ESTUDO DO EFEITO ANTIOXIDANTE DA CASCA DO ALHO (ALLIUM SATIVUM) PARA BIODIESEL DE CANOLA
Autor(a) principal: | |
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Data de Publicação: | 2022 |
Tipo de documento: | Dissertação |
Idioma: | por |
Título da fonte: | Biblioteca Digital de Teses e Dissertações do UNICENTRO |
Texto Completo: | http://tede.unicentro.br:8080/jspui/handle/jspui/2136 |
Resumo: | During the decades the planet has suffered several environmental problems due to the use of oil as a raw material in the manufacture of fuel, so the studies related to clean biofuels have increased significantly. Biodiesel has been an alternative to replace fossil fuels, opening a range of production techniques for better quality, innovative alternative routes and the addition of different antioxidants to prevent lipid oxidation of oils. These compounds can be synthetic or natural, both are widely used. However, the synthetic ones can cause harm to the human organism, unlike the natural ones. Tocopherol (vitamin E), present in citric acid, is an example of an antioxidant that is widely used because of its efficiency. Garlic peel is an inedible part and is not consumed, so it fits as agro-industrial waste that contains in its composition polyphenols that present antioxidant activity. The objective of this work is to use the residue of pulverized garlic peel as a natural antioxidant applied to canola oil in biodiesel production. As techniques were used infrared spectroscopy (FTIR) and analysis of elemental composition of garlic peel by EDXRF, accelerated oxidation test (Rancimat® 873), analysis of specific mass, conductivity, pH, viscosity, gas chromatography (GC) in determining the content of esters present in biodiesel and the star experimental planning was 2², cubic model. The extraction media used for this study were: acid, basic and neutral, which were used in the process of obtaining canola biodiesel. The result for canola biodiesel with the addition of 17 g.L-1 with an extraction time of 45 minutes, presented an induction time of 15.46 hours, when we compare this result with the one obtained by pure canola oil that presented a time of 7.95 hours, it is evident the antioxidant capacity of garlic peels. The results obtained for the combination of garlic peel and citric acid at 0.1% was 22 hours, such values meet the minimum required by the ANP of 12 hours. |
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Rodrigues, Paulo Rogério Pintohttp://lattes.cnpq.br/1559766893291724090.179.399-07http://lattes.cnpq.br/6455626509127017PELEGRINI, DÉBORA YUMI2024-02-01T13:31:40Z2022-06-10PELEGRINI, DÉBORA YUMI. ESTUDO DO EFEITO ANTIOXIDANTE DA CASCA DO ALHO (ALLIUM SATIVUM) PARA BIODIESEL DE CANOLA. 2022. 54 f. Dissertação (Programa de Pós-Graduação em Bioenergia - Mestrado) - Universidade Estadual do Centro-Oeste, Guarapuava.http://tede.unicentro.br:8080/jspui/handle/jspui/2136During the decades the planet has suffered several environmental problems due to the use of oil as a raw material in the manufacture of fuel, so the studies related to clean biofuels have increased significantly. Biodiesel has been an alternative to replace fossil fuels, opening a range of production techniques for better quality, innovative alternative routes and the addition of different antioxidants to prevent lipid oxidation of oils. These compounds can be synthetic or natural, both are widely used. However, the synthetic ones can cause harm to the human organism, unlike the natural ones. Tocopherol (vitamin E), present in citric acid, is an example of an antioxidant that is widely used because of its efficiency. Garlic peel is an inedible part and is not consumed, so it fits as agro-industrial waste that contains in its composition