Análise do desempenho de máscaras na retenção de nanopartículas de acordo com as normas técnicas

Detalhes bibliográficos
Autor(a) principal: Pereira, Tayanna Cristina Passos
Data de Publicação: 2022
Tipo de documento: Dissertação
Idioma: por
Título da fonte: Repositório Institucional da UFSCAR
Texto Completo: https://repositorio.ufscar.br/handle/ufscar/16433
Resumo: In early 2020, the SARS-CoV-2 virus caused a disease known as COVID-19 that caused a worldwide pandemic. As a result, there was an increase in the demand for PPE (masks, aprons, gown, etc.) in the hospital environment. With the growing alarming numbers of infected around the world, WHO recommended that the population also wear masks for their protection, increasing the consumption of this PPE, leading to a shortage of masks in the world market. Within this context, the understanding of the difference between the types of masks and the standards that exist on the characterization of these is very important. Thus, the present work objectives to study the current standards (American, European and Brazilian) and propose improvements in the characterizations of filtering materials. Therefore, this work consists of seeking innovation in the development of protocols to characterize masks. Eight masks were tested, six surgical masks and two respirators, to assess the best way to characterize them. The tests were: determination of permeability, fiber diameter through SEM images, particle filtration efficiency and pressure drop (breathability). These last two tests are carried out using the current standards as a basis. Some changes were made to evaluate the interference in the tests. The combination of filtration efficiency and breathability is very important for the quality of the mask. The permeability tests were consistent with the pressure drop tests, since the mask that obtained the highest permeability was the one with the lowest pressure drop. The results obtained by all surgical masks did not accomplish desired results by the standards, in any test condition. Only the respirators presented results close to what is stipulated by the standard (95%) at the lowest surface speed tested (6,51 cm/s). The standards do not use the correct conditions for the tests, since tests should be performed at speeds that simulate human respiratory activity. An example of this is the fact that the current Brazilian Standard and the American Standard allow a wide range in face velocity (0,5 to 25 cm/s) that do not represent any human activity, since the speed of a sneeze can vary between 20 and 50 m/s, that is, at least 100 times higher than the maximum limit proposed by the standard. The breathing of a person at rest is around 6 L/min. Thus, an ideal flow rate for performing the tests would be flows close to this value. In this work, tests were performed, following the standards, using the flow rate of 7 L/min and the masks did not present good performance, with the best result being close to 56% efficiency in the collection of particles of 100 nm. This low performance can be related to the size of the particles that the tests were carried out, because surgical masks are recommended for use against droplet-transmitted pathogens and respirators (PFF) are indicated for diseases transmitted by aerosols. And since the test was performed for 100 nm particles (aerosols) the surgical masks performed poorly. In general, this work made it possible to evaluate parameters that directly interfere with the results of the tests that are proposed by the technical standards for surgical masks. Concluding that the tests must be reviewed and define better parameters (concentration of aerosol particles, particle size, test flow rate, test area or surface velocity) and define the equipment that must be used according to the counting and classification efficiency of the particles.
