Microestrutura e propriedades mecânicas da liga AA6061 processada por deformação plástica severa em temperatura criogênica

Detalhes bibliográficos
Autor(a) principal: Magalhães, Danielle Cristina Camilo
Data de Publicação: 2017
Tipo de documento: Tese
Idioma: por
Título da fonte: Repositório Institucional da UFSCAR
Texto Completo: https://repositorio.ufscar.br/handle/ufscar/9446
Resumo: The present work aimed two fronts: to characterize the mechanical behavior of the AA6061 alloy at cryogenic temperature, and to study the microstructural and properties evolution after cryogenic severe plastic deformation. Samples of AA6061 alloy were solution heat-treated and processed by conventional rolling, asymmetric rolling and equal-channel angular pressing (ECAP), both at room temperature and cryogenic temperature. After processing, such samples were treated for precipitation at 25 °C and at 100 °C, for different times. On the cryogenic mechanical behavior it was observed the suppression of the dynamic strain aging, which also allowed the ECAP processing without cracking. Uniform and total elongation and mechanical strength were always higher at -196 °C than at room temperature. The strain-rate sensitivity, despite having low values, becomes positive for cryogenic deformation, directly affecting the deformation capacity. Regardless of the processing route employed, a saturation of the hardness around 125 HV has been seen. The microstructures after cryogenic ECAP were very refined in relation to the starting material (average grain size up to 500 nm). In addition, it was observed a homogeneous strains distribution after cryogenic processing, with detection of several new fine grains from grain boundaries, which suggests recrystallization. The tensile tests results, after cryogenic processing in combination with artificial aging at 100 °C (48 hours), indicated an increase in uniform elongation. Regarding mechanical strength, the highest values were observed for extrusion at room temperature combined with artificial aging. In addition, there was to some static recovery during artificial aging, especially for cryogenic processing, which generates thermodynamically unstable microstructures. The density of dislocations, in fact, decreases with the prolongation of artificial aging time. Thus, the present study was based on a study of the cryogenic mechanical behavior of the AA6061 alloy, as well as the possibility of processing by cryogenic severe deformation.
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spelling Magalhães, Danielle Cristina CamiloSordi, Vitor Luizhttp://lattes.cnpq.br/8364164402481940Kliauga, Andrea Madeirahttp://lattes.cnpq.br/3527528295399928http://lattes.cnpq.br/5486724956564584ae3f7e8f-0c98-440a-8034-a11e8ec3336b2018-02-20T12:12:38Z2018-02-20T12:12:38Z2017-08-08MAGALHÃES, Danielle Cristina Camilo. Microestrutura e propriedades mecânicas da liga AA6061 processada por deformação plástica severa em temperatura criogênica. 2017. Tese (Doutorado em Ciência e Engenharia de Materiais) – Universidade Federal de São Carlos, São Carlos, 2017. Disponível em: https://repositorio.ufscar.br/handle/ufscar/9446.https://repositorio.ufscar.br/handle/ufscar/9446The present work aimed two fronts: to characterize the mechanical behavior of the AA6061 alloy at cryogenic temperature, and to study the microstructural and properties evolution after cryogenic severe plastic deformation. Samples of AA6061 alloy were solution heat-treated and processed by conventional rolling, asymmetric rolling and equal-channel angular pressing (ECAP), both at room temperature and cryogenic temperature. After processing, such samples were treated for precipitation at 25 °C and at 100 °C, for different times. On the cryogenic mechanical behavior it was observed the suppression of the dynamic strain aging, which also allowed the ECAP processing without cracking. Uniform and total elongation and mechanical strength were always higher at -196 °C than at room temperature. The strain-rate sensitivity, despite having low values, becomes positive for cryogenic deformation, directly affecting the deformation capacity. Regardless of the processing route employed, a saturation of the hardness around 125 HV has been seen. The microstructures after cryogenic ECAP were very refined in relation to the starting material (average grain size up to 500 nm). In addition, it was observed a homogeneous strains distribution after cryogenic processing, with detection of several new fine grains from grain boundaries, which suggests recrystallization. The tensile tests results, after cryogenic processing in combination with artificial aging at 100 °C (48 hours), indicated an increase in uniform elongation. Regarding mechanical strength, the highest values were observed for extrusion at room temperature combined with artificial aging. In addition, there was to some static recovery during artificial aging, especially for cryogenic processing, which generates thermodynamically unstable microstructures. The density of dislocations, in fact, decreases with the prolongation of artificial aging time. Thus, the present study was based on a study of the cryogenic mechanical behavior of the AA6061 alloy, as well as the possibility of processing by cryogenic