Determination of mercury in airborne particulate matter collected on glass fiber filters using high-resolution continuum source graphite furnace atomic absorption spectrometry and direct solid sampling
Autor(a) principal: | |
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Data de Publicação: | 2011 |
Outros Autores: | , , , , , , , |
Tipo de documento: | Artigo |
Idioma: | eng |
Título da fonte: | Repositório Institucional da UFBA |
Texto Completo: | http://www.repositorio.ufba.br/ri/handle/ri/5394 |
Resumo: | Acesso restrito: Texto completo. |
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Araujo, Rennan Geovanny OliveiraVignola, FabíolaCastilho, Ivan N. B.Borges, Daniel L. G.Welz, BernhardVale, Maria Goreti R.Smichowski, PatriciaFerreira, Sergio Luis CostaBecker-Ross, HelmutAraujo, Rennan Geovanny OliveiraVignola, FabíolaCastilho, Ivan N. B.Borges, Daniel L. G.Welz, BernhardVale, Maria Goreti R.Smichowski, PatriciaFerreira, Sergio Luis CostaBecker-Ross, Helmut2012-02-13T17:53:21Z2011-050584-8547http://www.repositorio.ufba.br/ri/handle/ri/5394v. 66, n. 5.Acesso restrito: Texto completo.A study has been undertaken to assess the capability of high-resolution continuum source graphite furnace atomic absorption spectrometry for the determination ofmercury in airborne particulate matter (APM) collected on glass fiber filters using direct solid sampling. The main Hg absorption line at 253.652 nm was used for all determinations. The certified referencematerial NIST SRM1648 (Urban ParticulateMatter)was used to check the accuracy of the method, and good agreement was obtained between published and determined values. The characteristic mass was 22 pg Hg. The limit of detection (3σ), based on ten atomizations of an unexposed filter, was 40 ng g−1, corresponding to 0.12 ng m−3 in the air for a typical air volumeof 1440 m3 collectedwithin 24 h.The limit of quantification was 150 ng g−1, equivalent to 0.41 ng m−3 in the air. The repeatability of measurements was better than 17% RSD (n=5). Mercury concentrations found in filter samples loaded with APM collected in Buenos Aires, Argentina, were between b40 ng g−1 and 381±24 ng g−1. These values correspond to a mercury concentration in the air between b0.12 ng m−3 and 1.47±0.09 ng m−3. The proposed procedurewas found to be simple, fast and reliable, and suitable as a screening procedure for the determination of mercury in APM samples.Submitted by JURANDI DE SOUZA SILVA (jssufba@hotmail.com) on 2012-02-13T17:53:21Z No. of bitstreams: 1 __pdn.sciencedirect.com_....0-S0584854711000978-main.pdf: 258952 bytes, checksum: 86bd33481332a9aab32e51e65899989a (MD5)Made available in DSpace on 2012-02-13T17:53:21Z (GMT). No. of bitstreams: 1 __pdn.sciencedirect.com_....0-S0584854711000978-main.pdf: 258952 bytes, checksum: 86bd33481332a9aab32e51e65899989a (MD5) Previous issue date: 2011-05DOI: 10.1016/j.sab.2011.05.004reponame:Repositório Institucional da UFBAinstname:Universidade Federal da Bahia (UFBA)instacron:UFBAMercury determinationGlass fiber filterAirborne particulate matterDirect solid sampling analysisHR-CS GF AASDetermination of mercury in airborne particulate matter collected on glass fiber filters using high-resolution continuum source graphite furnace atomic absorption spectrometry and direct solid samplingSpectrochimica Acta Part B-Atomic Spectroscopyinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/article10000-01-01enginfo:eu-repo/semantics/openAccessORIGINAL__pdn.sciencedirect.com_....0-S0584854711000978-main.pdf__pdn.sciencedirect.com_....0-S0584854711000978-main.pdfapplication/pdf258952https://repositorio.ufba.br/bitstream/ri/5394/1/__pdn.sciencedirect.com_....0-S0584854711000978-main.pdf86bd33481332a9aab32e51e65899989aMD51LICENSElicense.txtlicense.txttext/plain1762https://repositorio.ufba.br/bitstream/ri/5394/2/license.txt1b89a9a0548218172d7c829f87a0eab9MD52TEXT__pdn.sciencedirect.com_....0-S0584854711000978-main.pdf.txt__pdn.sciencedirect.com_....0-S0584854711000978-main.pdf.txtExtracted texttext/plain32161https://repositorio.ufba.br/bitstream/ri/5394/3/__pdn.sciencedirect.com_....0-S0584854711000978-main.pdf.txt3218c2f01cf851d0dce92acc06f284cbMD53ri/53942022-07-05 14:03:11.996oai:repositorio.ufba.br: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Repositório InstitucionalPUBhttp://192.188.11.11:8080/oai/requestopendoar:19322022-07-05T17:03:11Repositório Institucional da UFBA - Universidade Federal da Bahia (UFBA)false |
dc.title.pt_BR.fl_str_mv |
