Biomimetism of Brazil nutshell (Bertholletia excelsa)

Detalhes bibliográficos
Autor(a) principal: Sônego, Marília
Data de Publicação: 2020
Tipo de documento: Tese
Idioma: eng
Título da fonte: Repositório Institucional da UFSCAR
Texto Completo: https://repositorio.ufscar.br/handle/ufscar/13153
Resumo: For thousands of years, nature has accumulated countless possibilities for optimized solutions to engineering problems using limited raw material, room temperature, aqueous solutions, solar energy and renewable resources. Recently, this natural accumulated knowledge has increasingly being studied and applied to solve technical problems in studies of biomimicry and bioinspiration.One from many examples are the fruit walls of nuts and drupes which are of special interest for the development of impact and puncture resistant bioinspired structures. This project aims to identify and apply the principles responsible for the excellent mechanical properties of Brazil’s nutshell (Bertholletia excelsa) to develop polymeric composites with superior toughness and mechanical resistance. Firstly, the hierarchical levels of organization of the nutshell structure were identified through chemical analysis, optical microscopy, scanning electron microscopy (SEM) and microtomography (MicroCT). Additionally, the mechanical properties of the nutshell were evaluated in tensile, compression, hardness, and fracture toughness tests, at different length-scales. Moreover, the analysis of fractured surface was carried out by optical microscopy, SEM and MicroCT, identifying the fracture and toughness mechanisms developed by Brazil’s nutshell. Finally, the principles responsible for Brazil’s nutshell mechanical performance were applied to optimize the mechanical performance of a bioinspired polymeric composite. The developed composite is composed of a 3D printed structure of polylactic acid reinforced with 30% of carbon fiber (PLA-30CF) which was impregnated with syntactic foam (epoxy resin and hollow glass microspheres). The mechanical performance of the bioinspired composite is promising. It has density of 0.96 g/cm3, flexural elastic modulus of 2.52 GPa, and impact strength of 1.8 kJ/m2. However, adjustments and improvements in the syntactic foam are still required.
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spelling Sônego, MaríliaPessan, Luiz Antoniohttp://lattes.cnpq.br/8276650236213537http://lattes.cnpq.br/3460853436777584e3ca4ba0-6da5-4056-8e4a-00588dd963e52020-08-13T21:07:01Z2020-08-13T21:07:01Z2020-08-07SÔNEGO, Marília. Biomimetism of Brazil nutshell (Bertholletia excelsa). 2020. Tese (Doutorado em Ciência e Engenharia de Materiais) – Universidade Federal de São Carlos, São Carlos, 2020. Disponível em: https://repositorio.ufscar.br/handle/ufscar/13153.https://repositorio.ufscar.br/handle/ufscar/13153For thousands of years, nature has accumulated countless possibilities for optimized solutions to engineering problems using limited raw material, room temperature, aqueous solutions, solar energy and renewable resources. Recently, this natural accumulated knowledge has increasingly being studied and applied to solve technical problems in studies of biomimicry and bioinspiration.One from many examples are the fruit walls of nuts and drupes which are of special interest for the development of impact and puncture resistant bioinspired structures. This project aims to identify and apply the principles responsible for the excellent mechanical properties of Brazil’s nutshell (Bertholletia excelsa) to develop polymeric composites with superior toughness and mechanical resistance. Firstly, the hierarchical levels of organization of the nutshell structure were identified through chemical analysis, optical microscopy, scanning electron microscopy (SEM) and microtomography (MicroCT). Additionally, the mechanical properties of the nutshell were evaluated in tensile, compression, hardness, and fracture toughness tests, at different length-scales. Moreover, the analysis of fractured surface was carried out by optical microscopy, SEM and MicroCT, identifying the fracture and toughness mechanisms developed by Brazil’s nutshell. Finally, the principles responsible for Brazil’s nutshell mechanical performance were applied to optimize the mechanical performance of a bioinspired polymeric composite. The developed composite is composed of a 3D printed structure of polylactic acid reinforced with 30% of carbon fiber (PLA-30CF) which was impregnated with syntactic foam (epoxy resin and hollow glass microspheres). The mechanical performance of the bioinspired composite is promising. It has density of 0.96 g/cm3, flexural elastic modulus of 2.52 GPa, and impact strength of 1.8 kJ/m2. However, adjustments and improvements in the syntactic foam are still required.Por milhares de anos, a