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spelling Pereira, Tayanna Cristina PassosAguiar, Mônica Lopeshttp://lattes.cnpq.br/0431688649128529Lima, Bruno de Araújohttp://lattes.cnpq.br/8754392911364716http://lattes.cnpq.br/41944662192842156e111634-4174-495e-9e6e-61b7152a2afa2022-07-29T13:26:42Z2022-07-29T13:26:42Z2022-05-31PEREIRA, Tayanna Cristina Passos. Análise do desempenho de máscaras na retenção de nanopartículas de acordo com as normas técnicas. 2022. Dissertação (Mestrado em Engenharia Química) – Universidade Federal de São Carlos, São Carlos, 2022. Disponível em: https://repositorio.ufscar.br/handle/ufscar/16433.https://repositorio.ufscar.br/handle/ufscar/16433In early 2020, the SARS-CoV-2 virus caused a disease known as COVID-19 that caused a worldwide pandemic. As a result, there was an increase in the demand for PPE (masks, aprons, gown, etc.) in the hospital environment. With the growing alarming numbers of infected around the world, WHO recommended that the population also wear masks for their protection, increasing the consumption of this PPE, leading to a shortage of masks in the world market. Within this context, the understanding of the difference between the types of masks and the standards that exist on the characterization of these is very important. Thus, the present work objectives to study the current standards (American, European and Brazilian) and propose improvements in the characterizations of filtering materials. Therefore, this work consists of seeking innovation in the development of protocols to characterize masks. Eight masks were tested, six surgical masks and two respirators, to assess the best way to characterize them. The tests were: determination of permeability, fiber diameter through SEM images, particle filtration efficiency and pressure drop (breathability). These last two tests are carried out using the current standards as a basis. Some changes were made to evaluate the interference in the tests. The combination of filtration efficiency and breathability is very important for the quality of the mask. The permeability tests were consistent with the pressure drop tests, since the mask that obtained the highest permeability was the one with the lowest pressure drop. The results obtained by all surgical masks did not accomplish desired results by the standards, in any test condition. Only the respirators presented results close to what is stipulated by the standard (95%) at the lowest surface speed tested (6,51 cm/s). The standards do not use the correct conditions for the tests, since tests should be performed at speeds that simulate human respiratory activity. An example of this is the fact that the current Brazilian Standard and the American Standard allow a wide range in face velocity (0,5 to 25 cm/s) that do not represent any human activity, since the speed of a sneeze can vary between 20 and 50 m/s, that is, at least 100 times higher than the maximum limit proposed by the standard. The breathing of a person at rest is around 6 L/min. Thus, an ideal flow rate for performing the tests would be flows close to this value. In this work, tests were performed, following the standards, using the flow rate of 7 L/min and the masks did not present good performance, with the best result being close to 56% efficiency in the collection of particles of 100 nm. This low performance can be related to the size of the particles that the tests were carried out, because surgical masks are recommended for use against droplet-transmitted pathogens and respirators (PFF) are indicated for diseases transmitted by aerosols. And since the test was performed for 100 nm particles (aerosols) the surgical masks performed poorly. In general, this work made it possible to evaluate parameters that directly interfere with the results of the tests that are proposed by the technical standards for surgical masks. Concluding that the tests must be reviewed and define better parameters (concentration of aerosol particles, particle size, test flow rate, test area or surface velocity) and define the equipment that must be used according to the counting and classification efficiency of the particles.No início do ano de 2020, o vírus SARS-CoV-2 causou uma doença denominada COVID-19 que provocou uma pandemia mundial. Em decorrência, houve o aumento da demanda de EPI’s (máscaras, aventais, toucas, etc) no meio hospitalar. Com os números