polyphenols that present antioxidant activity. The objective of this work is to use the residue of pulverized garlic peel as a natural antioxidant applied to canola oil in biodiesel production. As techniques were used infrared spectroscopy (FTIR) and analysis of elemental composition of garlic peel by EDXRF, accelerated oxidation test (Rancimat® 873), analysis of specific mass, conductivity, pH, viscosity, gas chromatography (GC) in determining the content of esters present in biodiesel and the star experimental planning was 2², cubic model. The extraction media used for this study were: acid, basic and neutral, which were used in the process of obtaining canola biodiesel. The result for canola biodiesel with the addition of 17 g.L-1 with an extraction time of 45 minutes, presented an induction time of 15.46 hours, when we compare this result with the one obtained by pure canola oil that presented a time of 7.95 hours, it is evident the antioxidant capacity of garlic peels. The results obtained for the combination of garlic peel and citric acid at 0.1% was 22 hours, such values meet the minimum required by the ANP of 12 hours.Durante décadas o planeta vem sofrendo diversos problemas ambientais devido a utilização do petróleo como matéria-prima na fabricação de combustível, por isso aumentou - se significativamente os estudos relacionados aos biocombustíveis limpos. O biodiesel vem sendo uma alternativa de substituição dos combustíveis fosseis, abrindo um leque de técnicas de produção para melhor qualidade, rotas alternativas inovadoras e a adição de diferentes antioxidantes para evitar a oxidação lipídicados óleos. Esses compostos podem ser sintéticos ou naturais, ambos são largamente utilizados. Entretanto os sintéticos podem causar danos ao organismo humano ao contrário dos naturais. O tocoferol (vitamina E), presente no ácido cítrico, é um exemplo de antioxidante muito utilizado devido a sua eficiência. A casca do alho é uma parte não comestível e não é consumida, podendo ser classificada como resíduo agroindustrial que contém em sua composição polifenóis que apresentam atividade antioxidante. O objetivo desse trabalho é utilizar o resíduo da casca do alho como antioxidante natural aplicado ao óleo de canola na produção de biodiesel. Como técnicas foram utilizadas espectroscopia no infravermelho (FTIR) e análise de composição elementar da casca do alho por EDXRF, teste de oxidação acelerada (Rancimat® 873), análise demassa específica, condutividade, pH, viscosidade,cromatografia gasosa (CG) na determinação de teor de ésteres presente no biodiesel e o planejamento experimental estrela 2² modelo cúbico. O meios de extração utilizados para este estudo foram: ácido, básico e neutro, os quais foram utilizados no processo de obtenção do biodiesel de canola. O resultado para o biodiesel de canola com a adição de 17 g.L-1 com um tempo de extração de 45 minutos, apresentou um tempo de indução de 15,46 horas, ao compararmos este resultado com o obtido pelo óleo de canola puro que apresentou um tempo de 7,95 horas, é evidente a capacidade antioxidante das cascas de alho. Os resultados obtidos para a combinação de cascas de alho e ácido cítrico a 0,1% foi de 22 horas, tais valores cumprem o mínimo exigido pela ANP de 12 horas.Submitted by Fabiano Jucá (fjuca@unicentro.br) on 2024-02-01T13:31:40Z No. of bitstreams: 1 Dissertação - Débora Yumi Pelegrini.pdf: 3377142 bytes, checksum: 619d77afc5cb54eabb0e3277cd6f358a (MD5)Made available in DSpace on 2024-02-01T13:31:40Z (GMT). No. of bitstreams: 1 Dissertação - Débora Yumi Pelegrini.pdf: 3377142 bytes, checksum: 619d77afc5cb54eabb0e3277cd6f358a (MD5) Previous issue date: 2022-06-10Coordenação de Aperfeiçoamento de Pessoal de Nível Superior - CAPESapplication/pdfhttp://tede.unicentro.br:8080/jspui/retrieve/9248/Disserta%c3%a7%c3%a3o%20-%20D%c3%a9bora%20Yumi%20Pelegrini.pdf.jpgporUniversidade Estadual do Centro-OestePrograma de Pós-Graduação em Bioenergia (Mestrado)UNICENTROBrasilUnicentro::Departamento de Ciências Agrárias e AmbientaisSustentabilidadeCombustíveis limposResíduo AgroindustrialOleaginosasOxidação aceleradaSustainabilityClean fuelsGarlic peelOilseedsCIENCIAS EXATAS E DA TERRA::QUIMICAENGENHARIASCIENCIAS BIOLOGICASCIENCIAS SOCIAIS APLICADAS::ADMINISTRACAOESTUDO DO EFEITO ANTIOXIDANTE DA CASCA DO ALHO (ALLIUM SATIVUM) PARA BIODIESEL DE CANOLAStudy of antioxidante effect of agroindustrial residue for Canola biodieselinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/masterThesis-2202725866144043770600600600600600600600-766110263886347971715717003253031171954518971056484826825-343917884306820216180240354326327782212075167498588264571info:eu-repo/semantics/openAccessreponame:Biblioteca Digital de Teses e Dissertações do UNICENTROinstname:Universidade Estadual do Centro-Oeste (UNICENTRO)instacron:UNICENTROTHUMBNAILDissertação - Débora Yumi Pelegrini.pdf.jpgDissertação - Débora Yumi Pelegrini.pdf.jpgimage/jpeg2991http://localhost:8080/tede/bitstream/jspui/2136/4/Disserta%C3%A7%C3%A3o+-+D%C3%A9bora+Yumi+Pelegrini.pdf.jpgb8842808870201163efdef3a5497cf02MD54TEXTDissertação - Débora Yumi Pelegrini.pdf.txtDissertação - Débora Yumi Pelegrini.pdf.txttext/plain115375http://localhost:8080/tede/bitstream/jspui/2136/3/Disserta%C3%A7%C3%A3o+-+D%C3%A9bora+Yumi+Pelegrini.pdf.txtd441f80966bfbab979190dde7d69ad74MD53ORIGINALDissertação - Débora Yumi Pelegrini.pdfDissertação - Débora Yumi Pelegrini.pdfapplication/pdf3377142http://localhost:8080/tede/bitstream/jspui/2136/2/Disserta%C3%A7%C3%A3o+-+D%C3%A9bora+Yumi+Pelegrini.pdf619d77afc5cb54eabb0e3277cd6f358aMD52LICENSElicense.txtlicense.txttext/plain; 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dc.title.por.fl_str_mv |
ESTUDO DO EFEITO ANTIOXIDANTE DA CASCA DO ALHO (ALLIUM SATIVUM) PARA BIODIESEL DE CANOLA |
dc.title.alternative.eng.fl_str_mv |
Study of antioxidante effect of agroindustrial residue for Canola biodiesel |
title |
ESTUDO DO EFEITO ANTIOXIDANTE DA CASCA DO ALHO (ALLIUM SATIVUM) PARA BIODIESEL DE CANOLA |
spellingShingle |
ESTUDO DO EFEITO ANTIOXIDANTE DA CASCA DO ALHO (ALLIUM SATIVUM) PARA BIODIESEL DE CANOLA PELEGRINI, DÉBORA YUMI Sustentabilidade Combustíveis limpos Resíduo Agroindustrial Oleaginosas Oxidação acelerada Sustainability Clean fuels Garlic peel Oilseeds CIENCIAS EXATAS E DA TERRA::QUIMICA ENGENHARIAS CIENCIAS BIOLOGICAS CIENCIAS SOCIAIS APLICADAS::ADMINISTRACAO |
title_short |
ESTUDO DO EFEITO ANTIOXIDANTE DA CASCA DO ALHO (ALLIUM SATIVUM) PARA BIODIESEL DE CANOLA |
title_full |
ESTUDO DO EFEITO ANTIOXIDANTE DA CASCA DO ALHO (ALLIUM SATIVUM) PARA BIODIESEL DE CANOLA |
title_fullStr |
ESTUDO DO EFEITO ANTIOXIDANTE DA CASCA DO ALHO (ALLIUM SATIVUM) PARA BIODIESEL DE CANOLA |
title_full_unstemmed |
ESTUDO DO EFEITO ANTIOXIDANTE DA CASCA DO ALHO (ALLIUM SATIVUM) PARA BIODIESEL DE CANOLA |
title_sort |
ESTUDO DO EFEITO ANTIOXIDANTE DA CASCA DO ALHO (ALLIUM SATIVUM) PARA BIODIESEL DE CANOLA |
author |
PELEGRINI, DÉBORA YUMI |
author_facet |
PELEGRINI, DÉBORA YUMI |
author_role |
author |
dc.contributor.advisor1.fl_str_mv |
Rodrigues, Paulo Rogério Pinto |
dc.contributor.advisor1Lattes.fl_str_mv |
http://lattes.cnpq.br/1559766893291724 |
dc.contributor.authorID.fl_str_mv |
090.179.399-07 |
dc.contributor.authorLattes.fl_str_mv |
http://lattes.cnpq.br/6455626509127017 |
dc.contributor.author.fl_str_mv |
PELEGRINI, DÉBORA YUMI |
contributor_str_mv |
Rodrigues, Paulo Rogério Pinto |
dc.subject.por.fl_str_mv |
Sustentabilidade Combustíveis limpos Resíduo Agroindustrial Oleaginosas Oxidação acelerada |
