Determination of Mo and V in multiphase gasoline emulsions by electrothermal atomic absorption spectrometry

Detalhes bibliográficos
Autor(a) principal: Santos, Denilson Santana Sodré dos
Data de Publicação: 2006
Outros Autores: Teixeira, Alete Paixão, Korn, Maria das Graças Andrade
Tipo de documento: Artigo
Idioma: eng
Título da fonte: Repositório Institucional da UFBA
Texto Completo: http://www.repositorio.ufba.br/ri/handle/ri/12742
Resumo: Texto completo: acesso restrito. p.592–595
id UFBA-2_4f9ef2f5cded79235fe562892606c33d
oai_identifier_str oai:repositorio.ufba.br:ri/12742
network_acronym_str UFBA-2
network_name_str Repositório Institucional da UFBA
repository_id_str 1932
spelling Santos, Denilson Santana Sodré dosTeixeira, Alete PaixãoKorn, Maria das Graças AndradeSantos, Denilson Santana Sodré dosTeixeira, Alete PaixãoKorn, Maria das Graças Andrade2013-08-27T10:59:11Z20060584-8547http://www.repositorio.ufba.br/ri/handle/ri/12742v.61 n. 5Texto completo: acesso restrito. p.592–595This paper proposes an alternative analytical method using electrothermal atomic absorption spectrometry to determine Mo and V in multiphase gasoline emulsions. Samples were prepared by mixing gasoline with a nitric acid solution (0.1% v/v) and two cationic surfactants. The mixture was sonicated, resulting in an emulsive system. Calibration was done by using the aforementioned solutions with added analyte. The detection limits (3σ) of Mo and V were 0.9 μg l− 1 and 4.7 μg l− 1, respectively. The accuracy and precision of the proposed method were evaluated by the analysis of samples spiked with metallo-organic standard and the relative standard deviation obtained ranged from 1.2% to 4.4% in samples spiked with 2 μg l− 1 of each metal. The recovery rates varied from 91.2% to 101.6%. The proposed method was applied to determine Mo and V in samples of gasoline from different gas stations.Submitted by Edileide Reis (leyde-landy@hotmail.com) on 2013-08-27T10:59:11Z No. of bitstreams: 1 1-s2.0-S0584854706000917-main.pdf: 104931 bytes, checksum: 1765d1a83889c3a6c930bea33eab946b (MD5)Made available in DSpace on 2013-08-27T10:59:11Z (GMT). No. of bitstreams: 1 1-s2.0-S0584854706000917-main.pdf: 104931 bytes, checksum: 1765d1a83889c3a6c930bea33eab946b (MD5) Previous issue date: 2006http://dx.doi.org.ez10.periodicos.capes.gov.br/10.1016/j.sab.2006.03.010reponame:Repositório Institucional da UFBAinstname:Universidade Federal da Bahia (UFBA)instacron:UFBAGasolineMultiphase emulsionElectrothermal atomic absorption spectrometryDetermination of Mo and V in multiphase gasoline emulsions by electrothermal atomic absorption spectrometrySpectrochimica Acta Part B: Atomic Spectroscopyinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/article10000-01-01enginfo:eu-repo/semantics/openAccessORIGINAL1-s2.0-S0584854706000917-main.pdf1-s2.0-S0584854706000917-main.pdfapplication/pdf104931https://repositorio.ufba.br/bitstream/ri/12742/1/1-s2.0-S0584854706000917-main.pdf1765d1a83889c3a6c930bea33eab946bMD51LICENSElicense.txtlicense.txttext/plain1762https://repositorio.ufba.br/bitstream/ri/12742/2/license.txt1b89a9a0548218172d7c829f87a0eab9MD52TEXT1-s2.0-S0584854706000917-main.pdf.txt1-s2.0-S0584854706000917-main.pdf.txtExtracted