cada vez mais alarmantes de infectados pelo mundo, a OMS recomendou que a população também usasse máscaras para a sua proteção, aumentando o consumo deste EPI, levando a escassez de máscaras no mercado mundial. Dentro deste contexto, o entendimento sobre a diferença entre os tipos de máscaras e as normas que vigoram sobre a caracterização destas é muito importante. Dessa forma, o presente trabalho visa estudar as normas vigentes (americanas, europeias e brasileiras) e propor melhorias nas caracterizações de materiais filtrantes. Sendo assim, este trabalho consiste em buscar inovação no desenvolvimento de protocolos para caracterizar as máscaras. Oito máscaras foram testadas, sendo seis máscaras cirúrgicas e dois respiradores, para avaliar a melhor forma de caracterizá-las. Os testes realizados foram: determinação de permeabilidade, diâmetro de fibras através de Imagens de MEV, eficiência de filtração de partículas e queda de pressão (respirabilidade). Sendo estes dois últimos testes realizados utilizando as normas vigentes como base. Algumas alterações foram realizadas para avaliar a interferência nos testes. A combinação da eficiência de filtração e a respirabilidade é muito importante para a qualidade da máscara. Os testes de permeabilidade foram condizentes com os testes de queda de pressão, visto que a máscara que obteve maior permeabilidade, foi a que apresentou menor queda de pressão. Os resultados obtidos por todas as máscaras cirúrgicas não atingiram resultados desejados pelas normas, em nenhuma condição de teste. Apenas os respiradores apresentaram resultados próximos ao que é estipulado pela norma (95%) na velocidade superficial mais baixa testada (6,51 cm/s). As normas não utilizam condições corretas para a realização dos testes, uma vez que deveria ser realizado testes em velocidades que simulam atividade respiratória humana. Um exemplo disso é o fato da norma brasileira atual e a norma americana permitir uma ampla faixa na velocidade de face (0,5 a 25 cm/s) que não representam nenhuma atividade humana, visto que a velocidade de um espirro pode variar entre 20 e 50 m/s, ou seja pelo menos 100 vezes maior que o limite máximo proposto pela norma. A respiração de uma pessoa em repouso é em torno de 6 L/min. Dessa forma, uma vazão ideal para a realização dos testes seriam vazões próximas a esse valor. Neste trabalho foram realizados testes, seguindo as normas, utilizando a vazão de 7 L/min e as máscaras não apresentaram bom desempenho, sendo o melhor resultado próximo a 56% de eficiência na coleta de partículas de 100 nm. Este baixo desempenho pode estar relacionado ao tamanho das partículas que os testes foram realizados, porque as máscaras cirúrgicas são indicadas para são recomendadas para serem utilizadas contra patógenos transmitidos por gotículas e os respiradores (PFF) são indicadas para doenças transmitidas por aerossóis. E como o teste foi realizado para partículas de 100 nm (aerossóis) as máscaras cirúrgicas apresentaram um desempenho inferior. De forma geral, este trabalho possibilitou avaliar parâmetros que interferem diretamente nos resultados dos testes que são propostos pelas normas técnicas para máscara cirúrgica. Concluindo que os testes devem ser revistos e definir melhores parâmetros (concentração de partículas de aerossóis, tamanho das partículas, vazão do teste, área de teste ou a velocidade superficial) e definir o equipamento que deve ser utilizado de acordo com a eficiência de contagem e de classificação das partículas.Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)88887.508315/2020-00porUniversidade Federal de São CarlosCâmpus São CarlosPrograma de Pós-Graduação em Engenharia Química - PPGEQUFSCarAttribution-NonCommercial-NoDerivs 3.0 Brazilhttp://creativecommons.org/licenses/by-nc-nd/3.0/br/info:eu-repo/semantics/openAccessMáscarasNormas TécnicasEficiência de filtraçãoRespirabilidadeMasksStandardsFiltration EfficiencyBreathabilityENGENHARIAS::ENGENHARIA QUIMICAAnálise do desempenho de máscaras na retenção de nanopartículas de acordo com as normas técnicasAnalysis of the performance of masks in the retention of nanoparticles according to standardsinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/masterThesis600cfe199c5-37b6-4d5a-a38c-e0503b6b1995reponame:Repositório Institucional da UFSCARinstname:Universidade Federal de São Carlos (UFSCAR)instacron:UFSCARORIGINALDissertação de Mestrado - Tayanna