Determination of Mo and V in multiphase gasoline emulsions by electrothermal atomic absorption spectrometry
Autor(a) principal: | |
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Data de Publicação: | 2006 |
Outros Autores: | , |
Tipo de documento: | Artigo |
Idioma: | eng |
Título da fonte: | Repositório Institucional da UFBA |
Texto Completo: | http://www.repositorio.ufba.br/ri/handle/ri/12742 |
Resumo: | Texto completo: acesso restrito. p.592–595 |
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Santos, Denilson Santana Sodré dosTeixeira, Alete PaixãoKorn, Maria das Graças AndradeSantos, Denilson Santana Sodré dosTeixeira, Alete PaixãoKorn, Maria das Graças Andrade2013-08-27T10:59:11Z20060584-8547http://www.repositorio.ufba.br/ri/handle/ri/12742v.61 n. 5Texto completo: acesso restrito. p.592–595This paper proposes an alternative analytical method using electrothermal atomic absorption spectrometry to determine Mo and V in multiphase gasoline emulsions. Samples were prepared by mixing gasoline with a nitric acid solution (0.1% v/v) and two cationic surfactants. The mixture was sonicated, resulting in an emulsive system. Calibration was done by using the aforementioned solutions with added analyte. The detection limits (3σ) of Mo and V were 0.9 μg l− 1 and 4.7 μg l− 1, respectively. The accuracy and precision of the proposed method were evaluated by the analysis of samples spiked with metallo-organic standard and the relative standard deviation obtained ranged from 1.2% to 4.4% in samples spiked with 2 μg l− 1 of each metal. The recovery rates varied from 91.2% to 101.6%. The proposed method was applied to determine Mo and V in samples of gasoline from different gas stations.Submitted by Edileide Reis (leyde-landy@hotmail.com) on 2013-08-27T10:59:11Z No. of bitstreams: 1 1-s2.0-S0584854706000917-main.pdf: 104931 bytes, checksum: 1765d1a83889c3a6c930bea33eab946b (MD5)Made available in DSpace on 2013-08-27T10:59:11Z (GMT). No. of bitstreams: 1 1-s2.0-S0584854706000917-main.pdf: 104931 bytes, checksum: 1765d1a83889c3a6c930bea33eab946b (MD5) Previous issue date: 2006http://dx.doi.org.ez10.periodicos.capes.gov.br/10.1016/j.sab.2006.03.010reponame:Repositório Institucional da UFBAinstname:Universidade Federal da Bahia (UFBA)instacron:UFBAGasolineMultiphase emulsionElectrothermal atomic absorption spectrometryDetermination of Mo and V in multiphase gasoline emulsions by electrothermal atomic absorption spectrometrySpectrochimica Acta Part B: Atomic Spectroscopyinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/article10000-01-01enginfo:eu-repo/semantics/openAccessORIGINAL1-s2.0-S0584854706000917-main.pdf1-s2.0-S0584854706000917-main.pdfapplication/pdf104931https://repositorio.ufba.br/bitstream/ri/12742/1/1-s2.0-S0584854706000917-main.pdf1765d1a83889c3a6c930bea33eab946bMD51LICENSElicense.txtlicense.txttext/plain1762https://repositorio.ufba.br/bitstream/ri/12742/2/license.txt1b89a9a0548218172d7c829f87a0eab9MD52TEXT1-s2.0-S0584854706000917-main.pdf.txt1-s2.0-S0584854706000917-main.pdf.txtExtracted texttext/plain17874https://repositorio.ufba.br/bitstream/ri/12742/3/1-s2.0-S0584854706000917-main.pdf.txte66d6c7bf6817ca0d048ce0104ecc9b5MD53ri/127422022-07-05 14:02:49.878oai:repositorio.ufba.br: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Repositório InstitucionalPUBhttp://192.188.11.11:8080/oai/requestopendoar:19322022-07-05T17:02:49Repositório Institucional da UFBA - Universidade Federal da Bahia (UFBA)false |
dc.title.pt_BR.fl_str_mv |
Determination of Mo and V in multiphase gasoline emulsions by electrothermal atomic absorption spectrometry |
dc.title.alternative.pt_BR.fl_str_mv |
Spectrochimica Acta Part B: Atomic Spectroscopy |
title |
Determination of Mo and V in multiphase gasoline emulsions by electrothermal atomic absorption spectrometry |
spellingShingle |
Determination of Mo and V in multiphase gasoline emulsions by electrothermal atomic absorption spectrometry Santos, Denilson Santana Sodré dos Gasoline Multiphase emulsion Electrothermal atomic absorption spectrometry |
title_short |
Determination of Mo and V in multiphase gasoline emulsions by electrothermal atomic absorption spectrometry |
title_full |
Determination of Mo and V in multiphase gasoline emulsions by electrothermal atomic absorption spectrometry |
title_fullStr |
Determination of Mo and V in multiphase gasoline emulsions by electrothermal atomic absorption spectrometry |
title_full_unstemmed |
Determination of Mo and V in multiphase gasoline emulsions by electrothermal atomic absorption spectrometry |
title_sort |
Determination of Mo and V in multiphase gasoline emulsions by electrothermal atomic absorption spectrometry |
author |
Santos, Denilson Santana Sodré dos |
author_facet |
Santos, Denilson Santana Sodré dos Teixeira, Alete Paixão Korn, Maria das Graças Andrade |
author_role |
author |
author2 |
Teixeira, Alete Paixão Korn, Maria das Graças Andrade |
author2_role |
author author |
dc.contributor.author.fl_str_mv |
Santos, Denilson Santana Sodré dos Teixeira, Alete Paixão Korn, Maria das Graças Andrade Santos, Denilson Santana Sodré dos Teixeira, Alete Paixão Korn, Maria das Graças Andrade |
dc.subject.por.fl_str_mv |
Gasoline Multiphase emulsion Electrothermal atomic absorption spectrometry |
topic |
Gasoline Multiphase emulsion Electrothermal atomic absorption spectrometry |
description |
Texto completo: acesso restrito. p.592–595 |
publishDate |
2006 |
dc.date.issued.fl_str_mv |
2006 |
dc.date.accessioned.fl_str_mv |
2013-08-27T10:59:11Z |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
http://www.repositorio.ufba.br/ri/handle/ri/12742 |
dc.identifier.issn.none.fl_str_mv |
0584-8547 |
dc.identifier.number.pt_BR.fl_str_mv |
v.61 n. 5 |
identifier_str_mv |
0584-8547 v.61 n. 5 |
url |
http://www.repositorio.ufba.br/ri/handle/ri/12742 |
dc.language.iso.fl_str_mv |
eng |
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eng |
dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess |
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openAccess |
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http://dx.doi.org.ez10.periodicos.capes.gov.br/10.1016/j.sab.2006.03.010 |
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Universidade Federal da Bahia (UFBA) |
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