topic |
Sustentabilidade Combustíveis limpos Resíduo Agroindustrial Oleaginosas Oxidação acelerada Sustainability Clean fuels Garlic peel Oilseeds CIENCIAS EXATAS E DA TERRA::QUIMICA ENGENHARIAS CIENCIAS BIOLOGICAS CIENCIAS SOCIAIS APLICADAS::ADMINISTRACAO |
dc.subject.eng.fl_str_mv |
Sustainability Clean fuels Garlic peel Oilseeds |
dc.subject.cnpq.fl_str_mv |
CIENCIAS EXATAS E DA TERRA::QUIMICA ENGENHARIAS CIENCIAS BIOLOGICAS CIENCIAS SOCIAIS APLICADAS::ADMINISTRACAO |
description |
During the decades the planet has suffered several environmental problems due to the use of oil as a raw material in the manufacture of fuel, so the studies related to clean biofuels have increased significantly. Biodiesel has been an alternative to replace fossil fuels, opening a range of production techniques for better quality, innovative alternative routes and the addition of different antioxidants to prevent lipid oxidation of oils. These compounds can be synthetic or natural, both are widely used. However, the synthetic ones can cause harm to the human organism, unlike the natural ones. Tocopherol (vitamin E), present in citric acid, is an example of an antioxidant that is widely used because of its efficiency. Garlic peel is an inedible part and is not consumed, so it fits as agro-industrial waste that contains in its composition polyphenols that present antioxidant activity. The objective of this work is to use the residue of pulverized garlic peel as a natural antioxidant applied to canola oil in biodiesel production. As techniques were used infrared spectroscopy (FTIR) and analysis of elemental composition of garlic peel by EDXRF, accelerated oxidation test (Rancimat® 873), analysis of specific mass, conductivity, pH, viscosity, gas chromatography (GC) in determining the content of esters present in biodiesel and the star experimental planning was 2², cubic model. The extraction media used for this study were: acid, basic and neutral, which were used in the process of obtaining canola biodiesel. The result for canola biodiesel with the addition of 17 g.L-1 with an extraction time of 45 minutes, presented an induction time of 15.46 hours, when we compare this result with the one obtained by pure canola oil that presented a time of 7.95 hours, it is evident the antioxidant capacity of garlic peels. The results obtained for the combination of garlic peel and citric acid at 0.1% was 22 hours, such values meet the minimum required by the ANP of 12 hours. |
publishDate |
2022 |
dc.date.issued.fl_str_mv |
2022-06-10 |
dc.date.accessioned.fl_str_mv |
2024-02-01T13:31:40Z |
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masterThesis |
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PELEGRINI, DÉBORA YUMI. ESTUDO DO EFEITO ANTIOXIDANTE DA CASCA DO ALHO (ALLIUM SATIVUM) PARA BIODIESEL DE CANOLA. 2022. 54 f. Dissertação (Programa de Pós-Graduação em Bioenergia - Mestrado) - Universidade Estadual do Centro-Oeste, Guarapuava. |
dc.identifier.uri.fl_str_mv |
http://tede.unicentro.br:8080/jspui/handle/jspui/2136 |
identifier_str_mv |
PELEGRINI, DÉBORA YUMI. ESTUDO DO EFEITO ANTIOXIDANTE DA CASCA DO ALHO (ALLIUM SATIVUM) PARA BIODIESEL DE CANOLA. 2022. 54 f. Dissertação (Programa de Pós-Graduação em Bioenergia - Mestrado) - Universidade Estadual do Centro-Oeste, Guarapuava. |
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por |
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UNICENTRO |
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Brasil |
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Unicentro::Departamento de Ciências Agrárias e Ambientais |
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Universidade Estadual do Centro-Oeste |
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