidade Federal de São Carlos, Araras, 2017. Disponível em: https://repositorio.ufscar.br/handle/ufscar/9248.https://repositorio.ufscar.br/handle/ufscar/9248Sugarcane bagasse and hydroponic lettuce roots were used as biosorbents for Cu(II), Fe(II), Zn(II) and Mn(II) removal from mono and multielement solutions, as well as in lake water, at pH 5.5, in batch processes. These biomasses were studied in natura (lettuce roots, NLR, and sugarcane bagasse, NSB) and chemically modified with HNO3 (lettuce roots, MLR, and sugarcane bagasse, MSB). The results showed that higher adsorption efficiency was achieved with the modified biomass, with the exception of lettuce roots, which also presented similar efficiency when used in natura. The removal experimental quantities (qexp) in monoelement solution, calculated using the Langmuir isothermal model for Cu(II), Fe(II), Zn(II) and Mn(II) were respectively, 1.22, 1.08, 1.40 and 1.23 mg g-1 in NLR, and 1.69, 1.68, 1.09 and 1.48 mg g-1 in MLR and 0.58, 0.036, 0.40 e 0.24 mg g-1 in NSB, and 1.30, 1.41, 1.55 and 1.02 mg g-1 in MSB. The removal experimental quantities (qexp) in multielement solution containing Cu(II), Fe(II), Zn(II), and Mn(II) in multielement solution were 1.28, 1.41, 1.29 and 1.05 mg g-1 in NLR, and 1.30, 1.09, 1.72 e 1.64 mg g-1 in MLR, and 0.47, 0.58, 0.09 and 0.02 mg g-1 in NSB, and 1.30, 1.09, 1.06 and 1.62 mg g-1 in MSB, respectively. We used the isothermal models of Langmuir and Freundlich, however for multielement solutions the adsorption did not conform to the Freundlich isotherm. In the kinetic studies with modified biomasses, sorption was achieved in the first 5 minutes and reached equilibrium in 30 min. The O-H, C-O-C, C-C, C-H, and C=O groups were found in the characterization of the biomass sorption sites by Fourier transform infrared spectrometry (FTIR). In the determination of the biomass surface charges using blue methylene and red amaranth dyes, there was a predominance of negative charges. Modified biomasses were used in the adsorption of Cu(II), Fe(II), Zn(II), and Mn(II) in lake water, in which retention of 24.31, 14.50, 8.21, and 8.03 mg g-1 by MLR, and 13.15, 10.50, 5.14 and 6,10 mg g-1 by MSB was found, respectively.Biomassas de bagaço de cana-de-açúcar e raízes de alface hidropônica foram empregadas como biossorventes na remoção Cu(II), Fe(II), Zn(II) e Mn(II), em soluções mono e multielementares, assim como em água de lago, em pH 5,5, usando processos em batelada. Estas foram estudadas na forma in natura (raízes de alface, RAN, e bagaço de cana, BCN) e modificadas quimicamente com HNO3 (raízes de alface, RAM, e bagaço de cana, BCM). Os resultados mostraram que maior eficiência de sorção foi obtida com as biomassas modificadas, com exceção das raízes de alface, que também apresentaram semelhante eficiência mesmo in natura. As quantidades experimentais (qexp) de remoção em solução monoelementar Cu(II), Fe(II), Zn(II) e Mn(II) foram, respectivamente, 1,22, 1,08, 1,40 e 1,23 mg g-1 em RAN, e 1,69, 1,68, 1,09 e 1,48 mg g-1 em RAM e 0,58, 0,036, 0,40 e 0,24 mg g-1 em BCN, e 1,30, 1,41, 1,55 e 1,02 mg g-1 em BCM. As quantidades de remoção em solução multielementar contendo Cu(II), Fe(II), Zn(II) e Mn(II) foram 1,28, 1,41, 1,29 e 1,05 mg g-1 em RAN, e 1,30, 1,09, 1,72 e 1,64 mg g-1 em RAM, e 0,47, 0,58, 0,09 e 0,02 mg g-1 em BCN, e 1,30, 1,09, 1,06 e 1,62 mg g-1 para BCM, respectivamente. Foram utilizados os modelos isotérmicos de Langmuir e Freundlich, entretanto para soluções multielementares a sorção não se ajusta à isoterma de Freundlich. Nos estudos de cinética em biomassas modificadas, a sorção foi alcançada nos primeiros 5 minutos e atingiu o equilíbrio em 30 min. Na caracterização dos sítios de sorção das biomassas por espectrometria de infravermelho com transformada de Fourier (FTIR), observou-se a presença dos grupamentos O-H, C-O-C, C-C, C-H, e C=O. Na determinação da carga superficial das biomassas usando os corantes azul de metileno e vermelho amaranto houve predominância de cargas negativas. Biomassas modificadas foram empregadas na sorção de Cu(II), Fe(II), Zn(II) e Mn(II) em amostra de água de lago, e verificou-se retenção de 24,31, 14,50, 8,21 e 8,03 mg g-1, em RAM, e 13,15, 10,50, 5,14 e 6,10 mg g-1 em BCM, respectivamente.Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)porUniversidade Federal de São CarlosCâmpus ArarasPrograma de Pós-Graduação em Agricultura e Ambiente - PPGAA-ArUFSCarBiossorçãoBiomassaBiorremediaçãoDescontaminação de águasBiosorptionBiomassBioremediationWater decontaminationCIENCIAS AGRARIAS::AGRONOMIABagaço de cana-de-açúcar e raízes de alface empregados como biossorventes de íons metálicos em meio aquosoSugarcane bagasse and lettuce roots used as biosorbent of metallic ions in aqueous mediuminfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/masterThesisOnline600600cd6aac36-4ab0-428d-be5c-61bc7099b00binfo:eu-repo/semantics/openAccessreponame:Repositório Institucional da UFSCARinstname:Universidade Federal de São Carlos (UFSCAR)instacron:UFSCARORIGINALMILANI_Priscila_2017.pdfMILANI_Priscila_2017.pdfapplication/pdf2467306https://repositorio.ufscar.br/bitstream/ufscar/9248/8/MILANI_Priscila_2017.pdf76afa6472bdbd78cca5e2a473ed85b98MD58LICENSElicense.txtlicense.txttext/plain; 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dc.title.por.fl_str_mv |
Bagaço de cana-de-açúcar e raízes de alface empregados como biossorventes de íons metálicos em meio aquoso |
dc.title.alternative.eng.fl_str_mv |
Sugarcane bagasse and lettuce roots used as biosorbent of metallic ions in aqueous medium |
title |
Bagaço de cana-de-açúcar e raízes de alface empregados como biossorventes de íons metálicos em meio aquoso |
spellingShingle |
Bagaço de cana-de-açúcar e raízes de alface empregados como biossorventes de íons metálicos em meio aquoso Milani, Priscila Aparecida Biossorção Biomassa Biorremediação Descontaminação de águas Biosorption Biomass Bioremediation Water decontamination CIENCIAS AGRARIAS::AGRONOMIA |
title_short |
Bagaço de cana-de-açúcar e raízes de alface empregados como biossorventes de íons metálicos em meio aquoso |
title_full |
Bagaço de cana-de-açúcar e raízes de alface empregados como biossorventes de íons metálicos em meio aquoso |
title_fullStr |
Bagaço de cana-de-açúcar e raízes de alface empregados como biossorventes de íons metálicos em meio aquoso |
title_full_unstemmed |
Bagaço de cana-de-açúcar e raízes de alface empregados como biossorventes de íons metálicos em meio aquoso |
title_sort |
Bagaço de cana-de-açúcar e raízes de alface empregados como biossorventes de íons metálicos em meio aquoso |
author |
Milani, Priscila Aparecida |
author_facet |
Milani, Priscila Aparecida |
author_role |
author |
dc.contributor.authorlattes.por.fl_str_mv |
http://lattes.cnpq.br/2420667904233275 |
dc.contributor.author.fl_str_mv |
Milani, Priscila Aparecida |
dc.contributor.advisor1.fl_str_mv |
Carrilho, Elma Neide Vasconcelos Martins |
dc.contributor.advisor1Lattes.fl_str_mv |
http://lattes.cnpq.br/5147872007117167 |
dc.contributor.authorID.fl_str_mv |
c0efcaf9-1125-4b98-a7fa-03f756029413 |
contributor_str_mv |
Carrilho, Elma Neide Vasconcelos Martins |
dc.subject.por.fl_str_mv |
Biossorção Biomassa Biorremediação Descontaminação de águas |
topic |
Biossorção Biomassa Biorremediação Descontaminação de águas Biosorption Biomass Bioremediation Water decontamination CIENCIAS AGRARIAS::AGRONOMIA |
dc.subject.eng.fl_str_mv |
Biosorption Biomass Bioremediation Water decontamination |
dc.subject.cnpq.fl_str_mv |
CIENCIAS AGRARIAS::AGRONOMIA |
description |