Pereira.pdfDissertação de Mestrado - Tayanna Pereira.pdfDissertação de Mestrado - Tayanna Pereiraapplication/pdf2511817https://repositorio.ufscar.br/bitstream/ufscar/16433/4/Disserta%c3%a7%c3%a3o%20de%20Mestrado%20-%20Tayanna%20Pereira.pdffb19ea1102337eba3ca22a194b84ca36MD54Carta_comprovante_-_Tayanna_Pereira_assinado.pdfCarta_comprovante_-_Tayanna_Pereira_assinado.pdfCarta comprovanteapplication/pdf109099https://repositorio.ufscar.br/bitstream/ufscar/16433/2/Carta_comprovante_-_Tayanna_Pereira_assinado.pdf5bb157a205f1ec885eb51c0bd89cc6eaMD52CC-LICENSElicense_rdflicense_rdfapplication/rdf+xml; charset=utf-8811https://repositorio.ufscar.br/bitstream/ufscar/16433/5/license_rdfe39d27027a6cc9cb039ad269a5db8e34MD55TEXTDissertação de Mestrado - Tayanna Pereira.pdf.txtDissertação de Mestrado - Tayanna Pereira.pdf.txtExtracted texttext/plain239941https://repositorio.ufscar.br/bitstream/ufscar/16433/6/Disserta%c3%a7%c3%a3o%20de%20Mestrado%20-%20Tayanna%20Pereira.pdf.txt4171de06d205c7ff8c941411c6821167MD56Carta_comprovante_-_Tayanna_Pereira_assinado.pdf.txtCarta_comprovante_-_Tayanna_Pereira_assinado.pdf.txtExtracted texttext/plain1274https://repositorio.ufscar.br/bitstream/ufscar/16433/8/Carta_comprovante_-_Tayanna_Pereira_assinado.pdf.txtaa3f59a101b741300cd03668fb5280b1MD58THUMBNAILDissertação de Mestrado - Tayanna Pereira.pdf.jpgDissertação de Mestrado - Tayanna Pereira.pdf.jpgIM Thumbnailimage/jpeg7220https://repositorio.ufscar.br/bitstream/ufscar/16433/7/Disserta%c3%a7%c3%a3o%20de%20Mestrado%20-%20Tayanna%20Pereira.pdf.jpgeda005dcc97a3a8f74021f46a26a40ebMD57Carta_comprovante_-_Tayanna_Pereira_assinado.pdf.jpgCarta_comprovante_-_Tayanna_Pereira_assinado.pdf.jpgIM Thumbnailimage/jpeg13816https://repositorio.ufscar.br/bitstream/ufscar/16433/9/Carta_comprovante_-_Tayanna_Pereira_assinado.pdf.jpg4f510b0c47c1c9c8090639333b38a5feMD59ufscar/164332023-09-18 18:32:26.592oai:repositorio.ufscar.br:ufscar/16433Repositório InstitucionalPUBhttps://repositorio.ufscar.br/oai/requestopendoar:43222023-09-18T18:32:26Repositório Institucional da UFSCAR - Universidade Federal de São Carlos (UFSCAR)false
dc.title.por.fl_str_mv Análise do desempenho de máscaras na retenção de nanopartículas de acordo com as normas técnicas
dc.title.alternative.eng.fl_str_mv Analysis of the performance of masks in the retention of nanoparticles according to standards
title Análise do desempenho de máscaras na retenção de nanopartículas de acordo com as normas técnicas
spellingShingle Análise do desempenho de máscaras na retenção de nanopartículas de acordo com as normas técnicas
Pereira, Tayanna Cristina Passos
Máscaras
Normas Técnicas
Eficiência de filtração
Respirabilidade
Masks
Standards
Filtration Efficiency
Breathability
ENGENHARIAS::ENGENHARIA QUIMICA
title_short Análise do desempenho de máscaras na retenção de nanopartículas de acordo com as normas técnicas
title_full Análise do desempenho de máscaras na retenção de nanopartículas de acordo com as normas técnicas
title_fullStr Análise do desempenho de máscaras na retenção de nanopartículas de acordo com as normas técnicas
title_full_unstemmed Análise do desempenho de máscaras na retenção de nanopartículas de acordo com as normas técnicas
title_sort Análise do desempenho de máscaras na retenção de nanopartículas de acordo com as normas técnicas
author Pereira, Tayanna Cristina Passos
author_facet Pereira, Tayanna Cristina Passos
author_role author
dc.contributor.authorlattes.por.fl_str_mv http://lattes.cnpq.br/4194466219284215
dc.contributor.author.fl_str_mv Pereira, Tayanna Cristina Passos
dc.contributor.advisor1.fl_str_mv Aguiar, Mônica Lopes
dc.contributor.advisor1Lattes.fl_str_mv http://lattes.cnpq.br/0431688649128529
dc.contributor.advisor-co1.fl_str_mv Lima, Bruno de Araújo
dc.contributor.advisor-co1Lattes.fl_str_mv http://lattes.cnpq.br/8754392911364716
dc.contributor.authorID.fl_str_mv 6e111634-4174-495e-9e6e-61b7152a2afa
contributor_str_mv Aguiar, Mônica Lopes
Lima, Bruno de Araújo
dc.subject.por.fl_str_mv Máscaras
Normas Técnicas
Eficiência de filtração
Respirabilidade
topic Máscaras
Normas Técnicas
Eficiência de filtração
Respirabilidade
Masks
Standards
Filtration Efficiency
Breathability
ENGENHARIAS::ENGENHARIA QUIMICA
dc.subject.eng.fl_str_mv Masks
Standards
Filtration Efficiency
Breathability
dc.subject.cnpq.fl_str_mv ENGENHARIAS::ENGENHARIA QUIMICA
