Alternativas analíticas para determinação de ferro e titânio em cimento Portland
Autor(a) principal: | |
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Data de Publicação: | 2001 |
Outros Autores: | , , , |
Tipo de documento: | Artigo |
Idioma: | por |
Título da fonte: | Repositório Institucional da UFBA |
Texto Completo: | http://www.repositorio.ufba.br/ri/handle/ri/4700 |
Resumo: | p. 195-199. |
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Franco Junior, Jorge de OliveiraKorn, Maria das Graças AndradeCosta, Antonio Celso SpinolaSantos Junior, Aníbal de FreitasTeixeira, Leonardo Sena GomesFranco Junior, Jorge de OliveiraKorn, Maria das Graças AndradeCosta, Antonio Celso SpinolaSantos Junior, Aníbal de FreitasTeixeira, Leonardo Sena Gomes2011-11-25T19:41:40Z2011-11-25T19:41:40Z20010100-4042http://www.repositorio.ufba.br/ri/handle/ri/4700v. 24, n. 2.p. 195-199.Comparative study of analytical methods for iron and titanium determination in Portland cement. In the present work four different analytical methodologies were studied for the determination of iron and titanium in Portland cement. The cement samples were dissolved with hot HCl and HF, being compared Fe and Ti concentrations through four analytical methods: molecular absorption spectrophotometry using the reagents 1,2-hydroxybenzene-3,5-disulfonic acid (Tiron) and the 5-chloro-salicylic acid (CSA), inductively coupled plasma atomic emission spectrometry (ICP-AES) and flame atomic absorption spectrophotometry (FAAS). In the spectrophotometric determinations were studied pH conditions, reagents addition order, interferences, amount of reagents, linear range and stability of the system. In the techniques of ICP-AES and FAAS were studied the best lines, interferences, sensibility and linear range. The obtained results were compared and the agreement was evaluated among the methods for the determination of the metals of interest.Submitted by JURANDI DE SOUZA SILVA (jssufba@hotmail.com) on 2011-11-25T19:41:40Z No. of bitstreams: 1 4281.pdf: 47758 bytes, checksum: 30d179a206d48c8aa8e36edb2a7c2cb3 (MD5)Made available in DSpace on 2011-11-25T19:41:40Z (GMT). No. of bitstreams: 1 4281.pdf: 47758 bytes, checksum: 30d179a206d48c8aa8e36edb2a7c2cb3 (MD5) Previous issue date: 2001São PauloPortland cementiron determinationtitanium determinationAlternativas analíticas para determinação de ferro e titânio em cimento PortlandQuímica Novainfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/articleporreponame:Repositório Institucional da UFBAinstname:Universidade Federal da Bahia (UFBA)instacron:UFBAinfo:eu-repo/semantics/openAccessLICENSElicense.txtlicense.txttext/plain1906https://repositorio.ufba.br/bitstream/ri/4700/2/license.txt87f418423b0afd58ee3c9be120c0d47eMD52ORIGINAL4281.pdf4281.pdfapplication/pdf47758https://repositorio.ufba.br/bitstream/ri/4700/1/4281.pdf30d179a206d48c8aa8e36edb2a7c2cb3MD51TEXT4281.pdf.txt4281.pdf.txtExtracted texttext/plain26453https://repositorio.ufba.br/bitstream/ri/4700/3/4281.pdf.txtb4c1b7ecb066ed52c2c10ce76f995fcdMD53ri/47002022-07-05 14:03:44.347oai:repositorio.ufba.br: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Repositório InstitucionalPUBhttp://192.188.11.11:8080/oai/requestopendoar:19322022-07-05T17:03:44Repositório Institucional da UFBA - Universidade Federal da Bahia (UFBA)false |
dc.title.pt_BR.fl_str_mv |
Alternativas analíticas para determinação de ferro e titânio em cimento Portland |
dc.title.alternative.pt_BR.fl_str_mv |
Química Nova |
title |
Alternativas analíticas para determinação de ferro e titânio em cimento Portland |
spellingShingle |
Alternativas analíticas para determinação de ferro e titânio em cimento Portland Franco Junior, Jorge de Oliveira Portland cement iron determination titanium determination |
title_short |
Alternativas analíticas para determinação de ferro e titânio em cimento Portland |
title_full |
Alternativas analíticas para determinação de ferro e titânio em cimento Portland |
title_fullStr |
Alternativas analíticas para determinação de ferro e titânio em cimento Portland |
title_full_unstemmed |
Alternativas analíticas para determinação de ferro e titânio em cimento Portland |
title_sort |
Alternativas analíticas para determinação de ferro e titânio em cimento Portland |
author |
Franco Junior, Jorge de Oliveira |
author_facet |
Franco Junior, Jorge de Oliveira Korn, Maria das Graças Andrade Costa, Antonio Celso Spinola Santos Junior, Aníbal de Freitas Teixeira, Leonardo Sena Gomes |
author_role |
author |
author2 |
Korn, Maria das Graças Andrade Costa, Antonio Celso Spinola Santos Junior, Aníbal de Freitas Teixeira, Leonardo Sena Gomes |
author2_role |
author author author author |
dc.contributor.author.fl_str_mv |
Franco Junior, Jorge de Oliveira Korn, Maria das Graças Andrade Costa, Antonio Celso Spinola Santos Junior, Aníbal de Freitas Teixeira, Leonardo Sena Gomes Franco Junior, Jorge de Oliveira Korn, Maria das Graças Andrade Costa, Antonio Celso Spinola Santos Junior, Aníbal de Freitas Teixeira, Leonardo Sena Gomes |
dc.subject.por.fl_str_mv |
Portland cement iron determination titanium determination |
topic |
Portland cement iron determination titanium determination |
description |
p. 195-199. |
publishDate |
2001 |
dc.date.issued.fl_str_mv |
2001 |
dc.date.accessioned.fl_str_mv |
2011-11-25T19:41:40Z |
dc.date.available.fl_str_mv |
2011-11-25T19:41:40Z |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
http://www.repositorio.ufba.br/ri/handle/ri/4700 |
dc.identifier.issn.none.fl_str_mv |
0100-4042 |
dc.identifier.number.pt_BR.fl_str_mv |
v. 24, n. 2. |
identifier_str_mv |
0100-4042 v. 24, n. 2. |
url |
http://www.repositorio.ufba.br/ri/handle/ri/4700 |
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por |
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por |
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openAccess |
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