Synthesis and characterization of aliphatic polyesters from glycerol, by-product of biodiesel production, and adipic acid

Detalhes bibliográficos
Autor(a) principal: Brioude, Michel de Meireles
Data de Publicação: 2007
Outros Autores: Guimarães, Danilo Hansen, Fiuza, Raigenis da Paz, Prado, Luis Antônio Sanches de Almeida, Boaventura Filho, Jaime Soares, José, Nadia Mamede
Tipo de documento: Artigo
Idioma: eng
Título da fonte: Repositório Institucional da UFBA
Texto Completo: http://www.repositorio.ufba.br/ri/handle/ri/4913
Resumo: p. 335-339,Oct/Dec.
id UFBA-2_1a27f86b9e95ff392bf7fc2348c1fdf2
oai_identifier_str oai:repositorio.ufba.br:ri/4913
network_acronym_str UFBA-2
network_name_str Repositório Institucional da UFBA
repository_id_str 1932
spelling Brioude, Michel de MeirelesGuimarães, Danilo HansenFiuza, Raigenis da PazPrado, Luis Antônio Sanches de AlmeidaBoaventura Filho, Jaime SoaresJosé, Nadia MamedeBrioude, Michel de MeirelesGuimarães, Danilo HansenFiuza, Raigenis da PazPrado, Luis Antônio Sanches de AlmeidaBoaventura Filho, Jaime SoaresJosé, Nadia Mamede2011-12-20T09:54:13Z2011-12-20T09:54:13Z20071516-1439http://www.repositorio.ufba.br/ri/handle/ri/4913v. 10, n. 4.p. 335-339,Oct/Dec.In the present work, polyesters were prepared from the polycondensation between glycerol and adipic acid using dibutyltin dilaurate as catalyst. Three glycerol: adipic acid molar ratio were used for the bulk polymerization namely: 2:2; 2:3 and 2:4. FTIR confirmed the esterification of glycerol by the acid for all the polymers. DSC and XRD indicated no crystallinity for all the polymers. The morphology of the materials are characterized by globular structure, which may suggest compositional fluctuations throughout the samples.Submitted by JURANDI DE SOUZA SILVA (jssufba@hotmail.com) on 2011-12-20T09:54:13Z No. of bitstreams: 1 a03v10n4.pdf: 1960034 bytes, checksum: 398e914256455ee6a8df5974a70fb083 (MD5)Made available in DSpace on 2011-12-20T09:54:13Z (GMT). No. of bitstreams: 1 a03v10n4.pdf: 1960034 bytes, checksum: 398e914256455ee6a8df5974a70fb083 (MD5) Previous issue date: 2007São Carloshttp://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392007000400003&lng=en&nrm=isoreponame:Repositório Institucional da UFBAinstname:Universidade Federal da Bahia (UFBA)instacron:UFBAPolyesterGlycerolBiodieselSynthesis and characterization of aliphatic polyesters from glycerol, by-product of biodiesel production, and adipic acidMaterials Researchinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/articleenginfo:eu-repo/semantics/openAccessORIGINALa03v10n4.pdfa03v10n4.pdfapplication/pdf1960034https://repositorio.ufba.br/bitstream/ri/4913/1/a03v10n4.pdf398e914256455ee6a8df5974a70fb083MD51LICENSElicense.txtlicense.txttext/plain1809https://repositorio.ufba.br/bitstream/ri/4913/2/license.txt8bb3e3eb871f5854a9ec419f68651b60MD52TEXTa03v10n4.pdf.txta03v10n4.pdf.txtExtracted texttext/plain17989https://repositorio.ufba.br/bitstream/ri/4913/3/a03v10n4.pdf.txt06ab22f1b2c5a82e9beaf506a5ef7847MD53ri/49132022-07-05 14:03:08.629oai:repositorio.ufba.br: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ório InstitucionalPUBhttp://192.188.11.11:8080/oai/requestopendoar:19322022-07-05T17:03:08Repositório Institucional da UFBA - Universidade Federal da Bahia (UFBA)false
dc.title.pt_BR.fl_str_mv Synthesis and characterization of aliphatic polyesters from glycerol, by-product of biodiesel production, and adipic acid