natureza acumulou inúmeras possibilidades de soluções otimizadas para problemas de engenharia, usando matéria-prima limitada, temperatura ambiente, soluções aquosas, energia solar e recursos renováveis. Recentemente, esse conhecimento natural acumulado tem sido cada vez mais estudado e aplicado para solucionar problemas técnicos em estudos de biomimetismo e bioinspiração. Um dos muitos exemplos são as cascas de nozes e drupas que são interessantes para o desenvolvimento de estruturas bioinspiradas resistentes a impactos e perfurações. Este projeto tem como objetivo identificar e aplicar os princípios responsáveis pelas excelentes propriedades mecânicas do ouriço da castanha do Pará (Bertholletia excelsa) para desenvolver compósitos poliméricos com tenacidade e resistência mecânica superiores. Primeiramente, os níveis hierárquicos de organização da estrutura do ouriço foram identificados através de análises químicas, microscopia óptica, microscopia eletrônica de varredura (MEV) e microtomografia (MicroCT). Além disso, as propriedades mecânicas do ouriço foram avaliadas em ensaios de resistência a tração, à compressão, dureza e tenacidade à fratura em diferentes escalas de comprimento. Além disso, a análise da superfície fraturada foi realizada por microscopia óptica, MEV e MicroCT, para identificar os mecanismos de fratura e tenacidade desenvolvidos pelo ouriço da castanha do Pará. Finalmente, os princípios responsáveis pelo desempenho mecânico do ouriço foram aplicados para otimizar o desempenho mecânico de um composto polimérico bioinspirado. O compósito desenvolvido contém uma estrutura impressa em 3D de poli(ácido lácteo) com 30% de fibra de carbono (PLA-30CF) e foi impregnado com uma espuma de resina epoxy e microesferas de vidro ocas. O desempenho mecânico do compósito bioinspirado é promissor. Ele tem densidade de 0,96 g/cm3, módulo elástico em flexão de 2,52 GPa, e resistência ao impacto de 1,8 kJ/m2. No entanto, ajustes e melhoramentos na espuma de epoxy e microesferas de vidro ainda são necessáriosFundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)FAPESP: 2015/25523-1engUniversidade Federal de São CarlosCâmpus São CarlosPrograma de Pós-Graduação em Ciência e Engenharia de Materiais - PPGCEMUFSCarAttribution-NonCommercial-NoDerivs 3.0 Brazilhttp://creativecommons.org/licenses/by-nc-nd/3.0/br/info:eu-repo/semantics/openAccessBioinspiraçãoOuriço da castanha do ParáMicroestruturaPropriedades mecânicasCompósitoBioinspirationBrazil nutshellMechanical propertiesCompositeENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA::MATERIAIS NAO METALICOSBiomimetism of Brazil nutshell (Bertholletia excelsa)Biomimetismo do ouriço da castanha do Pará (Bertholletia excelsa)info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/doctoralThesis60060027e170ed-63e5-4ae6-96cf-f7ccb26a3076reponame:Repositório Institucional da UFSCARinstname:Universidade Federal de São Carlos (UFSCAR)instacron:UFSCARORIGINALMarília Sônego - Tese .pdfMarília Sônego - Tese .pdfTese de doutoradoapplication/pdf147683721https://repositorio.ufscar.br/bitstream/ufscar/13153/1/Mar%c3%adlia%20S%c3%b4nego%20-%20Tese%20.pdffd5acef2ed5624bdf83827117a0d90e3MD51BCO carta comprovante autoarquivamento .pdfBCO carta comprovante autoarquivamento .pdfCarta comprovante da versão final de teseapplication/pdf310966https://repositorio.ufscar.br/bitstream/ufscar/13153/2/BCO%20carta%20comprovante%20autoarquivamento%20.pdf2d29a3add202abdd9bea854e025aee20MD52CC-LICENSElicense_rdflicense_rdfapplication/rdf+xml; charset=utf-8811https://repositorio.ufscar.br/bitstream/ufscar/13153/3/license_rdfe39d27027a6cc9cb039ad269a5db8e34MD53TEXTMarília Sônego - Tese .pdf.txtMarília Sônego - Tese .pdf.txtExtracted texttext/plain227761https://repositorio.ufscar.br/bitstream/ufscar/13153/4/Mar%c3%adlia%20S%c3%b4nego%20-%20Tese%20.pdf.txt45e8acc421e22b13d96cec295a0ad0fcMD54BCO carta comprovante autoarquivamento .pdf.txtBCO carta comprovante autoarquivamento .pdf.txtExtracted texttext/plain1215https://repositorio.ufscar.br/bitstream/ufscar/13153/6/BCO%20carta%20comprovante%20autoarquivamento%20.pdf.txt735e2cf2b472d8c63f19f019562cbb0cMD56THUMBNAILMarília Sônego - Tese .pdf.jpgMarília Sônego - Tese .pdf.jpgIM Thumbnailimage/jpeg6021https://repositorio.ufscar.br/bitstream/ufscar/13153/5/Mar%c3%adlia%20S%c3%b4nego%20-%20Tese%20.pdf.jpg1d672597bc0bf9719da687570003b4fbMD55BCO carta comprovante autoarquivamento .pdf.jpgBCO carta comprovante autoarquivamento .pdf.jpgIM Thumbnailimage/jpeg10152https://repositorio.ufscar.br/bitstream/ufscar/13153/7/BCO%20carta%20comprovante%20autoarquivamento%20.pdf.jpgbbacb9161239dcd189af2f21dff6949cMD57ufscar/131532023-09-18 18:31:59.714oai:repositorio.ufscar.br:ufscar/13153Repositório InstitucionalPUBhttps://repositorio.ufscar.br/oai/requestopendoar:43222023-09-18T18:31:59Repositório Institucional da UFSCAR - Universidade Federal de São Carlos (UFSCAR)false