severe deformation.A ênfase do presente trabalho deu-se em duas frentes: caracterizar o comportamento mecânico da liga AA6061 em temperatura criogênica, e estudar a evolução microestrutural e de propriedades após deformação plástica severa criogênica. Amostras da liga AA6061 foram solubilizadas e submetidas a processos de laminação convencional, laminação assimétrica e extrusão em canal angular, tanto em temperatura ambiente quanto criogênica. Após os processamentos, tais amostras foram termicamente tratadas para precipitação a 25 ºC e a 100 ºC, por diferentes tempos. Quanto ao comportamento mecânico criogênico, observou-se a supressão da precipitação dinâmica, a qual permitiu também a deformação por extrusão sem trincamento. A resistência mecânica e alongamentos uniforme e total são sempre maiores a -196 ºC do que em temperatura ambiente. A sensibilidade à taxa de deformação, apesar de possuir valores baixos, torna-se positiva para deformação criogênica, impactando diretamente na capacidade de deformação. Independentemente do processamento empregado, observou-se uma saturação das durezas em torno de 125 HV. As microestruturas após extrusão em canal angular criogênica apresentam-se bastante refinadas em relação ao material original, com tamanho médio de grão igual a 500 nm. Adicionalmente, observou-se uma distribuição de deformações mais homogênea no processamento criogênico, verificando-se a presença de grão muito finos, sugerindo recristalização. Os resultados de tração pós-processamento criogênico indicaram um aumento do alongamento uniforme na combinação com o envelhecimento artificial a 100 ºC (48 horas). Quanto à resistência mecânica, os maiores valores foram observados para a extrusão em temperatura ambiente combinada com envelhecimento artificial. Além disso, houve recuperação estática durante o envelhecimento artificial, principalmente para as deformações criogênicas, as quais geram microestruturas termodinamicamente mais instáveis. A densidade de discordâncias, de fato, diminui com o prolongamento do tempo de envelhecimento artificial. Dessa forma, o presente trabalho constituiu-se de um estudo dirigido do comportamento mecânico criogênico da liga AA6061, bem como da possibilidade de processamento por deformação severa criogênica.Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)CNPq: 153181/2013-3FAPESP: 2014/15091-7porUniversidade Federal de São CarlosCâmpus São CarlosPrograma de Pós-Graduação em Ciência e Engenharia de Materiais - PPGCEMUFSCarAlumínio AA6061Deformação plástica severa criogênicaComportamento mecânico criogênicoExtrusão em canal angularPrecipitaçãoAluminum AA6061Cryogenic severe plastic deformationCryogenic mechanical behaviorEqual-channel angular pressingAgingENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICAMicroestrutura e propriedades mecânicas da liga AA6061 processada por deformação plástica severa em temperatura criogênicainfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/doctoralThesisOnline6006003ecbc8ef-0ebd-4b04-9d94-9ea2a68cf81finfo:eu-repo/semantics/openAccessreponame:Repositório Institucional da UFSCARinstname:Universidade Federal de São Carlos (UFSCAR)instacron:UFSCARORIGINALTeseDCCM.pdfTeseDCCM.pdfapplication/pdf8210400https://repositorio.ufscar.br/bitstream/ufscar/9446/1/TeseDCCM.pdfaa7c4ffb6808f655dbda64d16775bd21MD51LICENSElicense.txtlicense.txttext/plain; charset=utf-81957https://repositorio.ufscar.br/bitstream/ufscar/9446/2/license.txtae0398b6f8b235e40ad82cba6c50031dMD52TEXTTeseDCCM.pdf.txtTeseDCCM.pdf.txtExtracted texttext/plain274156https://repositorio.ufscar.br/bitstream/ufscar/9446/3/TeseDCCM.pdf.txt3795729a6be7dc97cd7aca0a38ea218dMD53THUMBNAILTeseDCCM.pdf.jpgTeseDCCM.pdf.jpgIM Thumbnailimage/jpeg6884https://repositorio.ufscar.br/bitstream/ufscar/9446/4/TeseDCCM.pdf.jpga03bc0d454a5034f7e36bc67d4163127MD54ufscar/94462023-09-18 18:31:12.899oai:repositorio.ufscar.br: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Repositório InstitucionalPUBhttps://repositorio.ufscar.br/oai/requestopendoar:43222023-09-18T18:31:12Repositório Institucional da UFSCAR - Universidade Federal de São Carlos (UFSCAR)false
dc.title.por.fl_str_mv Microestrutura e propriedades mecânicas da liga AA6061 processada por deformação plástica severa em temperatura criogênica
title Microestrutura e propriedades mecânicas da liga AA6061 processada por deformação plástica severa em temperatura criogênica
spellingShingle Microestrutura e propriedades mecânicas da liga AA6061 processada por deformação plástica severa em temperatura criogênica
Magalhães, Danielle Cristina Camilo
Alumínio AA6061
Deformação plástica severa criogênica
Comportamento mecânico criogênico
Extrusão em canal angular
Precipitação
Aluminum AA6061
Cryogenic severe plastic deformation
Cryogenic mechanical behavior
Equal-channel angular pressing
Aging
ENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA
title_short Microestrutura e propriedades mecânicas da liga AA6061 processada por deformação plástica severa em temperatura criogênica
title_full Microestrutura e propriedades mecânicas da liga AA6061 processada por deformação plástica severa em temperatura criogênica
title_fullStr Microestrutura e propriedades mecânicas da liga AA6061 processada por deformação plástica severa em temperatura criogênica