Determination of mercury in airborne particulate matter collected on glass fiber filters using high-resolution continuum source graphite furnace atomic absorption spectrometry and direct solid sampling |
dc.title.alternative.pt_BR.fl_str_mv |
Spectrochimica Acta Part B-Atomic Spectroscopy |
title |
Determination of mercury in airborne particulate matter collected on glass fiber filters using high-resolution continuum source graphite furnace atomic absorption spectrometry and direct solid sampling |
spellingShingle |
Determination of mercury in airborne particulate matter collected on glass fiber filters using high-resolution continuum source graphite furnace atomic absorption spectrometry and direct solid sampling Araujo, Rennan Geovanny Oliveira Mercury determination Glass fiber filter Airborne particulate matter Direct solid sampling analysis HR-CS GF AAS |
title_short |
Determination of mercury in airborne particulate matter collected on glass fiber filters using high-resolution continuum source graphite furnace atomic absorption spectrometry and direct solid sampling |
title_full |
Determination of mercury in airborne particulate matter collected on glass fiber filters using high-resolution continuum source graphite furnace atomic absorption spectrometry and direct solid sampling |
title_fullStr |
Determination of mercury in airborne particulate matter collected on glass fiber filters using high-resolution continuum source graphite furnace atomic absorption spectrometry and direct solid sampling |
title_full_unstemmed |
Determination of mercury in airborne particulate matter collected on glass fiber filters using high-resolution continuum source graphite furnace atomic absorption spectrometry and direct solid sampling |
title_sort |
Determination of mercury in airborne particulate matter collected on glass fiber filters using high-resolution continuum source graphite furnace atomic absorption spectrometry and direct solid sampling |
author |
Araujo, Rennan Geovanny Oliveira |
author_facet |
Araujo, Rennan Geovanny Oliveira Vignola, Fabíola Castilho, Ivan N. B. Borges, Daniel L. G. Welz, Bernhard Vale, Maria Goreti R. Smichowski, Patricia Ferreira, Sergio Luis Costa Becker-Ross, Helmut |
author_role |
author |
author2 |
Vignola, Fabíola Castilho, Ivan N. B. Borges, Daniel L. G. Welz, Bernhard Vale, Maria Goreti R. Smichowski, Patricia Ferreira, Sergio Luis Costa Becker-Ross, Helmut |
author2_role |
author author author author author author author author |
dc.contributor.author.fl_str_mv |
Araujo, Rennan Geovanny Oliveira Vignola, Fabíola Castilho, Ivan N. B. Borges, Daniel L. G. Welz, Bernhard Vale, Maria Goreti R. Smichowski, Patricia Ferreira, Sergio Luis Costa Becker-Ross, Helmut Araujo, Rennan Geovanny Oliveira Vignola, Fabíola Castilho, Ivan N. B. Borges, Daniel L. G. Welz, Bernhard Vale, Maria Goreti R. Smichowski, Patricia Ferreira, Sergio Luis Costa Becker-Ross, Helmut |
dc.subject.por.fl_str_mv |
Mercury determination Glass fiber filter Airborne particulate matter Direct solid sampling analysis HR-CS GF AAS |
topic |
Mercury determination Glass fiber filter Airborne particulate matter Direct solid sampling analysis HR-CS GF AAS |
description |
Acesso restrito: Texto completo. |
publishDate |
2011 |
dc.date.issued.fl_str_mv |
2011-05 |
dc.date.accessioned.fl_str_mv |
2012-02-13T17:53:21Z |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
http://www.repositorio.ufba.br/ri/handle/ri/5394 |
dc.identifier.issn.none.fl_str_mv |
0584-8547 |
dc.identifier.number.pt_BR.fl_str_mv |
v. 66, n. 5. |
identifier_str_mv |
0584-8547 v. 66, n. 5. |
url |
http://www.repositorio.ufba.br/ri/handle/ri/5394 |
dc.language.iso.fl_str_mv |
eng |
language |
eng |
dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess |
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openAccess |
dc.source.pt_BR.fl_str_mv |
DOI: 10.1016/j.sab.2011.05.004 |
dc.source.none.fl_str_mv |
reponame:Repositório Institucional da UFBA instname:Universidade Federal da Bahia (UFBA) instacron:UFBA |
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Universidade Federal da Bahia (UFBA) |
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UFBA |
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UFBA |
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Repositório Institucional da UFBA |
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Repositório Institucional da UFBA |
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