description In early 2020, the SARS-CoV-2 virus caused a disease known as COVID-19 that caused a worldwide pandemic. As a result, there was an increase in the demand for PPE (masks, aprons, gown, etc.) in the hospital environment. With the growing alarming numbers of infected around the world, WHO recommended that the population also wear masks for their protection, increasing the consumption of this PPE, leading to a shortage of masks in the world market. Within this context, the understanding of the difference between the types of masks and the standards that exist on the characterization of these is very important. Thus, the present work objectives to study the current standards (American, European and Brazilian) and propose improvements in the characterizations of filtering materials. Therefore, this work consists of seeking innovation in the development of protocols to characterize masks. Eight masks were tested, six surgical masks and two respirators, to assess the best way to characterize them. The tests were: determination of permeability, fiber diameter through SEM images, particle filtration efficiency and pressure drop (breathability). These last two tests are carried out using the current standards as a basis. Some changes were made to evaluate the interference in the tests. The combination of filtration efficiency and breathability is very important for the quality of the mask. The permeability tests were consistent with the pressure drop tests, since the mask that obtained the highest permeability was the one with the lowest pressure drop. The results obtained by all surgical masks did not accomplish desired results by the standards, in any test condition. Only the respirators presented results close to what is stipulated by the standard (95%) at the lowest surface speed tested (6,51 cm/s). The standards do not use the correct conditions for the tests, since tests should be performed at speeds that simulate human respiratory activity. An example of this is the fact that the current Brazilian Standard and the American Standard allow a wide range in face velocity (0,5 to 25 cm/s) that do not represent any human activity, since the speed of a sneeze can vary between 20 and 50 m/s, that is, at least 100 times higher than the maximum limit proposed by the standard. The breathing of a person at rest is around 6 L/min. Thus, an ideal flow rate for performing the tests would be flows close to this value. In this work, tests were performed, following the standards, using the flow rate of 7 L/min and the masks did not present good performance, with the best result being close to 56% efficiency in the collection of particles of 100 nm. This low performance can be related to the size of the particles that the tests were carried out, because surgical masks are recommended for use against droplet-transmitted pathogens and respirators (PFF) are indicated for diseases transmitted by aerosols. And since the test was performed for 100 nm particles (aerosols) the surgical masks performed poorly. In general, this work made it possible to evaluate parameters that directly interfere with the results of the tests that are proposed by the technical standards for surgical masks. Concluding that the tests must be reviewed and define better parameters (concentration of aerosol particles, particle size, test flow rate, test area or surface velocity) and define the equipment that must be used according to the counting and classification efficiency of the particles.
publishDate 2022
dc.date.accessioned.fl_str_mv 2022-07-29T13:26:42Z
dc.date.available.fl_str_mv 2022-07-29T13:26:42Z
dc.date.issued.fl_str_mv 2022-05-31
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dc.identifier.citation.fl_str_mv PEREIRA, Tayanna Cristina Passos. Análise do desempenho de máscaras na retenção de nanopartículas de acordo com as normas técnicas. 2022. Dissertação (Mestrado em Engenharia Química) – Universidade Federal de São Carlos, São Carlos, 2022. Disponível em: https://repositorio.ufscar.br/handle/ufscar/16433.
dc.identifier.uri.fl_str_mv https://repositorio.ufscar.br/handle/ufscar/16433
identifier_str_mv PEREIRA, Tayanna Cristina Passos. Análise do desempenho de máscaras na retenção de nanopartículas de acordo com as normas técnicas. 2022. Dissertação (Mestrado em Engenharia Química) – Universidade Federal de São Carlos, São Carlos, 2022. Disponível em: https://repositorio.ufscar.br/handle/ufscar/16433.
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