title_full_unstemmed Microestrutura e propriedades mecânicas da liga AA6061 processada por deformação plástica severa em temperatura criogênica
title_sort Microestrutura e propriedades mecânicas da liga AA6061 processada por deformação plástica severa em temperatura criogênica
author Magalhães, Danielle Cristina Camilo
author_facet Magalhães, Danielle Cristina Camilo
author_role author
dc.contributor.authorlattes.por.fl_str_mv http://lattes.cnpq.br/5486724956564584
dc.contributor.author.fl_str_mv Magalhães, Danielle Cristina Camilo
dc.contributor.advisor1.fl_str_mv Sordi, Vitor Luiz
dc.contributor.advisor1Lattes.fl_str_mv http://lattes.cnpq.br/8364164402481940
dc.contributor.advisor-co1.fl_str_mv Kliauga, Andrea Madeira
dc.contributor.advisor-co1Lattes.fl_str_mv http://lattes.cnpq.br/3527528295399928
dc.contributor.authorID.fl_str_mv ae3f7e8f-0c98-440a-8034-a11e8ec3336b
contributor_str_mv Sordi, Vitor Luiz
Kliauga, Andrea Madeira
dc.subject.por.fl_str_mv Alumínio AA6061
Deformação plástica severa criogênica
Comportamento mecânico criogênico
Extrusão em canal angular
Precipitação
topic Alumínio AA6061
Deformação plástica severa criogênica
Comportamento mecânico criogênico
Extrusão em canal angular
Precipitação
Aluminum AA6061
Cryogenic severe plastic deformation
Cryogenic mechanical behavior
Equal-channel angular pressing
Aging
ENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA
dc.subject.eng.fl_str_mv Aluminum AA6061
Cryogenic severe plastic deformation
Cryogenic mechanical behavior
Equal-channel angular pressing
Aging
dc.subject.cnpq.fl_str_mv ENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA
description The present work aimed two fronts: to characterize the mechanical behavior of the AA6061 alloy at cryogenic temperature, and to study the microstructural and properties evolution after cryogenic severe plastic deformation. Samples of AA6061 alloy were solution heat-treated and processed by conventional rolling, asymmetric rolling and equal-channel angular pressing (ECAP), both at room temperature and cryogenic temperature. After processing, such samples were treated for precipitation at 25 °C and at 100 °C, for different times. On the cryogenic mechanical behavior it was observed the suppression of the dynamic strain aging, which also allowed the ECAP processing without cracking. Uniform and total elongation and mechanical strength were always higher at -196 °C than at room temperature. The strain-rate sensitivity, despite having low values, becomes positive for cryogenic deformation, directly affecting the deformation capacity. Regardless of the processing route employed, a saturation of the hardness around 125 HV has been seen. The microstructures after cryogenic ECAP were very refined in relation to the starting material (average grain size up to 500 nm). In addition, it was observed a homogeneous strains distribution after cryogenic processing, with detection of several new fine grains from grain boundaries, which suggests recrystallization. The tensile tests results, after cryogenic processing in combination with artificial aging at 100 °C (48 hours), indicated an increase in uniform elongation. Regarding mechanical strength, the highest values were observed for extrusion at room temperature combined with artificial aging. In addition, there was to some static recovery during artificial aging, especially for cryogenic processing, which generates thermodynamically unstable microstructures. The density of dislocations, in fact, decreases with the prolongation of artificial aging time. Thus, the present study was based on a study of the cryogenic mechanical behavior of the AA6061 alloy, as well as the possibility of processing by cryogenic severe deformation.
publishDate 2017
dc.date.issued.fl_str_mv 2017-08-08
dc.date.accessioned.fl_str_mv 2018-02-20T12:12:38Z
dc.date.available.fl_str_mv 2018-02-20T12:12:38Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/doctoralThesis
format doctoralThesis
status_str publishedVersion
dc.identifier.citation.fl_str_mv MAGALHÃES, Danielle Cristina Camilo. Microestrutura e propriedades mecânicas da liga AA6061 processada por deformação plástica severa em temperatura criogênica. 2017. Tese (Doutorado em Ciência e Engenharia de Materiais) – Universidade Federal de São Carlos, São Carlos, 2017. Disponível em: https://repositorio.ufscar.br/handle/ufscar/9446.
dc.identifier.uri.fl_str_mv https://repositorio.ufscar.br/handle/ufscar/9446
identifier_str_mv MAGALHÃES, Danielle Cristina Camilo. Microestrutura e propriedades mecânicas da liga AA6061 processada por deformação plástica severa em temperatura criogênica. 2017. Tese (Doutorado em Ciência e Engenharia de Materiais) – Universidade Federal de São Carlos, São Carlos, 2017. Disponível em: https://repositorio.ufscar.br/handle/ufscar/9446.
url https://repositorio.ufscar.br/handle/ufscar/9446
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dc.publisher.none.fl_str_mv Universidade Federal de São Carlos
Câmpus São Carlos
dc.publisher.program.fl_str_mv Programa de Pós-Graduação em Ciência e Engenharia de Materiais - PPGCEM
dc.publisher.initials.fl_str_mv UFSCar
publisher.none.fl_str_mv Universidade Federal de São Carlos
Câmpus São Carlos
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