dc.title.eng.fl_str_mv Biomimetism of Brazil nutshell (Bertholletia excelsa)
dc.title.alternative.por.fl_str_mv Biomimetismo do ouriço da castanha do Pará (Bertholletia excelsa)
title Biomimetism of Brazil nutshell (Bertholletia excelsa)
spellingShingle Biomimetism of Brazil nutshell (Bertholletia excelsa)
Sônego, Marília
Bioinspiração
Ouriço da castanha do Pará
Microestrutura
Propriedades mecânicas
Compósito
Bioinspiration
Brazil nutshell
Mechanical properties
Composite
ENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA::MATERIAIS NAO METALICOS
title_short Biomimetism of Brazil nutshell (Bertholletia excelsa)
title_full Biomimetism of Brazil nutshell (Bertholletia excelsa)
title_fullStr Biomimetism of Brazil nutshell (Bertholletia excelsa)
title_full_unstemmed Biomimetism of Brazil nutshell (Bertholletia excelsa)
title_sort Biomimetism of Brazil nutshell (Bertholletia excelsa)
author Sônego, Marília
author_facet Sônego, Marília
author_role author
dc.contributor.authorlattes.por.fl_str_mv http://lattes.cnpq.br/3460853436777584
dc.contributor.author.fl_str_mv Sônego, Marília
dc.contributor.advisor1.fl_str_mv Pessan, Luiz Antonio
dc.contributor.advisor1Lattes.fl_str_mv http://lattes.cnpq.br/8276650236213537
dc.contributor.authorID.fl_str_mv e3ca4ba0-6da5-4056-8e4a-00588dd963e5
contributor_str_mv Pessan, Luiz Antonio
dc.subject.por.fl_str_mv Bioinspiração
Ouriço da castanha do Pará
Microestrutura
Propriedades mecânicas
Compósito
topic Bioinspiração
Ouriço da castanha do Pará
Microestrutura
Propriedades mecânicas
Compósito
Bioinspiration
Brazil nutshell
Mechanical properties
Composite
ENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA::MATERIAIS NAO METALICOS
dc.subject.eng.fl_str_mv Bioinspiration
Brazil nutshell
Mechanical properties
Composite
dc.subject.cnpq.fl_str_mv ENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA::MATERIAIS NAO METALICOS
description For thousands of years, nature has accumulated countless possibilities for optimized solutions to engineering problems using limited raw material, room temperature, aqueous solutions, solar energy and renewable resources. Recently, this natural accumulated knowledge has increasingly being studied and applied to solve technical problems in studies of biomimicry and bioinspiration.One from many examples are the fruit walls of nuts and drupes which are of special interest for the development of impact and puncture resistant bioinspired structures. This project aims to identify and apply the principles responsible for the excellent mechanical properties of Brazil’s nutshell (Bertholletia excelsa) to develop polymeric composites with superior toughness and mechanical resistance. Firstly, the hierarchical levels of organization of the nutshell structure were identified through chemical analysis, optical microscopy, scanning electron microscopy (SEM) and microtomography (MicroCT). Additionally, the mechanical properties of the nutshell were evaluated in tensile, compression, hardness, and fracture toughness tests, at different length-scales. Moreover, the analysis of fractured surface was carried out by optical microscopy, SEM and MicroCT, identifying the fracture and toughness mechanisms developed by Brazil’s nutshell. Finally, the principles responsible for Brazil’s nutshell mechanical performance were applied to optimize the mechanical performance of a bioinspired polymeric composite. The developed composite is composed of a 3D printed structure of polylactic acid reinforced with 30% of carbon fiber (PLA-30CF) which was impregnated with syntactic foam (epoxy resin and hollow glass microspheres). The mechanical performance of the bioinspired composite is promising. It has density of 0.96 g/cm3, flexural elastic modulus of 2.52 GPa, and impact strength of 1.8 kJ/m2. However, adjustments and improvements in the syntactic foam are still required.
publishDate 2020
dc.date.accessioned.fl_str_mv 2020-08-13T21:07:01Z
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dc.date.issued.fl_str_mv 2020-08-07
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dc.identifier.citation.fl_str_mv SÔNEGO, Marília. Biomimetism of Brazil nutshell (Bertholletia excelsa). 2020. Tese (Doutorado em Ciência e Engenharia de Materiais) – Universidade Federal de São Carlos, São Carlos, 2020. Disponível em: https://repositorio.ufscar.br/handle/ufscar/13153.
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identifier_str_mv SÔNEGO, Marília. Biomimetism of Brazil nutshell (Bertholletia excelsa). 2020. Tese (Doutorado em Ciência e Engenharia de Materiais) – Universidade Federal de São Carlos, São Carlos, 2020. Disponível em: https://repositorio.ufscar.br/handle/ufscar/13153.
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