Determination of mercury in airborne particulate matter collected on glass fiber filters using high-resolution continuum source graphite furnace atomic absorption spectrometry and direct solid sampling

Detalhes bibliográficos
Autor(a) principal: Araujo, Rennan Geovanny Oliveira
Data de Publicação: 2011
Outros Autores: Vignola, Fabíola, Castilho, Ivan N. B., Borges, Daniel L. G., Welz, Bernhard, Vale, Maria Goreti R., Smichowski, Patricia, Ferreira, Sergio Luis Costa, Becker-Ross, Helmut
Tipo de documento: Artigo
Idioma: eng
Título da fonte: Repositório Institucional da UFBA
Texto Completo: http://www.repositorio.ufba.br/ri/handle/ri/5394
Resumo: Acesso restrito: Texto completo.
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spelling Araujo, Rennan Geovanny OliveiraVignola, FabíolaCastilho, Ivan N. B.Borges, Daniel L. G.Welz, BernhardVale, Maria Goreti R.Smichowski, PatriciaFerreira, Sergio Luis CostaBecker-Ross, HelmutAraujo, Rennan Geovanny OliveiraVignola, FabíolaCastilho, Ivan N. B.Borges, Daniel L. G.Welz, BernhardVale, Maria Goreti R.Smichowski, PatriciaFerreira, Sergio Luis CostaBecker-Ross, Helmut2012-02-13T17:53:21Z2011-050584-8547http://www.repositorio.ufba.br/ri/handle/ri/5394v. 66, n. 5.Acesso restrito: Texto completo.A study has been undertaken to assess the capability of high-resolution continuum source graphite furnace atomic absorption spectrometry for the determination ofmercury in airborne particulate matter (APM) collected on glass fiber filters using direct solid sampling. The main Hg absorption line at 253.652 nm was used for all determinations. The certified referencematerial NIST SRM1648 (Urban ParticulateMatter)was used to check the accuracy of the method, and good agreement was obtained between published and determined values. The characteristic mass was 22 pg Hg. The limit of detection (3σ), based on ten atomizations of an unexposed filter, was 40 ng g−1, corresponding to 0.12 ng m−3 in the air for a typical air volumeof 1440 m3 collectedwithin 24 h.The limit of quantification was 150 ng g−1, equivalent to 0.41 ng m−3 in the air. The repeatability of measurements was better than 17% RSD (n=5). Mercury concentrations found in filter samples loaded with APM collected in Buenos Aires, Argentina, were between b40 ng g−1 and 381±24 ng g−1. These values correspond to a mercury concentration in the air between b0.12 ng m−3 and 1.47±0.09 ng m−3. The proposed procedurewas found to be simple, fast and reliable, and suitable as a screening procedure for the determination of mercury in APM samples.Submitted by JURANDI DE SOUZA SILVA (jssufba@hotmail.com) on 2012-02-13T17:53:21Z No. of bitstreams: 1 __pdn.sciencedirect.com_....0-S0584854711000978-main.pdf: 258952 bytes, checksum: 86bd33481332a9aab32e51e65899989a (MD5)Made available in DSpace on 2012-02-13T17:53:21Z (GMT). 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dc.title.pt_BR.fl_str_mv Determination of mercury in airborne particulate matter collected on glass fiber filters using high-resolution continuum source graphite furnace atomic absorption spectrometry and direct solid sampling
dc.title.alternative.pt_BR.fl_str_mv Spectrochimica Acta Part B-Atomic Spectroscopy
title Determination of mercury in airborne particulate matter collected on glass fiber filters using high-resolution continuum source graphite furnace atomic absorption spectrometry and direct solid sampling
spellingShingle Determination of mercury in airborne particulate matter collected on glass fiber filters using high-resolution continuum source graphite furnace atomic absorption spectrometry and direct solid sampling
Araujo, Rennan Geovanny Oliveira
Mercury determination
Glass fiber filter
Airborne particulate matter
Direct solid sampling analysis
HR-CS GF AAS
title_short Determination of mercury in airborne particulate matter collected on glass fiber filters using high-resolution continuum source graphite furnace atomic absorption spectrometry and direct solid sampling
title_full Determination of mercury in airborne particulate matter collected on glass fiber filters using high-resolution continuum source graphite furnace atomic absorption spectrometry and direct solid sampling
title_fullStr Determination of mercury in airborne particulate matter collected on glass fiber filters using high-resolution continuum source graphite furnace atomic absorption spectrometry and direct solid sampling
title_full_unstemmed Determination of mercury in airborne particulate matter collected on glass fiber filters using high-resolution continuum source graphite furnace atomic absorption spectrometry and direct solid sampling
title_sort Determination of mercury in airborne particulate matter collected on glass fiber filters using high-resolution continuum source graphite furnace atomic absorption spectrometry and direct solid sampling
author Araujo, Rennan Geovanny Oliveira
author_facet Araujo, Rennan Geovanny Oliveira
Vignola, Fabíola
Castilho, Ivan N. B.
Borges, Daniel L. G.
Welz, Bernhard
Vale, Maria Goreti R.
Smichowski, Patricia
Ferreira, Sergio Luis Costa
Becker-Ross, Helmut
author_role author
author2 Vignola, Fabíola
Castilho, Ivan N. B.
Borges, Daniel L. G.
Welz, Bernhard
Vale, Maria Goreti R.
Smichowski, Patricia
Ferreira, Sergio Luis Costa
Becker-Ross, Helmut
author2_role author
author
author
author
author
author
author
author
dc.contributor.author.fl_str_mv Araujo, Rennan Geovanny Oliveira
Vignola, Fabíola
Castilho, Ivan N. B.
Borges, Daniel L. G.
Welz, Bernhard
Vale, Maria Goreti R.
Smichowski, Patricia
Ferreira, Sergio Luis Costa
Becker-Ross, Helmut
Araujo, Rennan Geovanny Oliveira
Vignola, Fabíola
Castilho, Ivan N. B.
Borges, Daniel L. G.
Welz, Bernhard
Vale, Maria Goreti R.
Smichowski, Patricia
Ferreira, Sergio Luis Costa
Becker-Ross, Helmut
dc.subject.por.fl_str_mv Mercury determination
Glass fiber filter
Airborne particulate matter
Direct solid sampling analysis
HR-CS GF AAS
topic Mercury determination
Glass fiber filter
Airborne particulate matter
Direct solid sampling analysis
HR-CS GF AAS
description Acesso restrito: Texto completo.
publishDate 2011
dc.date.issued.fl_str_mv 2011-05
dc.date.accessioned.fl_str_mv 2012-02-13T17:53:21Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
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status_str publishedVersion
dc.identifier.uri.fl_str_mv http://www.repositorio.ufba.br/ri/handle/ri/5394
dc.identifier.issn.none.fl_str_mv 0584-8547
dc.identifier.number.pt_BR.fl_str_mv v. 66, n. 5.
identifier_str_mv 0584-8547
v. 66, n. 5.
url http://www.repositorio.ufba.br/ri/handle/ri/5394
dc.language.iso.fl_str_mv eng
language eng
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.source.pt_BR.fl_str_mv DOI: 10.1016/j.sab.2011.05.004
dc.source.none.fl_str_mv reponame:Repositório Institucional da UFBA
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