Synthesis and characterization of aliphatic polyesters from glycerol, by-product of biodiesel production, and adipic acid
Autor(a) principal: | |
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Data de Publicação: | 2007 |
Outros Autores: | , , , , |
Tipo de documento: | Artigo |
Idioma: | eng |
Título da fonte: | Repositório Institucional da UFBA |
Texto Completo: | http://www.repositorio.ufba.br/ri/handle/ri/4913 |
Resumo: | p. 335-339,Oct/Dec. |
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Brioude, Michel de MeirelesGuimarães, Danilo HansenFiuza, Raigenis da PazPrado, Luis Antônio Sanches de AlmeidaBoaventura Filho, Jaime SoaresJosé, Nadia MamedeBrioude, Michel de MeirelesGuimarães, Danilo HansenFiuza, Raigenis da PazPrado, Luis Antônio Sanches de AlmeidaBoaventura Filho, Jaime SoaresJosé, Nadia Mamede2011-12-20T09:54:13Z2011-12-20T09:54:13Z20071516-1439http://www.repositorio.ufba.br/ri/handle/ri/4913v. 10, n. 4.p. 335-339,Oct/Dec.In the present work, polyesters were prepared from the polycondensation between glycerol and adipic acid using dibutyltin dilaurate as catalyst. Three glycerol: adipic acid molar ratio were used for the bulk polymerization namely: 2:2; 2:3 and 2:4. FTIR confirmed the esterification of glycerol by the acid for all the polymers. DSC and XRD indicated no crystallinity for all the polymers. The morphology of the materials are characterized by globular structure, which may suggest compositional fluctuations throughout the samples.Submitted by JURANDI DE SOUZA SILVA (jssufba@hotmail.com) on 2011-12-20T09:54:13Z No. of bitstreams: 1 a03v10n4.pdf: 1960034 bytes, checksum: 398e914256455ee6a8df5974a70fb083 (MD5)Made available in DSpace on 2011-12-20T09:54:13Z (GMT). No. of bitstreams: 1 a03v10n4.pdf: 1960034 bytes, checksum: 398e914256455ee6a8df5974a70fb083 (MD5) Previous issue date: 2007São Carloshttp://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392007000400003&lng=en&nrm=isoreponame:Repositório Institucional da UFBAinstname:Universidade Federal da Bahia (UFBA)instacron:UFBAPolyesterGlycerolBiodieselSynthesis and characterization of aliphatic polyesters from glycerol, by-product of biodiesel production, and adipic acidMaterials Researchinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/articleenginfo:eu-repo/semantics/openAccessORIGINALa03v10n4.pdfa03v10n4.pdfapplication/pdf1960034https://repositorio.ufba.br/bitstream/ri/4913/1/a03v10n4.pdf398e914256455ee6a8df5974a70fb083MD51LICENSElicense.txtlicense.txttext/plain1809https://repositorio.ufba.br/bitstream/ri/4913/2/license.txt8bb3e3eb871f5854a9ec419f68651b60MD52TEXTa03v10n4.pdf.txta03v10n4.pdf.txtExtracted texttext/plain17989https://repositorio.ufba.br/bitstream/ri/4913/3/a03v10n4.pdf.txt06ab22f1b2c5a82e9beaf506a5ef7847MD53ri/49132022-07-05 14:03:08.629oai:repositorio.ufba.br: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ório InstitucionalPUBhttp://192.188.11.11:8080/oai/requestopendoar:19322022-07-05T17:03:08Repositório Institucional da UFBA - Universidade Federal da Bahia (UFBA)false |
dc.title.pt_BR.fl_str_mv |
Synthesis and characterization of aliphatic polyesters from glycerol, by-product of biodiesel production, and adipic acid |
dc.title.alternative.pt_BR.fl_str_mv |
Materials Research |
title |
Synthesis and characterization of aliphatic polyesters from glycerol, by-product of biodiesel production, and adipic acid |
spellingShingle |
Synthesis and characterization of aliphatic polyesters from glycerol, by-product of biodiesel production, and adipic acid Brioude, Michel de Meireles Polyester Glycerol Biodiesel |
title_short |
Synthesis and characterization of aliphatic polyesters from glycerol, by-product of biodiesel production, and adipic acid |
title_full |
Synthesis and characterization of aliphatic polyesters from glycerol, by-product of biodiesel production, and adipic acid |
title_fullStr |
Synthesis and characterization of aliphatic polyesters from glycerol, by-product of biodiesel production, and adipic acid |
title_full_unstemmed |
Synthesis and characterization of aliphatic polyesters from glycerol, by-product of biodiesel production, and adipic acid |
title_sort |
Synthesis and characterization of aliphatic polyesters from glycerol, by-product of biodiesel production, and adipic acid |
author |
Brioude, Michel de Meireles |
author_facet |
Brioude, Michel de Meireles Guimarães, Danilo Hansen Fiuza, Raigenis da Paz Prado, Luis Antônio Sanches de Almeida Boaventura Filho, Jaime Soares José, Nadia Mamede |
author_role |
author |
author2 |
Guimarães, Danilo Hansen Fiuza, Raigenis da Paz Prado, Luis Antônio Sanches de Almeida Boaventura Filho, Jaime Soares José, Nadia Mamede |
author2_role |
author author author author author |
dc.contributor.author.fl_str_mv |
Brioude, Michel de Meireles Guimarães, Danilo Hansen Fiuza, Raigenis da Paz Prado, Luis Antônio Sanches de Almeida Boaventura Filho, Jaime Soares José, Nadia Mamede Brioude, Michel de Meireles Guimarães, Danilo Hansen Fiuza, Raigenis da Paz Prado, Luis Antônio Sanches de Almeida Boaventura Filho, Jaime Soares José, Nadia Mamede |
dc.subject.por.fl_str_mv |
Polyester Glycerol Biodiesel |
topic |
Polyester Glycerol Biodiesel |
description |
p. 335-339,Oct/Dec. |
publishDate |
2007 |
dc.date.issued.fl_str_mv |
2007 |
dc.date.accessioned.fl_str_mv |
2011-12-20T09:54:13Z |
dc.date.available.fl_str_mv |
2011-12-20T09:54:13Z |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
http://www.repositorio.ufba.br/ri/handle/ri/4913 |
dc.identifier.issn.none.fl_str_mv |
1516-1439 |
dc.identifier.number.pt_BR.fl_str_mv |
v. 10, n. 4. |
identifier_str_mv |
1516-1439 v. 10, n. 4. |
url |
http://www.repositorio.ufba.br/ri/handle/ri/4913 |
dc.language.iso.fl_str_mv |
eng |
language |
eng |
dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess |
eu_rights_str_mv |
openAccess |
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http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392007000400003&lng=en&nrm=iso |
dc.source.none.fl_str_mv |
reponame:Repositório Institucional da UFBA instname:Universidade Federal da Bahia (UFBA) instacron:UFBA |
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Universidade Federal da Bahia (UFBA) |
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UFBA |
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UFBA |
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Repositório Institucional da UFBA |
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Repositório Institucional da UFBA |
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