texttext/plain17874https://repositorio.ufba.br/bitstream/ri/12742/3/1-s2.0-S0584854706000917-main.pdf.txte66d6c7bf6817ca0d048ce0104ecc9b5MD53ri/127422022-07-05 14:02:49.878oai:repositorio.ufba.br:ri/12742VGVybW8gZGUgTGljZW7vv71hLCBu77+9byBleGNsdXNpdm8sIHBhcmEgbyBkZXDvv71zaXRvIG5vIHJlcG9zaXTvv71yaW8gSW5zdGl0dWNpb25hbCBkYSBVRkJBCgogICAgUGVsbyBwcm9jZXNzbyBkZSBzdWJtaXNz77+9byBkZSBkb2N1bWVudG9zLCBvIGF1dG9yIG91IHNldQpyZXByZXNlbnRhbnRlIGxlZ2FsLCBhbyBhY2VpdGFyIGVzc2UgdGVybW8gZGUgbGljZW7vv71hLCBjb25jZWRlIGFvClJlcG9zaXTvv71yaW8gSW5zdGl0dWNpb25hbCBkYSBVbml2ZXJzaWRhZGUgRmVkZXJhbCBkYSBCYWhpYSBvIGRpcmVpdG8KZGUgbWFudGVyIHVtYSBj77+9cGlhIGVtIHNldSByZXBvc2l077+9cmlvIGNvbSBhIGZpbmFsaWRhZGUsIHByaW1laXJhLCAKZGUgcHJlc2VydmHvv73vv71vLiBFc3NlcyB0ZXJtb3MsIG7vv71vIGV4Y2x1c2l2b3MsIG1hbnTvv71tIG9zIGRpcmVpdG9zIGRlIAphdXRvci9jb3B5cmlnaHQsIG1hcyBlbnRlbmRlIG8gZG9jdW1lbnRvIGNvbW8gcGFydGUgZG8gYWNlcnZvIGludGVsZWN0dWFsIGRlc3NhIFVuaXZlcnNpZGFkZS4gCgogICAgUGFyYSBvcyBkb2N1bWVudG9zIHB1YmxpY2Fkb3MgY29tIHJlcGFzc2UgZGUgZGlyZWl0b3MgZGUgZGlzdHJpYnVp77+977+9bywgZXNzZSB0ZXJtbyBkZSBsaWNlbu+/vWEgZW50ZW5kZSBxdWU6IAoKICAgIE1hbnRlbmRvIG9zICBkaXJlaXRvcyBhdXRvcmFpcywgcmVwYXNzYWRvcyBhIHRlcmNlaXJvcywgZW0gY2FzbyAKZGUgcHVibGljYe+/ve+/vWVzLCBvIHJlcG9zaXTvv71yaW8gcG9kZSByZXN0cmluZ2lyIG8gYWNlc3NvIGFvIHRleHRvIAppbnRlZ3JhbCwgbWFzIGxpYmVyYSBhcyBpbmZvcm1h77+977+9ZXMgc29icmUgbyBkb2N1bWVudG8gKE1ldGFkYWRvcyBkZXNjcml0aXZvcykuCgogRGVzdGEgZm9ybWEsIGF0ZW5kZW5kbyBhb3MgYW5zZWlvcyBkZXNzYSB1bml2ZXJzaWRhZGUgCmVtIG1hbnRlciBzdWEgcHJvZHXvv73vv71vIGNpZW5077+9ZmljYSBjb20gYXMgcmVzdHJp77+977+9ZXMgaW1wb3N0YXMgcGVsb3MgCmVkaXRvcmVzIGRlIHBlcmnvv71kaWNvcy4gCgogICAgUGFyYSBhcyBwdWJsaWNh77+977+9ZXMgZW0gaW5pY2lhdGl2YXMgcXVlIHNlZ3VlbSBhIHBvbO+/vXRpY2EgZGUgCkFjZXNzbyBBYmVydG8sIG9zIGRlcO+/vXNpdG9zIGNvbXB1bHPvv71yaW9zIG5lc3NlIHJlcG9zaXTvv71yaW8gbWFudO+/vW0gCm9zIGRpcmVpdG9zIGF1dG9yYWlzLCBtYXMgbWFudO+/vW0gbyBhY2Vzc28gaXJyZXN0cml0byBhbyBtZXRhZGFkb3MgCmUgdGV4dG8gY29tcGxldG8uIEFzc2ltLCBhIGFjZWl0Ye+/ve+/vW8gZGVzc2UgdGVybW8gbu+/vW8gbmVjZXNzaXRhIGRlIApjb25zZW50aW1lbnRvIHBvciBwYXJ0ZSBkZSBhdXRvcmVzL2RldGVudG9yZXMgZG9zIGRpcmVpdG9zLCBwb3IgCmVzdGFyZW0gZW0gaW5pY2lhdGl2YXMgZGUgYWNlc3NvIGFiZXJ0by4KCiAgICBFbSBhbWJvcyBvIGNhc28sIGVzc2UgdGVybW8gZGUgbGljZW7vv71hLCBwb2RlIHNlciBhY2VpdG8gcGVsbyAKYXV0b3IsIGRldGVudG9yZXMgZGUgZGlyZWl0b3MgZS9vdSB0ZXJjZWlyb3MgYW1wYXJhZG9zIHBlbGEgCnVuaXZlcnNpZGFkZS4gRGV2aWRvIGFvcyBkaWZlcmVudGVzIHByb2Nlc3NvcyBwZWxvIHF1YWwgYSBzdWJtaXNz77+9byAKcG9kZSBvY29ycmVyLCBvIHJlcG9zaXTvv71yaW8gcGVybWl0ZSBhIGFjZWl0Ye+/ve+/vW8gZGEgbGljZW7vv71hIHBvciAKdGVyY2Vpcm9zLCBzb21lbnRlIG5vcyBjYXNvcyBkZSBkb2N1bWVudG9zIHByb2R1emlkb3MgcG9yIGludGVncmFudGVzIApkYSBVRkJBIGUgc3VibWV0aWRvcyBwb3IgcGVzc29hcyBhbXBhcmFkYXMgcG9yIGVzdGEgaW5zdGl0dWnvv73vv71vLgo=Repositório InstitucionalPUBhttp://192.188.11.11:8080/oai/requestopendoar:19322022-07-05T17:02:49Repositório Institucional da UFBA - Universidade Federal da Bahia (UFBA)false
dc.title.pt_BR.fl_str_mv Determination of Mo and V in multiphase gasoline emulsions by electrothermal atomic absorption spectrometry
dc.title.alternative.pt_BR.fl_str_mv Spectrochimica Acta Part B: Atomic Spectroscopy
