Alternativas analíticas para determinação de ferro e titânio em cimento Portland

Detalhes bibliográficos
Autor(a) principal: Franco Junior, Jorge de Oliveira
Data de Publicação: 2001
Outros Autores: Korn, Maria das Graças Andrade, Costa, Antonio Celso Spinola, Santos Junior, Aníbal de Freitas, Teixeira, Leonardo Sena Gomes
Tipo de documento: Artigo
Idioma: por
Título da fonte: Repositório Institucional da UFBA
Texto Completo: http://www.repositorio.ufba.br/ri/handle/ri/4700
Resumo: p. 195-199.
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spelling Franco Junior, Jorge de OliveiraKorn, Maria das Graças AndradeCosta, Antonio Celso SpinolaSantos Junior, Aníbal de FreitasTeixeira, Leonardo Sena GomesFranco Junior, Jorge de OliveiraKorn, Maria das Graças AndradeCosta, Antonio Celso SpinolaSantos Junior, Aníbal de FreitasTeixeira, Leonardo Sena Gomes2011-11-25T19:41:40Z2011-11-25T19:41:40Z20010100-4042http://www.repositorio.ufba.br/ri/handle/ri/4700v. 24, n. 2.p. 195-199.Comparative study of analytical methods for iron and titanium determination in Portland cement. In the present work four different analytical methodologies were studied for the determination of iron and titanium in Portland cement. The cement samples were dissolved with hot HCl and HF, being compared Fe and Ti concentrations through four analytical methods: molecular absorption spectrophotometry using the reagents 1,2-hydroxybenzene-3,5-disulfonic acid (Tiron) and the 5-chloro-salicylic acid (CSA), inductively coupled plasma atomic emission spectrometry (ICP-AES) and flame atomic absorption spectrophotometry (FAAS). In the spectrophotometric determinations were studied pH conditions, reagents addition order, interferences, amount of reagents, linear range and stability of the system. In the techniques of ICP-AES and FAAS were studied the best lines, interferences, sensibility and linear range. The obtained results were compared and the agreement was evaluated among the methods for the determination of the metals of interest.Submitted by JURANDI DE SOUZA SILVA (jssufba@hotmail.com) on 2011-11-25T19:41:40Z No. of bitstreams: 1 4281.pdf: 47758 bytes, checksum: 30d179a206d48c8aa8e36edb2a7c2cb3 (MD5)Made available in DSpace on 2011-11-25T19:41:40Z (GMT). No. of bitstreams: 1 4281.pdf: 47758 bytes, checksum: 30d179a206d48c8aa8e36edb2a7c2cb3 (MD5) Previous issue date: 2001São PauloPortland cementiron determinationtitanium determinationAlternativas analíticas para determinação de ferro e titânio em cimento PortlandQuímica Novainfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/articleporreponame:Repositório Institucional da UFBAinstname:Universidade Federal da Bahia (UFBA)instacron:UFBAinfo:eu-repo/semantics/openAccessLICENSElicense.txtlicense.txttext/plain1906https://repositorio.ufba.br/bitstream/ri/4700/2/license.txt87f418423b0afd58ee3c9be120c0d47eMD52ORIGINAL4281.pdf4281.pdfapplication/pdf47758https://repositorio.ufba.br/bitstream/ri/4700/1/4281.pdf30d179a206d48c8aa8e36edb2a7c2cb3MD51TEXT4281.pdf.txt4281.pdf.txtExtracted texttext/plain26453https://repositorio.ufba.br/bitstream/ri/4700/3/4281.pdf.txtb4c1b7ecb066ed52c2c10ce76f995fcdMD53ri/47002022-07-05 14:03:44.347oai:repositorio.ufba.br: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Repositório InstitucionalPUBhttp://192.188.11.11:8080/oai/requestopendoar:19322022-07-05T17:03:44Repositório Institucional da UFBA - Universidade Federal da Bahia (UFBA)false
dc.title.pt_BR.fl_str_mv Alternativas analíticas para determinação de ferro e titânio em cimento Portland
dc.title.alternative.pt_BR.fl_str_mv Química Nova
title Alternativas analíticas para determinação de ferro e titânio em cimento Portland
spellingShingle Alternativas analíticas para determinação de ferro e titânio em cimento Portland
Franco Junior, Jorge de Oliveira
Portland cement
iron determination
titanium determination
title_short Alternativas analíticas para determinação de ferro e titânio em cimento Portland
title_full Alternativas analíticas para determinação de ferro e titânio em cimento Portland
title_fullStr Alternativas analíticas para determinação de ferro e titânio em cimento Portland
title_full_unstemmed Alternativas analíticas para determinação de ferro e titânio em cimento Portland
title_sort Alternativas analíticas para determinação de ferro e titânio em cimento Portland
author Franco Junior, Jorge de Oliveira
author_facet Franco Junior, Jorge de Oliveira
Korn, Maria das Graças Andrade
Costa, Antonio Celso Spinola
Santos Junior, Aníbal de Freitas
Teixeira, Leonardo Sena Gomes
author_role author
author2 Korn, Maria das Graças Andrade
Costa, Antonio Celso Spinola
Santos Junior, Aníbal de Freitas
Teixeira, Leonardo Sena Gomes
author2_role author
author
author
author
dc.contributor.author.fl_str_mv Franco Junior, Jorge de Oliveira
Korn, Maria das Graças Andrade
Costa, Antonio Celso Spinola
Santos Junior, Aníbal de Freitas
Teixeira, Leonardo Sena Gomes
Franco Junior, Jorge de Oliveira
Korn, Maria das Graças Andrade
Costa, Antonio Celso Spinola
Santos Junior, Aníbal de Freitas
Teixeira, Leonardo Sena Gomes
dc.subject.por.fl_str_mv Portland cement
iron determination
titanium determination
topic Portland cement
iron determination
titanium determination
description p. 195-199.
publishDate 2001
dc.date.issued.fl_str_mv 2001
dc.date.accessioned.fl_str_mv 2011-11-25T19:41:40Z
dc.date.available.fl_str_mv 2011-11-25T19:41:40Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
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dc.identifier.issn.none.fl_str_mv 0100-4042
dc.identifier.number.pt_BR.fl_str_mv v. 24, n. 2.
identifier_str_mv 0100-4042
v. 24, n. 2.
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