Sugarcane bagasse and hydroponic lettuce roots were used as biosorbents for Cu(II), Fe(II), Zn(II) and Mn(II) removal from mono and multielement solutions, as well as in lake water, at pH 5.5, in batch processes. These biomasses were studied in natura (lettuce roots, NLR, and sugarcane bagasse, NSB) and chemically modified with HNO3 (lettuce roots, MLR, and sugarcane bagasse, MSB). The results showed that higher adsorption efficiency was achieved with the modified biomass, with the exception of lettuce roots, which also presented similar efficiency when used in natura. The removal experimental quantities (qexp) in monoelement solution, calculated using the Langmuir isothermal model for Cu(II), Fe(II), Zn(II) and Mn(II) were respectively, 1.22, 1.08, 1.40 and 1.23 mg g-1 in NLR, and 1.69, 1.68, 1.09 and 1.48 mg g-1 in MLR and 0.58, 0.036, 0.40 e 0.24 mg g-1 in NSB, and 1.30, 1.41, 1.55 and 1.02 mg g-1 in MSB. The removal experimental quantities (qexp) in multielement solution containing Cu(II), Fe(II), Zn(II), and Mn(II) in multielement solution were 1.28, 1.41, 1.29 and 1.05 mg g-1 in NLR, and 1.30, 1.09, 1.72 e 1.64 mg g-1 in MLR, and 0.47, 0.58, 0.09 and 0.02 mg g-1 in NSB, and 1.30, 1.09, 1.06 and 1.62 mg g-1 in MSB, respectively. We used the isothermal models of Langmuir and Freundlich, however for multielement solutions the adsorption did not conform to the Freundlich isotherm. In the kinetic studies with modified biomasses, sorption was achieved in the first 5 minutes and reached equilibrium in 30 min. The O-H, C-O-C, C-C, C-H, and C=O groups were found in the characterization of the biomass sorption sites by Fourier transform infrared spectrometry (FTIR). In the determination of the biomass surface charges using blue methylene and red amaranth dyes, there was a predominance of negative charges. Modified biomasses were used in the adsorption of Cu(II), Fe(II), Zn(II), and Mn(II) in lake water, in which retention of 24.31, 14.50, 8.21, and 8.03 mg g-1 by MLR, and 13.15, 10.50, 5.14 and 6,10 mg g-1 by MSB was found, respectively. |
publishDate |
2017 |
dc.date.issued.fl_str_mv |
2017-06-05 |
dc.date.accessioned.fl_str_mv |
2018-01-11T18:10:11Z |
dc.date.available.fl_str_mv |
2018-01-11T18:10:11Z |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/masterThesis |
format |
masterThesis |
status_str |
publishedVersion |
dc.identifier.citation.fl_str_mv |
MILANI, Priscila Aparecida. Bagaço de cana-de-açúcar e raízes de alface empregados como biossorventes de íons metálicos em meio aquoso. 2017. Dissertação (Mestrado em Agricultura e Ambiente) – Universidade Federal de São Carlos, Araras, 2017. Disponível em: https://repositorio.ufscar.br/handle/ufscar/9248. |
dc.identifier.uri.fl_str_mv |
https://repositorio.ufscar.br/handle/ufscar/9248 |
identifier_str_mv |
MILANI, Priscila Aparecida. Bagaço de cana-de-açúcar e raízes de alface empregados como biossorventes de íons metálicos em meio aquoso. 2017. Dissertação (Mestrado em Agricultura e Ambiente) – Universidade Federal de São Carlos, Araras, 2017. Disponível em: https://repositorio.ufscar.br/handle/ufscar/9248. |
url |
https://repositorio.ufscar.br/handle/ufscar/9248 |
dc.language.iso.fl_str_mv |
por |
language |
por |
dc.relation.confidence.fl_str_mv |
600 600 |
dc.relation.authority.fl_str_mv |
cd6aac36-4ab0-428d-be5c-61bc7099b00b |
dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess |
eu_rights_str_mv |
openAccess |
dc.publisher.none.fl_str_mv |
Universidade Federal de São Carlos Câmpus Araras |
dc.publisher.program.fl_str_mv |
Programa de Pós-Graduação em Agricultura e Ambiente - PPGAA-Ar |
dc.publisher.initials.fl_str_mv |
UFSCar |
publisher.none.fl_str_mv |
Universidade Federal de São Carlos Câmpus Araras |
dc.source.none.fl_str_mv |
reponame:Repositório Institucional da UFSCAR instname:Universidade Federal de São Carlos (UFSCAR) instacron:UFSCAR |
instname_str |
Universidade Federal de São Carlos (UFSCAR) |
instacron_str |
UFSCAR |
institution |
UFSCAR |
reponame_str |
Repositório Institucional da UFSCAR |
collection |
Repositório Institucional da UFSCAR |
bitstream.url.fl_str_mv |
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bitstream.checksum.fl_str_mv |
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bitstream.checksumAlgorithm.fl_str_mv |
MD5 MD5 MD5 MD5 MD5 MD5 MD5 MD5 |
repository.name.fl_str_mv |
Repositório Institucional da UFSCAR - Universidade Federal de São Carlos (UFSCAR) |
repository.mail.fl_str_mv |
|
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1802136331260788736 |