title Determination of Mo and V in multiphase gasoline emulsions by electrothermal atomic absorption spectrometry
spellingShingle Determination of Mo and V in multiphase gasoline emulsions by electrothermal atomic absorption spectrometry
Santos, Denilson Santana Sodré dos
Gasoline
Multiphase emulsion
Electrothermal atomic absorption spectrometry
title_short Determination of Mo and V in multiphase gasoline emulsions by electrothermal atomic absorption spectrometry
title_full Determination of Mo and V in multiphase gasoline emulsions by electrothermal atomic absorption spectrometry
title_fullStr Determination of Mo and V in multiphase gasoline emulsions by electrothermal atomic absorption spectrometry
title_full_unstemmed Determination of Mo and V in multiphase gasoline emulsions by electrothermal atomic absorption spectrometry
title_sort Determination of Mo and V in multiphase gasoline emulsions by electrothermal atomic absorption spectrometry
author Santos, Denilson Santana Sodré dos
author_facet Santos, Denilson Santana Sodré dos
Teixeira, Alete Paixão
Korn, Maria das Graças Andrade
author_role author
author2 Teixeira, Alete Paixão
Korn, Maria das Graças Andrade
author2_role author
author
dc.contributor.author.fl_str_mv Santos, Denilson Santana Sodré dos
Teixeira, Alete Paixão
Korn, Maria das Graças Andrade
Santos, Denilson Santana Sodré dos
Teixeira, Alete Paixão
Korn, Maria das Graças Andrade
dc.subject.por.fl_str_mv Gasoline
Multiphase emulsion
Electrothermal atomic absorption spectrometry
topic Gasoline
Multiphase emulsion
Electrothermal atomic absorption spectrometry
description Texto completo: acesso restrito. p.592–595
publishDate 2006
dc.date.issued.fl_str_mv 2006
dc.date.accessioned.fl_str_mv 2013-08-27T10:59:11Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv http://www.repositorio.ufba.br/ri/handle/ri/12742
dc.identifier.issn.none.fl_str_mv 0584-8547
dc.identifier.number.pt_BR.fl_str_mv v.61 n. 5
identifier_str_mv 0584-8547
v.61 n. 5
url http://www.repositorio.ufba.br/ri/handle/ri/12742
dc.language.iso.fl_str_mv eng
language eng
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.source.pt_BR.fl_str_mv http://dx.doi.org.ez10.periodicos.capes.gov.br/10.1016/j.sab.2006.03.010
dc.source.none.fl_str_mv reponame:Repositório Institucional da UFBA
instname:Universidade Federal da Bahia (UFBA)
instacron:UFBA
instname_str Universidade Federal da Bahia (UFBA)
instacron_str UFBA
institution UFBA
reponame_str Repositório Institucional da UFBA
collection Repositório Institucional da UFBA
bitstream.url.fl_str_mv https://repositorio.ufba.br/bitstream/ri/12742/1/1-s2.0-S0584854706000917-main.pdf
https://repositorio.ufba.br/bitstream/ri/12742/2/license.txt
https://repositorio.ufba.br/bitstream/ri/12742/3/1-s2.0-S0584854706000917-main.pdf.txt
bitstream.checksum.fl_str_mv 1765d1a83889c3a6c930bea33eab946b
1b89a9a0548218172d7c829f87a0eab9
e66d6c7bf6817ca0d048ce0104ecc9b5
bitstream.checksumAlgorithm.fl_str_mv MD5
MD5
MD5
repository.name.fl_str_mv Repositório Institucional da UFBA - Universidade Federal da Bahia (UFBA)
repository.mail.fl_str_mv
_version_ 1808459456346849280