dc.title.alternative.pt_BR.fl_str_mv Materials Research
title Synthesis and characterization of aliphatic polyesters from glycerol, by-product of biodiesel production, and adipic acid
spellingShingle Synthesis and characterization of aliphatic polyesters from glycerol, by-product of biodiesel production, and adipic acid
Brioude, Michel de Meireles
Polyester
Glycerol
Biodiesel
title_short Synthesis and characterization of aliphatic polyesters from glycerol, by-product of biodiesel production, and adipic acid
title_full Synthesis and characterization of aliphatic polyesters from glycerol, by-product of biodiesel production, and adipic acid
title_fullStr Synthesis and characterization of aliphatic polyesters from glycerol, by-product of biodiesel production, and adipic acid
title_full_unstemmed Synthesis and characterization of aliphatic polyesters from glycerol, by-product of biodiesel production, and adipic acid
title_sort Synthesis and characterization of aliphatic polyesters from glycerol, by-product of biodiesel production, and adipic acid
author Brioude, Michel de Meireles
author_facet Brioude, Michel de Meireles
Guimarães, Danilo Hansen
Fiuza, Raigenis da Paz
Prado, Luis Antônio Sanches de Almeida
Boaventura Filho, Jaime Soares
José, Nadia Mamede
author_role author
author2 Guimarães, Danilo Hansen
Fiuza, Raigenis da Paz
Prado, Luis Antônio Sanches de Almeida
Boaventura Filho, Jaime Soares
José, Nadia Mamede
author2_role author
author
author
author
author
dc.contributor.author.fl_str_mv Brioude, Michel de Meireles
Guimarães, Danilo Hansen
Fiuza, Raigenis da Paz
Prado, Luis Antônio Sanches de Almeida
Boaventura Filho, Jaime Soares
José, Nadia Mamede
Brioude, Michel de Meireles
Guimarães, Danilo Hansen
Fiuza, Raigenis da Paz
Prado, Luis Antônio Sanches de Almeida
Boaventura Filho, Jaime Soares
José, Nadia Mamede
dc.subject.por.fl_str_mv Polyester
Glycerol
Biodiesel
topic Polyester
Glycerol
Biodiesel
description p. 335-339,Oct/Dec.
publishDate 2007
dc.date.issued.fl_str_mv 2007
dc.date.accessioned.fl_str_mv 2011-12-20T09:54:13Z
dc.date.available.fl_str_mv 2011-12-20T09:54:13Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv http://www.repositorio.ufba.br/ri/handle/ri/4913
dc.identifier.issn.none.fl_str_mv 1516-1439
dc.identifier.number.pt_BR.fl_str_mv v. 10, n. 4.
identifier_str_mv 1516-1439
v. 10, n. 4.
url http://www.repositorio.ufba.br/ri/handle/ri/4913
dc.language.iso.fl_str_mv eng
language eng
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.source.pt_BR.fl_str_mv http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392007000400003&lng=en&nrm=iso
dc.source.none.fl_str_mv reponame:Repositório Institucional da UFBA
instname:Universidade Federal da Bahia (UFBA)
instacron:UFBA
instname_str Universidade Federal da Bahia (UFBA)
instacron_str UFBA
institution UFBA
reponame_str Repositório Institucional da UFBA
collection Repositório Institucional da UFBA
bitstream.url.fl_str_mv https://repositorio.ufba.br/bitstream/ri/4913/1/a03v10n4.pdf
https://repositorio.ufba.br/bitstream/ri/4913/2/license.txt
https://repositorio.ufba.br/bitstream/ri/4913/3/a03v10n4.pdf.txt
bitstream.checksum.fl_str_mv 398e914256455ee6a8df5974a70fb083
8bb3e3eb871f5854a9ec419f68651b60
06ab22f1b2c5a82e9beaf506a5ef7847
bitstream.checksumAlgorithm.fl_str_mv MD5
MD5
MD5
repository.name.fl_str_mv Repositório Institucional da UFBA - Universidade Federal da Bahia (UFBA)
repository.mail.fl_str_mv
_version_ 1808459390592745472